#------------------------------------------------------------------------------ #$Date: 2016-04-06 16:41:11 +0300 (Wed, 06 Apr 2016) $ #$Revision: 181871 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/02/01/2020104.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_2020104 _cell_angle_alpha 80.946 _cell_angle_beta 79.029 _cell_angle_gamma 87.039 _cell_length_a 13.0174 _cell_length_b 14.3273 _cell_length_c 24.1557 _exptl_crystal_F_000 1708.00 _reflns_d_resolution_high 0.7445 _cod_data_source_file fn3203Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' FeTpivPP_KCl20130726 in P-1 No2' _shelx_refln_list_code 4 _shelx_f_calc_maximum 356.86 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 633.72 901.46 38.54 o 3 0 0 21007.12 19284.55 169.27 o 4 0 0 13093.00 14271.10 158.46 o 5 0 0 367.83 352.14 13.21 o 6 0 0 3522.27 3937.50 43.05 o 7 0 0 4.59 11.20 8.65 o 8 0 0 32.79 14.70 9.52 o 9 0 0 150.63 144.07 15.34 o 10 0 0 10.43 51.46 17.53 o 11 0 0 1316.82 1326.59 46.71 o 12 0 0 0.58 -14.31 28.57 o 13 0 0 465.14 414.53 65.06 o 14 0 0 469.71 562.12 57.79 o 15 0 0 53.79 92.71 61.07 o -15 1 0 58.98 119.09 72.05 o -14 1 0 0.53 5.43 53.52 o -13 1 0 308.03 360.13 94.88 o -12 1 0 1.04 24.42 37.42 o -11 1 0 828.27 855.74 52.63 o -10 1 0 862.61 986.81 35.13 o -9 1 0 311.55 309.09 22.82 o -8 1 0 0.37 11.77 13.15 o -7 1 0 846.61 903.96 25.29 o -6 1 0 12256.26 12216.11 92.92 o -5 1 0 1287.50 1228.31 23.13 o -4 1 0 4761.42 4621.00 48.35 o -3 1 0 127346.19 131551.69 484.76 o -2 1 0 9764.83 9676.71 227.02 o 2 1 0 551.67 473.32 27.34 o 3 1 0 11508.63 12777.22 59.57 o 4 1 0 2924.72 2957.32 34.05 o 5 1 0 686.93 920.87 19.49 o 6 1 0 5803.67 5736.18 51.09 o 7 1 0 1223.08 1031.46 24.08 o 8 1 0 362.46 389.54 17.23 o 9 1 0 64.07 86.04 12.78 o 10 1 0 1239.97 1160.03 40.69 o 11 1 0 1.35 16.38 25.41 o 12 1 0 1739.95 1738.47 85.39 o 13 1 0 21.67 9.93 25.99 o 14 1 0 10.61 38.23 33.37 o 15 1 0 74.26 209.63 84.63 o -15 2 0 2.34 -40.77 58.69 o -14 2 0 138.93 284.01 81.40 o -13 2 0 279.03 305.97 52.22 o -12 2 0 331.63 276.56 40.86 o -11 2 0 11.83 -0.23 16.48 o -10 2 0 1528.62 1473.31 42.53 o -9 2 0 322.14 385.71 31.61 o -8 2 0 25.24 24.87 11.48 o -7 2 0 163.03 156.99 20.37 o -6 2 0 6681.45 7253.37 61.53 o -5 2 0 129.58 136.89 12.35 o -4 2 0 10021.14 10447.95 80.67 o -3 2 0 43832.59 45098.45 170.94 o -2 2 0 69815.15 66904.07 194.04 o -1 2 0 9008.46 8759.55 79.29 o 1 2 0 674.35 649.27 20.79 o 2 2 0 258.16 374.72 19.56 o 3 2 0 45.22 346.05 50.75 o 4 2 0 7069.78 7481.23 95.34 o 5 2 0 524.63 530.79 17.22 o 6 2 0 