#------------------------------------------------------------------------------ #$Date: 2016-04-06 16:41:11 +0300 (Wed, 06 Apr 2016) $ #$Revision: 181871 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/02/01/2020115.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_2020115 _cell_angle_alpha 90.000 _cell_angle_beta 94.005 _cell_angle_gamma 90.000 _cell_length_a 14.4601 _cell_length_b 21.1163 _cell_length_c 19.6068 _exptl_crystal_F_000 2888.00 _reflns_d_resolution_high 0.7495 _cod_data_source_file yo3013Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' [Zn3(MPP)4](PF6)2(CH3OH) at -100C in P2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 467.89 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 13181.39 13429.47 329.85 o 3 0 0 6235.93 7506.38 206.00 o 4 0 0 42872.28 42685.53 1174.44 o 5 0 0 17576.20 16413.74 496.40 o 6 0 0 12062.07 9306.56 321.57 o 7 0 0 6630.78 6192.86 254.91 o 8 0 0 197.47 21.83 93.37 o 9 0 0 165.97 376.61 211.14 o 10 0 0 5934.70 6220.04 288.53 o 11 0 0 11906.28 13127.49 1114.13 o 12 0 0 20.84 -127.17 205.30 o 13 0 0 12.26 -144.55 297.37 o 14 0 0 3087.45 3454.01 517.39 o 15 0 0 218.93 391.51 398.98 o 16 0 0 66.86 -149.35 367.24 o 17 0 0 261.41 36.54 412.58 o 18 0 0 14.60 -405.38 405.38 o 19 0 0 240.42 259.76 500.86 o 1 1 0 7046.83 7228.31 162.40 o 2 1 0 16739.08 14264.56 313.89 o 3 1 0 11844.54 10542.61 193.53 o 4 1 0 3359.53 2913.81 88.40 o 5 1 0 11924.41 11831.52 267.05 o 6 1 0 59.52 -58.70 58.70 o 7 1 0 2956.44 2731.04 114.45 o 8 1 0 15.55 -36.14 62.80 o 9 1 0 20948.00 20282.39 456.03 o 10 1 0 9916.99 9291.17 265.06 o 11 1 0 96.45 333.65 128.23 o 12 1 0 1218.91 1329.03 213.33 o 13 1 0 219.25 129.57 220.17 o 14 1 0 4340.88 4417.24 403.84 o 15 1 0 3895.38 3926.38 409.72 o 16 1 0 98.75 -99.88 257.13 o 17 1 0 87.23 -267.12 267.12 o 18 1 0 180.88 55.43 298.79 o 19 1 0 985.58 1176.29 495.53 o 0 2 0 126272.66 156708.28 11591.04 o 1 2 0 28292.97 31574.43 566.49 o 2 2 0 31806.23 31759.58 614.80 o 3 2 0 52.15 -30.63 47.32 o 4 2 0 3002.10 2610.92 107.81 o 5 2 0 776.29 421.22 72.77 o 6 2 0 4626.78 4393.61 159.80 o 7 2 0 6372.13 6138.55 205.98 o 8 2 0 80.65 73.07 64.47 o 9 2 0 3958.43 3888.50 248.59 o 10 2 0 10073.52 11080.41 410.33 o 11 2 0 3812.32 3739.17 233.81 o 12 2 0 1623.31 1896.81 231.62 o 13 2 0 25.59 77.12 183.00 o 14 2 0 341.67 -172.24 840.37 o 15 2 0 103.97 31.31 298.44 o 16 2 0 229.97 441.64 280.12 o 17 2 0 464.11 301.29 324.97 o 18 2 0 46.50 -24.36 317.83 o 19 2 0 313.42 175.64 660.74 o 1 3 0 21147.06 24492.10 439.42 o 2 3 0 23810.31 26485.45 563.97 o 3 3 0 57301.31 55167.75 1158.69 o 4 3 0 288.52 224.55 58.98 o 5 3 0 1055.26 1533.37 96.93 o 6 3 0 290.00 173.81 74.54 o 7 3 0 2550.54 2776.89 178.69 o 8 3 0 774.57 941.18 108.46 o 9 3 0 11409.37 11132.92 330.80 o 10 3 0 14501.90 15485.14 427.54 o 11 3 0 