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Information card for entry 2020109
Preview
| Coordinates | 2020109.cif |
|---|---|
| Structure factors | 2020109.hkl |
| Original IUCr paper | HTML |
| Chemical name | Ammonium hexachloridoantimonate(V)‒1,4,7,10,13,16-hexaoxacyclooctadecane (1/1) |
|---|---|
| Formula | C12 H28 Cl6 N O6 Sb |
| Calculated formula | C12 H28 Cl6 N O6 Sb |
| Title of publication | Unusual centrosymmetric structure of [<i>M</i>(18-crown-6)]^+^ (<i>M</i> = Rb, Cs and NH~4~) complexes stabilized in an environment of hexachloridoantimonate(V) anions |
| Authors of publication | Ponomarova, Vira V.; Rusanova, Julia A.; Rusanov, Eduard B.; Domasevitch, Konstantin V. |
| Journal of publication | Acta Crystallographica Section C |
| Year of publication | 2015 |
| Journal volume | 71 |
| Journal issue | 10 |
| a | 14.1069 ± 0.0009 Å |
| b | 14.1069 ± 0.0009 Å |
| c | 10.1908 ± 0.0008 Å |
| α | 90° |
| β | 90° |
| γ | 120° |
| Cell volume | 1756.3 ± 0.2 Å3 |
| Cell temperature | 223 ± 2 K |
| Ambient diffraction temperature | 223 ± 2 K |
| Number of distinct elements | 6 |
| Space group number | 148 |
| Hermann-Mauguin space group symbol | R -3 :H |
| Hall space group symbol | -R 3 |
| Residual factor for all reflections | 0.0236 |
| Residual factor for significantly intense reflections | 0.0217 |
| Weighted residual factors for significantly intense reflections | 0.0547 |
| Weighted residual factors for all reflections included in the refinement | 0.0556 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.135 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | No |
| Has Fobs | Yes |
| Revision | Date | Message | Files |
|---|---|---|---|
| 181871 (current) | 2016-04-06 | hkl/2/02/ (antanas@echidna) Adding IUCr specific svn headers to multiple entries in subrange 2/02/01 |
2020109.cif 2020109.hkl |
| 176428 | 2016-02-13 | Replaced deprecated COD CIF data names with their more modern alternatives. The _cod_cif_authors_sg_Hall and _cod_cif_authors_sg_H-M data items were renamed to _cod_original_sg_symbol_Hall and _cod_cif_authors_sg_H-M respectively. |
2020109.cif 2020109.hkl |
| 158192 | 2015-09-21 | cif/ hkl/ Adding structures of 2020107, 2020108, 2020109 via cif-deposit CGI script. |
2020109.cif 2020109.hkl |
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Users of the data should acknowledge the original authors of the
structural data.