355.10 404.94 16.39 o 7 2 0 141.51 160.57 11.55 o 8 2 0 61.09 70.32 10.20 o 9 2 0 100.31 122.70 20.89 o 10 2 0 437.19 423.30 21.38 o 11 2 0 2733.82 3016.02 101.35 o 12 2 0 272.13 266.48 39.67 o 13 2 0 851.42 955.26 68.63 o 14 2 0 13.18 -8.67 28.30 o 15 2 0 220.19 220.11 66.34 o -15 3 0 16.99 -73.49 73.49 o -14 3 0 11.56 59.06 59.17 o -13 3 0 38.56 48.24 28.71 o -12 3 0 25.40 -8.22 27.32 o -11 3 0 2081.66 2271.52 121.15 o -10 3 0 1.91 -3.57 16.90 o -9 3 0 1889.22 1955.30 61.62 o -8 3 0 988.63 1062.51 35.77 o -7 3 0 2616.14 2887.88 51.19 o -6 3 0 11863.00 12530.38 107.16 o -5 3 0 11084.00 11444.40 79.94 o -4 3 0 967.30 1048.15 31.66 o -3 3 0 9.22 -2.35 11.01 o -2 3 0 264.18 256.17 19.65 o -1 3 0 9791.56 10049.68 100.48 o 0 3 0 122.87 106.03 15.01 o 1 3 0 3777.88 3942.25 61.50 o 2 3 0 3662.90 3988.88 61.07 o 3 3 0 9426.93 9164.74 164.90 o 4 3 0 4777.68 4437.23 61.67 o 5 3 0 1287.96 1331.67 35.93 o 6 3 0 684.51 690.10 27.55 o 7 3 0 104.15 68.32 24.52 o 8 3 0 636.32 787.93 35.50 o 9 3 0 58.31 42.84 14.46 o 10 3 0 338.92 390.96 43.08 o 11 3 0 500.86 478.84 47.53 o 12 3 0 1262.33 1355.91 75.86 o 13 3 0 194.45 192.59 59.58 o 14 3 0 68.39 129.98 34.06 o 15 3 0 0.58 -72.06 72.06 o 16 3 0 155.76 434.22 95.19 o -15 4 0 15.87 20.37 61.69 o -14 4 0 0.48 -63.27 67.80 o -13 4 0 390.15 456.33 53.39 o -12 4 0 75.55 110.39 55.23 o -11 4 0 252.98 170.89 25.85 o -10 4 0 361.22 332.02 32.09 o -9 4 0 132.87 98.14 22.13 o -8 4 0 178.13 145.27 16.74 o -7 4 0 2442.28 2353.64 63.19 o -6 4 0 1038.96 1234.62 37.08 o -5 4 0 5436.43 5766.74 65.63 o -4 4 0 3001.27 3070.66 46.30 o -3 4 0 4593.63 4389.47 57.55 o -2 4 0 3191.83 3020.90 75.81 o -1 4 0 6010.21 5504.43 70.76 o 0 4 0 7077.94 6437.90 125.52 o 1 4 0 13663.19 14543.98 107.11 o 2 4 0 1185.47 1085.51 39.12 o 3 4 0 4550.39 4339.74 72.99 o 4 4 0 2225.67 2232.27 49.33 o 5 4 0 3142.71 3396.63 71.73 o 6 4 0 297.82 375.86 51.29 o 7 4 0 127.04 80.38 17.40 o 8 4 0 284.28 303.92 48.27 o 9 4 0 7.20 27.44 19.45 o 10 4 0 279.34 266.99 41.23 o 11 4 0 109.60 190.89 35.09 o 12 4 0 187.20 203.71 36.70 o 13 4 0 1.35 31.81 30.83 o 14 4 0 120.67 250.01 71.80 o 15 4 0 655.51 684.28 98.20 o 16 4 0 174.31 172.79 70.93 o -15 5 0 5.93 -71.28 71.28 o -14 5 0 17.27 35.88 60.14 o -13 5 0 7.33 59.65 63.14 o -12 5 0 70.22 100.92 34.99 o -11 5 0 1579.03 1630.21 64.55 o -10 5 0 186.17 156.32 27.86 o -9 5 0 300.88 312.83 23.57 o -8 5 0 1143.49 1214.58 50.85 o -7 5 0 939.83 1049.67 45.97 o -6 5 0 99.35 46.59 18.45 o -5 5 0 13411.94 13732.99 139.15 o -4 5 0 4786.60 5235.39 71.41 o -3 5 0 5169.32 