32.59 155.85 188.40 o 12 3 0 620.47 772.03 156.66 o 13 3 0 0.00 -156.91 169.36 o 14 3 0 603.08 464.89 257.79 o 15 3 0 2331.71 2038.06 623.94 o 16 3 0 7.82 101.56 267.26 o 17 3 0 13.34 -270.80 270.80 o 18 3 0 35.82 30.20 314.30 o 19 3 0 675.65 974.52 365.00 o 0 4 0 12380.58 20552.33 2298.41 o 1 4 0 8809.38 10569.79 216.46 o 2 4 0 54723.87 55927.62 1076.33 o 3 4 0 19299.62 19329.19 433.88 o 4 4 0 30488.57 29773.36 655.88 o 5 4 0 16584.87 15819.44 349.39 o 6 4 0 10040.97 10156.41 278.73 o 7 4 0 1494.82 1570.32 163.49 o 8 4 0 2461.42 2656.45 147.22 o 9 4 0 2438.30 2655.55 161.76 o 10 4 0 2946.25 2931.58 336.13 o 11 4 0 187.02 56.73 208.83 o 12 4 0 2076.43 1956.64 274.08 o 13 4 0 302.86 225.97 209.22 o 14 4 0 1974.38 2392.20 285.79 o 15 4 0 280.96 118.02 463.39 o 16 4 0 45.53 58.79 266.50 o 17 4 0 251.16 358.85 382.85 o 18 4 0 19.36 -266.68 303.90 o 1 5 0 14330.56 14126.60 288.86 o 2 5 0 1184.34 937.22 49.54 o 3 5 0 2355.36 2489.81 75.76 o 4 5 0 4892.26 4716.63 143.49 o 5 5 0 98.47 42.26 69.45 o 6 5 0 4422.90 4557.74 221.43 o 7 5 0 4022.22 4448.43 213.46 o 8 5 0 454.49 317.64 98.81 o 9 5 0 1256.42 1050.86 130.06 o 10 5 0 1978.32 1931.45 243.71 o 11 5 0 349.91 257.83 142.74 o 12 5 0 3.69 -16.26 137.08 o 13 5 0 455.46 623.87 292.60 o 14 5 0 69.10 300.46 205.86 o 15 5 0 238.58 833.33 286.43 o 16 5 0 176.10 -167.03 349.24 o 17 5 0 95.82 198.63 310.17 o 18 5 0 6.94 -243.47 287.55 o 0 6 0 152.76 234.29 50.92 o 1 6 0 141.75 163.86 86.67 o 2 6 0 3802.23 4272.81 108.93 o 3 6 0 3804.87 4033.25 120.11 o 4 6 0 6040.31 5508.40 130.77 o 6 6 0 43.91 233.21 77.78 o 7 6 0 6.42 -77.99 77.99 o 8 6 0 4.93 29.93 141.73 o 9 6 0 540.40 686.50 134.09 o 10 6 0 143.71 21.49 133.52 o 11 6 0 1.82 -34.59 167.76 o 12 6 0 1114.33 1355.26 242.59 o 13 6 0 67.27 108.47 153.63 o 14 6 0 93.84 -105.95 202.54 o 15 6 0 20.22 35.85 218.42 o 16 6 0 64.59 -336.15 395.51 o 17 6 0 10.08 -89.83 277.35 o 18 6 0 12.60 274.33 316.16 o 1 7 0 7777.16 7196.61 170.85 o 2 7 0 582.11 563.09 62.21 o 3 7 0 6845.30 6114.63 158.08 o 4 7 0 5090.91 4445.59 120.14 o 5 7 0 5780.26 5611.24 156.15 o 6 7 0 1802.67 1503.43 103.20 o 7 7 0 52.17 72.83 72.67 o 8 7 0 248.55 126.85 111.84 o 9 7 0 1508.87 1568.49 160.07 o 10 7 0 194.51 252.89 134.91 o 11 7 0 930.29 1163.76 168.38 o 12 7 0 206.19 403.40 157.63 o 13 7 0 59.84 204.19 158.41 o 14 7 0 811.58 1194.69 241.45 o 15 7 0 761.39 609.63 379.76 o 16 7 0 138.87 22.90 229.73 o 17 7 0 8.09 417.13 300.27 o 18 7 0 6.53 -100.80 293.15 o 0 8 0 16978.66 16856.73 695.95 o 1 8 0 10494.05 11138.51 330.75 o 2 8 0 3099.65 2807.99 82.29 o 3 8 0 765.13 929.18 65.00 o 4 8 0 98.13 19.23 64.92 o 5 8 0 12930.14 12138.97 245.05 o 6 8 0 843.62 987.87 84.48 o 7 8 0 249.88 11.99 71.76 o 8 8 0 13.22 -38.25 143.52 o 9 8 0 21.79 -116.60 116.60 o 10 8 0 901.86 889.62 166.82 o 11 8 0 269.35 -54.75 