5487.87 70.12 o -2 5 0 307.33 387.84 21.76 o -1 5 0 3338.87 2994.54 60.21 o 0 5 0 660.60 505.04 27.80 o 1 5 0 256.59 188.10 19.64 o 2 5 0 7105.07 6982.57 84.37 o 3 5 0 5332.94 5101.69 88.62 o 4 5 0 11228.34 11135.87 105.39 o 5 5 0 1496.84 1509.88 40.36 o 6 5 0 1408.11 1481.68 56.41 o 7 5 0 533.02 615.52 39.43 o 8 5 0 539.47 430.02 32.55 o 9 5 0 954.50 904.18 43.92 o 10 5 0 432.50 409.75 65.67 o 11 5 0 458.93 526.46 52.88 o 12 5 0 3.66 9.32 28.79 o 13 5 0 586.78 733.51 78.67 o 14 5 0 38.06 8.72 49.42 o 15 5 0 523.15 420.68 84.00 o -15 6 0 39.16 111.92 74.49 o -14 6 0 47.49 44.27 62.15 o -13 6 0 568.60 426.33 90.29 o -12 6 0 43.75 31.30 23.18 o -11 6 0 1350.76 1233.43 59.63 o -10 6 0 1289.42 1200.56 58.12 o -9 6 0 2.68 52.23 25.54 o -8 6 0 432.81 380.82 33.69 o -7 6 0 723.71 695.70 49.38 o -6 6 0 432.42 572.19 71.53 o -5 6 0 2863.42 2891.14 89.11 o -4 6 0 5593.69 5618.59 116.63 o -3 6 0 3502.13 3431.15 53.32 o -2 6 0 13.55 2.45 14.92 o -1 6 0 7148.47 7279.15 104.97 o 0 6 0 1261.52 1119.18 35.53 o 1 6 0 0.01 -7.13 15.16 o 2 6 0 3593.60 3572.92 65.69 o 3 6 0 21255.57 22905.27 206.35 o 4 6 0 462.23 487.29 26.84 o 5 6 0 30.98 53.09 13.91 o 6 6 0 2355.00 2341.64 54.36 o 7 6 0 1384.05 1425.96 69.57 o 8 6 0 38.24 30.26 13.78 o 9 6 0 1.85 20.10 16.95 o 10 6 0 98.70 165.34 48.53 o 11 6 0 117.54 125.40 44.13 o 12 6 0 0.25 -12.61 71.66 o 13 6 0 1427.51 1523.76 92.21 o 14 6 0 516.86 580.71 97.39 o 15 6 0 42.19 116.86 67.30 o -15 7 0 19.96 63.05 71.37 o -14 7 0 0.97 -74.50 74.50 o -13 7 0 573.28 448.54 90.20 o -12 7 0 940.46 716.84 50.48 o -11 7 0 32.38 -14.01 25.64 o -10 7 0 70.43 162.16 29.83 o -9 7 0 4313.28 4119.38 121.14 o -8 7 0 4720.50 4740.17 225.92 o -7 7 0 9719.88 9636.43 429.37 o -6 7 0 318.24 216.68 50.31 o -5 7 0 55.48 48.46 56.01 o -4 7 0 3427.12 3000.92 72.12 o -3 7 0 531.54 450.42 32.55 o -2 7 0 720.09 1074.66 56.89 o -1 7 0 903.09 946.69 43.00 o 0 7 0 2001.79 2197.48 73.55 o 1 7 0 72.86 37.47 16.23 o 2 7 0 186.44 240.10 23.65 o 3 7 0 5197.73 4607.47 101.99 o 4 7 0 130.24 126.91 25.69 o 5 7 0 324.01 302.86 41.72 o 6 7 0 22.19 8.40 20.40 o 7 7 0 1985.93 1795.77 51.61 o 8 7 0 953.51 1083.71 40.63 o 9 7 0 65.36 44.18 19.24 o 10 7 0 1466.44 1382.04 117.16 o 11 7 0 872.27 834.23 93.83 o 12 7 0 228.52 341.75 72.71 o 13 7 0 296.52 243.83 44.18 o 14 7 0 282.38 310.20 86.79 o 15 7 0 261.48 356.02 84.94 o -12 8 0 193.64 180.96 52.62 o -11 8 0 97.86 99.41 52.34 o -10 8 0 739.42 745.01 59.69 o -9 8 0 907.34 1065.14 49.06 o -8 8 0 839.67 970.54 48.15 o -7 8 0 7499.97 7358.03 121.01 o -6 8 0 30.06 36.77 27.78 o -5 8 0 0.14 -26.06 26.06 o -4 8 0 2885.61 3201.55 80.94 o -3 8 0 2640.69 2582.93 71.18 o -2 8 0 1929.62 2032.05 64.27 o -1 8 0 4422.59 4848.63 95.36 o 0 8 0 3994.03 4442.08 109.49 o 1 8 0 532.66 772.92 48.98 o 2 8 0 4513.95 4303.15 107.07 o 3 8 0 56.66 62.89 28.73 o 4 8 0 8690.49 8827.80 149.87 o 5 8 0 4016.93 4375.12 105.77 o 6 8 0 290.84 287.92 32.05 o 7 8 0 205.88 172.24 27.16 o 8 8 0 625.99 574.65 42.39 o 9 8 0 55.18 5.79 46.71 o 10 8 0 1136.44 1124.84 110.15 o 11 8 0 257.37 268.89 64.60 o 12 8 0 12.82 -30.36 49.63 o 13 8 0 123.68 116.14 42.36 o 14 8 0 0.71 -63.37 65.35 o -12 9 0 56.32 123.72 52.73 o -11 9 0 18.90 24.49 76.45 o -10 9 0 219.00 213.82 40.91 o -9 9 0 1194.80 955.04 88.07 o -8 9 0 2420.77 2212.44 72.64 o -7 9 0 577.02 649.95 43.94 o -6 9 0 1490.48 1599.37 74.86 o -5 9 0 88.89 156.43 35.23 o -4 9 0 139.93 141.59 28.28 o -3 9 0 4946.38 5008.35 105.23 o -2 9 0 1291.49 1463.93 58.99 o -1 9 0 179.45 179.84 27.57 o 0 9 0 236.34 216.98 35.13 o 1 9 0 2.98 8.95 30.03 o 2 9 0 566.23 652.02 50.45 o 3 9 0 770.88 951.65 56.75 o 4 9 0 80.08 108.88 30.49 o 5 9 0 3889.08 3656.85 104.61 o 6 9 0 104.61 135.73 29.20 o 7 9 0 550.36 442.17 39.17 o 8 9 0 1794.29 1680.61 91.55 o 9 9 0 1.63 42.88 40.50 o 10 9 0 334.97 185.33 56.81 o 11 9 0 278.04 230.99 61.24 o 12 9 0 162.11 248.20 69.85 o 13 9 0 6.91 -57.86 57.86 o 14 9 0 29.28 137.76 60.08 o -12 10 0 1.94 2.95 44.46 o -11 10 0 1.05 -19.18 29.76 o -10 10 0 680.51 645.31 61.86 o -9 10 0 96.01 59.59 33.94 o -8 10 0 160.41 252.24 39.77 o -7 10 0 70.41 93.38 25.46 o -6 10 0 1525.17 1601.89 90.98 o -5 10 0 7.87 29.27 25.03 o -4 10 0 27.82 8.99 25.82 o -3 10 0 1185.14 1182.42 58.13 o -2 10 0 229.00 167.67 30.68 o -1 10 0 33.58 48.67 30.95 o 0 10 0 833.92 809.98 92.97 o 1 10 0 622.06 499.95 46.92 o 2 10 0 141.50 110.21 42.03 o 3 10 0 1233.76 1185.16 67.97 o 4 10 0 2779.23 2933.38 99.89 o 5 10 0 19.83 -18.09 35.07 o 6 10 0 53.09 19.50 23.22 o 7 10 0 377.72 371.94 41.16 o 8 10 0 358.08 294.42 68.44 o 9 10 0 280.04 251.27 70.33 o 10 10 0 151.97 181.66 61.55 o 11 10 0 59.05 107.00 58.82 o 12 10 0 137.23 245.80 73.89 o 13 10 0 6.68 -23.65 47.33 o 14 10 0 54.38 89.96 63.45 o -12 11 0 206.94 378.98 80.48 o -11 11 0 16.02 -57.45 57.45 o -10 11 0 397.75 331.68 74.73 o -9 11 0 186.56 189.00 42.98 o -8 11 0 6.98 31.59 34.73 o -7 11 0 327.59 442.14 40.42 o -6 11 0 47.15 47.80 31.64 o -5 11 0 61.37 5.03 25.45 o -4 11 0 626.28 533.96 45.48 o -3 11 0 16.50 48.51 28.09 o -2 11 0 32.63 14.70 26.77 o -1 11 0 14.86 66.08 34.60 o 0 11 0 2.59 11.32 31.88 o 1 11 0 888.68 948.33 66.28 o 2 11 0 152.76 160.26 38.08 o 3 11 0 818.31 623.36 54.71 o 4 11 0 409.04 485.75 95.87 o 5 11 0 0.99 16.66 26.08 o 6 11 0 125.70 74.86 27.24 o 7 11 0 40.29 60.98 26.76 o 8 11 0 309.57 396.26 80.98 o 9 11 0 4.74 54.83 54.04 o 10 11 0 317.90 372.91 82.47 o 11 11 0 57.68 95.00 48.98 o 12 11 0 2.10 9.25 50.80 o 13 11 0 8.13 33.35 53.14 o 14 11 0 17.00 30.20 53.00 o -12 12 0 30.95 45.56 52.49 o -11 12 0 11.44 -56.01 56.01 o -10 12 0 7.46 -16.80 34.96 o -9 12 0 159.57 157.48 57.55 o -8 12 0 135.15 127.00 39.42 o -7 12 0 294.91 226.68 49.75 o -6 12 0 344.06 396.17 80.86 o -5 12 0 79.35 100.40 28.47 o -4 12 0 0.90 -26.54 26.54 o -3 12 0 426.63 408.67 42.88 o -2 12 0 52.34 62.59 33.08 o -1 12 0 5.75 -26.32 31.86 o 0 12 0 136.47 141.76 38.07 o 1 12 0 176.10 171.59 39.54 o 2 12 0 1098.57 1068.05 72.66 o 3 12 0 1144.46 1291.43 77.28 o 4 12 0 1931.02 1660.55 86.51 o 5 12 0 81.69 136.44 36.64 o 6 12 0 117.04 152.92 41.69 o 7 12 0 5.37 54.26 54.23 o 8 12 0 77.12 42.48 48.16 o 9 12 0 83.91 173.16 62.93 o 10 12 0 61.86 21.83 57.51 o 11 12 0 27.83 -7.97 51.71 o 12 12 0 7.54 -56.32 56.32 o 13 12 0 3.03 -38.57 59.38 o -12 13 0 154.88 107.58 57.29 o -11 13 0 4.51 178.43 67.69 o -10 13 0 13.31 80.25 61.58 o -9 13 0 60.33 -4.65 36.31 o -8 13 0 322.45 465.50 60.54 o -7 13 0 108.67 9.09 122.02 o -6 13 0 154.49 122.63 40.08 o -5 13 0 71.86 56.86 40.28 o -4 13 0 386.15 391.71 44.20 o -3 13 0 23.11 -10.95 34.75 o -2 13 0 599.36 505.87 61.17 o -1 13 0 593.87 603.97 80.86 o 0 13 0 741.09 790.32 117.58 o 1 13 0 1515.73 1536.91 89.91 o 2 13 0 407.29 305.92 46.98 o 3 13 0 29.95 -14.43 31.17 o 4 13 0 0.18 1.09 28.02 o 5 13 0 55.53 72.01 32.52 o 6 13 0 945.90 988.96 69.75 o 7 13 0 17.27 60.80 56.33 o 8 13 0 86.15 114.77 59.64 o 9 13 0 380.25 450.19 82.86 o 10 13 0 61.86 44.84 54.02 o 11 13 0 1.14 -48.79 64.67 o -10 14 0 3.70 -56.90 56.90 o -9 14 0 241.63 245.81 52.00 o -8 14 0 9.01 28.44 36.55 o -7 14 0 377.00 448.44 65.67 o -6 14 0 113.11 133.93 87.29 o -5 14 0 0.86 -0.74 29.71 o -4 14 0 684.14 694.64 77.13 o -3 14 0 48.88 4.82 32.28 o -2 14 0 154.95 113.87 41.99 o -1 14 0 456.18 416.87 57.08 o 0 14 0 1091.26 1139.35 82.63 o 1 14 0 1.36 43.49 33.70 o 2 14 0 11.58 -30.51 33.50 o 3 14 0 394.90 486.61 56.07 o 4 14 0 628.26 717.51 66.15 o 5 14 0 237.57 243.53 107.94 o 6 14 0 93.11 66.13 63.67 o 7 14 0 246.31 263.20 74.94 o 8 14 0 328.95 361.26 83.20 o 9 14 0 26.41 41.61 57.15 o 10 14 0 50.93 202.74 81.48 o -8 15 0 25.75 24.03 41.62 o -7 15 0 69.96 107.08 46.38 o -6 15 0 317.98 413.62 90.08 o -5 15 0 197.88 283.65 69.46 o -4 15 0 272.95 214.34 52.16 o -3 15 0 591.07 593.30 66.08 o -2 15 0 630.49 623.44 67.04 o -1 15 0 829.52 855.49 123.93 o 0 15 0 100.05 73.64 35.77 o 1 15 0 97.62 109.24 40.58 o 2 15 0 92.66 34.99 32.49 o 3 15 0 260.05 290.09 50.97 o 4 15 0 0.92 -31.66 31.66 o 5 15 0 593.97 661.86 79.71 o 6 15 0 49.36 -50.14 63.65 o 7 15 0 90.68 203.42 79.29 o 8 15 0 185.77 24.71 52.58 o -8 16 0 113.82 45.59 64.16 o -5 16 0 628.08 625.04 93.67 o -4 16 0 14.44 -28.07 46.57 o -3 16 0 481.32 554.31 73.25 o -2 16 0 317.61 364.22 56.27 o -1 16 0 273.26 308.62 51.31 o 0 16 0 1.70 11.66 35.56 o 1 16 0 73.91 94.11 36.75 o 2 16 0 7.64 -34.70 34.70 o 3 16 0 58.07 93.36 39.57 o 4 16 0 0.66 28.86 39.19 o 5 16 0 138.37 218.00 76.74 o 6 16 0 34.65 97.94 68.63 o -4 17 0 614.62 533.67 92.57 o -3 17 0 248.74 179.23 64.95 o -2 17 0 2.17 -1.93 38.85 o -1 17 0 2.02 -44.29 44.29 o 0 17 0 5.32 -24.22 38.47 o 1 17 0 11.80 11.59 57.20 o 2 17 0 5.05 -42.02 42.02 o 3 17 0 0.38 -57.74 82.47 o -3 18 0 175.28 225.68 69.54 o -2 18 0 3.71 48.35 52.90 o -1 18 0 249.34 278.27 80.18 o 0 18 0 154.62 106.75 64.56 o 1 18 0 3.79 -54.21 59.57 o 2 18 0 21.92 36.09 53.29 o -2 -18 1 35.41 130.34 64.62 o -1 -18 1 104.78 116.55 60.55 o 0 -18 1 42.05 -63.36 63.36 o 2 -18 1 63.70 25.56 58.12 o 3 -18 1 0.84 -39.49 64.24 o 4 -18 1 19.61 -63.61 63.61 o -3 -17 1 0.06 29.47 46.16 o -2 -17 1 298.63 432.81 62.40 o -1 -17 1 480.99 680.08 74.60 o 0 -17 1 0.38 23.62 52.97 o 1 -17 1 65.13 59.96 38.70 o 2 -17 1 2.60 -40.47 40.47 o 3 -17 1 95.23 99.81 55.07 o 4 -17 1 1.07 -69.38 69.38 o -5 -16 1 34.85 253.12 83.20 o -4 -16 1 84.26 35.03 35.66 o -3 -16 1 4.53 -25.17 36.47 o -2 -16 1 23.15 68.67 98.95 o -1 -16 1 213.16 303.68 95.72 o 0 -16 1 39.17 88.26 55.06 o 1 -16 1 202.82 138.50 49.16 o 2 -16 1 393.89 562.85 67.41 o 3 -16 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60.28 o 1 0 28 550.70 512.22 102.81 o 2 0 28 272.21 270.47 77.29 o 3 0 28 4.38 47.04 48.03 o 4 0 28 28.63 43.27 34.72 o 5 0 28 41.38 40.75 77.32 o 6 0 28 6.57 6.53 36.47 o 7 0 28 10.70 -12.44 36.69 o 8 0 28 48.45 8.84 50.19 o 9 0 28 271.51 213.63 77.09 o -1 1 28 500.31 643.67 109.76 o 0 1 28 88.37 150.32 68.03 o 1 1 28 12.68 63.56 57.41 o 2 1 28 182.20 82.03 49.85 o 3 1 28 32.36 11.22 47.50 o 4 1 28 19.61 47.36 50.37 o 5 1 28 102.33 126.96 56.15 o 6 1 28 78.06 130.91 45.58 o 7 1 28 65.55 57.54 82.40 o 8 1 28 36.73 -57.89 57.89 o 9 1 28 240.91 174.67 71.08 o -2 2 28 176.77 209.06 71.09 o -1 2 28 0.82 140.15 78.36 o 0 2 28 157.48 71.63 49.76 o 1 2 28 264.68 468.76 88.45 o 2 2 28 75.67 53.41 55.29 o 3 2 28 69.61 14.21 55.21 o 4 2 28 38.31 32.25 33.93 o 5 2 28 6.61 70.37 60.93 o 6 2 28 6.51 25.26 33.14 o 7 2 28 28.62 -2.50 32.07 o 8 2 28 9.92 101.18 63.37 o 9 2 28 89.45 152.18 62.70 o -2 3 28 604.10 757.35 116.62 o -1 3 28 223.10 139.19 59.93 o 0 3 28 35.28 -30.70 61.01 o 1 3 28 384.00 590.70 103.61 o 2 3 28 133.56 70.75 54.57 o 3 3 28 20.74 42.03 47.44 o 4 3 28 694.88 698.71 100.04 o 5 3 28 20.84 34.06 33.84 o 6 3 28 131.11 86.36 36.26 o 7 3 28 12.75 18.82 52.44 o 8 3 28 95.01 173.08 62.08 o 9 3 28 69.06 -12.86 50.80 o -1 4 28 88.32 105.17 61.63 o 0 4 28 19.26 43.74 51.91 o 1 4 28 2.14 21.98 48.48 o 2 4 28 144.36 171.34 69.02 o 3 4 28 396.04 427.81 86.35 o 4 4 28 144.20 129.61 55.69 o 5 4 28 162.85 181.11 41.73 o 6 4 28 14.36 13.82 37.22 o 7 4 28 12.54 -1.90 34.28 o 8 4 28 41.42 17.50 50.80 o 9 4 28 49.95 148.24 67.11 o -1 5 28 264.55 308.90 76.96 o 0 5 28 171.63 193.55 70.75 o 1 5 28 14.71 -15.43 50.76 o 2 5 28 23.35 39.98 44.54 o 3 5 28 286.02 222.28 68.14 o 4 5 28 7.56 33.65 48.45 o 5 5 28 202.73 247.83 47.24 o 6 5 28 206.02 270.99 70.97 o 7 5 28 149.58 180.38 59.40 o 8 5 28 158.71 223.77 68.13 o 9 5 28 0.29 142.49 71.47 o -1 6 28 54.55 143.80 70.59 o 0 6 28 26.15 59.85 59.59 o 1 6 28 228.92 165.58 66.81 o 2 6 28 5.77 -57.68 60.19 o 3 6 28 235.98 228.90 64.85 o 4 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77.46 90.42 53.90 o 5 10 28 209.47 227.01 70.40 o 8 10 28 28.42 16.89 46.43 o 3 11 28 88.27 183.23 72.24 o 4 11 28 14.33 81.01 62.52 o 5 11 28 102.05 20.60 54.07 o 4 -5 29 16.04 12.16 62.05 o 4 -4 29 1.09 -71.80 71.80 o 5 -4 29 180.98 217.52 78.85 o 6 -4 29 420.62 317.20 89.12 o 4 -3 29 74.65 106.79 45.12 o 5 -3 29 13.43 -41.37 41.79 o 6 -3 29 102.28 44.97 43.64 o 7 -3 29 123.99 121.14 67.33 o 8 -3 29 37.42 -13.41 55.48 o 3 -2 29 4.86 -47.74 53.96 o 4 -2 29 33.64 26.98 75.96 o 5 -2 29 84.01 142.61 43.89 o 6 -2 29 44.63 -35.22 37.06 o 7 -2 29 46.97 137.44 37.02 o 8 -2 29 478.92 448.25 87.24 o 2 -1 29 96.64 139.54 67.08 o 3 -1 29 29.87 14.14 55.07 o 4 -1 29 0.03 54.37 50.47 o 5 -1 29 31.19 66.09 44.64 o 6 -1 29 43.15 41.95 85.44 o 7 -1 29 38.66 79.72 34.68 o 8 -1 29 118.96 140.12 48.05 o 1 0 29 5.81 -38.93 47.54 o 2 0 29 13.28 30.23 52.32 o 3 0 29 9.38 24.41 51.14 o 4 0 29 11.34 38.02 54.16 o 5 0 29 45.73 -16.39 35.99 o 6 0 29 49.08 58.62 38.83 o 7 0 29 230.62 279.57 52.64 o 8 0 29 1.71 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37.62 12.55 53.07 o 4 9 29 119.31 87.84 63.89 o 5 9 29 186.57 216.43 69.97 o 8 9 29 1.27 73.57 53.73 o 4 10 29 3.52 -14.97 49.36 o 5 10 29 0.70 -58.94 58.94 o 5 -4 30 17.30 36.01 64.21 o 5 -3 30 60.34 52.60 64.55 o 6 -3 30 29.60 -70.82 70.82 o 5 -2 30 0.34 23.68 39.95 o 6 -2 30 0.41 102.36 74.64 o 7 -2 30 5.76 -40.23 40.23 o 4 -1 30 23.11 10.28 51.78 o 5 -1 30 136.06 139.35 65.29 o 6 -1 30 19.39 -12.95 40.62 o 7 -1 30 3.64 -32.37 32.37 o 3 0 30 53.97 227.33 81.84 o 4 0 30 62.12 -15.17 52.20 o 5 0 30 0.44 11.67 50.32 o 6 0 30 4.91 20.04 38.69 o 7 0 30 10.26 -24.48 33.48 o 2 1 30 9.62 43.45 52.22 o 3 1 30 1.50 -43.94 58.53 o 4 1 30 30.01 -57.53 57.53 o 5 1 30 27.50 -47.71 47.71 o 6 1 30 5.44 -10.07 78.58 o 7 1 30 7.59 -23.58 40.81 o 8 1 30 19.41 -31.26 59.61 o 2 2 30 96.44 67.66 55.09 o 3 2 30 167.93 169.84 65.00 o 4 2 30 109.53 80.91 50.20 o 5 2 30 6.92 31.50 46.43 o 6 2 30 0.87 12.58 111.39 o 7 2 30 6.81 69.73 56.48 o 8 2 30 80.92 88.11 64.08 o 2 3 30 44.60 38.21 63.92 o 3 3 30 41.76 38.81 54.60 o 4 3 30 49.86 -66.44 66.44 o 5 3 30 10.69 -63.56 63.56 o 6 3 30 0.17 2.11 48.75 o 7 3 30 39.64 50.13 49.50 o 8 3 30 58.27 116.63 55.40 o 2 4 30 176.43 184.51 67.34 o 3 4 30 0.55 10.92 54.45 o 4 4 30 134.49 192.87 74.45 o 5 4 30 98.23 -7.39 56.07 o 6 4 30 11.08 -5.40 46.50 o 7 4 30 5.10 -23.49 48.50 o 8 4 30 3.32 -56.61 56.61 o 2 5 30 30.16 50.28 48.28 o 3 5 30 105.56 260.52 71.19 o 4 5 30 5.02 19.34 45.50 o 5 5 30 111.47 3.87 53.10 o 6 5 30 231.72 108.95 44.85 o 7 5 30 37.61 -19.62 47.99 o 8 5 30 50.00 29.37 48.07 o 2 6 30 25.92 20.16 48.58 o 3 6 30 128.81 257.62 80.74 o 4 6 30 415.82 195.43 61.75 o 5 6 30 110.02 92.29 54.07 o 6 6 30 113.41 93.95 50.63 o 8 6 30 30.08 228.35 72.19 o 3 7 30 0.05 -46.68 65.70 o 4 7 30 7.90 44.65 48.83 o 5 7 30 155.41 105.40 58.08 o 8 7 30 1.28 -62.63 62.63 o 4 8 30 320.54 434.97 91.82 o 5 8 30 31.29 136.39 72.50 o 4 9 30 105.97 75.85 53.97 o 5 9 30 0.10 66.14 52.23 o 6 0 31 20.77 65.46 51.07 o 7 0 31 156.71 178.58 50.49 o 5 1 31 1.88 168.66 70.89 o 6 1 31 29.72 137.33 68.77 o 7 1 31 452.83 384.88 81.83 o 4 2 31 1.65 -76.47 76.47 o 5 2 31 13.34 16.16 51.02 o 6 2 31 7.80 10.71 54.70 o 7 2 31 16.36 150.16 66.14 o 4 3 31 4.70 125.56 67.89 o 5 3 31 0.76 32.16 52.32 o 6 3 31 268.54 476.49 94.68 o 8 3 31 105.89 89.03 59.41 o 4 4 31 185.66 36.56 59.67 o 5 4 31 218.16 314.87 76.66 o 6 4 31 40.19 54.67 47.73 o 8 4 31 167.29 144.27 63.28 o 4 5 31 188.34 116.81 62.25 o 5 5 31 425.10 503.35 95.59 o 6 5 31 91.66 121.65 65.53 o 4 6 31 0.03 -44.45 58.06 o 5 6 31 16.78 0.64 49.78 o 5 7 31 0.87 -65.61 65.61 o 5 8 31 0.52 77.85 57.68 o 6 3 32 73.27 7.97 51.77 o