206.64 o 12 8 0 149.66 352.35 159.95 o 13 8 0 257.21 43.76 157.76 o 14 8 0 6.42 188.16 184.38 o 15 8 0 29.79 124.35 222.30 o 16 8 0 133.25 138.47 230.57 o 17 8 0 55.43 86.75 297.57 o 18 8 0 3.28 -296.85 307.04 o 1 9 0 3137.44 3569.66 140.77 o 2 9 0 1.03 73.28 47.76 o 3 9 0 5.06 32.48 42.74 o 4 9 0 14963.00 13217.94 287.65 o 5 9 0 5828.91 6104.40 165.68 o 6 9 0 183.76 264.34 71.32 o 7 9 0 188.49 90.85 76.00 o 8 9 0 1063.02 1450.80 121.01 o 9 9 0 4819.73 5591.61 314.19 o 10 9 0 4748.66 5024.92 258.90 o 11 9 0 15.23 -34.65 162.49 o 12 9 0 25.45 -52.42 173.11 o 13 9 0 2.37 6.14 159.21 o 14 9 0 2429.84 3026.03 257.84 o 15 9 0 1787.36 1937.22 288.14 o 16 9 0 123.62 141.33 239.59 o 17 9 0 0.97 -240.55 240.55 o 18 9 0 30.32 -221.33 303.40 o 0 10 0 26618.35 26289.37 751.37 o 1 10 0 176.72 11.14 68.15 o 2 10 0 12088.11 12272.45 351.02 o 3 10 0 1367.62 1726.57 106.92 o 4 10 0 16338.19 17267.32 347.88 o 5 10 0 29970.24 28715.02 551.13 o 6 10 0 8934.44 7959.60 225.38 o 7 10 0 3517.73 3429.46 151.63 o 8 10 0 2.47 -92.99 92.99 o 9 10 0 118.62 98.28 131.27 o 10 10 0 628.63 385.53 150.06 o 11 10 0 1056.60 1516.89 266.93 o 12 10 0 159.45 99.47 153.15 o 13 10 0 16.38 -87.13 160.16 o 14 10 0 52.33 175.82 183.03 o 15 10 0 250.45 394.38 330.41 o 16 10 0 347.35 539.93 254.26 o 17 10 0 51.36 190.03 260.66 o 1 11 0 4916.76 5197.24 146.00 o 2 11 0 400.63 276.09 57.48 o 3 11 0 17.03 -45.40 45.40 o 4 11 0 3986.10 4332.04 155.39 o 5 11 0 2997.11 2383.88 98.29 o 6 11 0 204.17 222.02 76.03 o 7 11 0 437.46 342.86 115.71 o 8 11 0 491.62 379.78 131.22 o 9 11 0 14507.80 14351.16 878.08 o 10 11 0 6067.56 5758.65 282.46 o 11 11 0 2.12 26.36 199.02 o 12 11 0 1.49 -78.49 156.87 o 13 11 0 277.17 124.25 190.24 o 14 11 0 3253.43 3675.21 395.65 o 15 11 0 3220.78 3452.94 335.93 o 16 11 0 70.39 171.80 238.84 o 17 11 0 7.23 538.13 342.49 o 0 12 0 6355.66 5747.61 290.11 o 1 12 0 1921.94 1868.17 135.14 o 2 12 0 128.47 223.10 58.63 o 3 12 0 601.74 540.46 66.56 o 4 12 0 13677.40 13545.05 273.68 o 5 12 0 35065.57 33301.49 684.14 o 6 12 0 3950.03 3715.54 145.30 o 7 12 0 232.19 253.92 116.01 o 8 12 0 207.79 252.98 127.92 o 9 12 0 27.19 17.48 126.77 o 10 12 0 2445.82 2594.94 208.73 o 11 12 0 4.80 -103.17 142.23 o 12 12 0 812.02 752.22 184.59 o 13 12 0 1.49 -5.87 174.86 o 14 12 0 66.70 107.11 226.54 o 15 12 0 37.66 -37.97 241.86 o 16 12 0 30.05 155.54 326.86 o 17 12 0 75.75 -306.05 306.05 o 1 13 0 12580.77 12531.06 262.06 o 2 13 0 285.83 273.12 57.79 o 3 13 0 9550.91 7691.57 243.22 o 4 13 0 20131.36 18435.64 414.47 o 5 13 0 4399.04 4555.08 215.17 o 6 13 0 225.28 -20.51 86.80 o 7 13 0 818.62 451.81 125.75 o 8 13 0 1184.05 1211.66 154.55 o 9 13 0 2626.36 2102.17 188.48 o 10 13 0 11875.50 13256.47 539.70 o 11 13 0 1.71 -146.23 194.66 o 12 13 0 24.39 -50.51 193.18 o 13 13 0 1.37 -199.47 199.47 o 14 13 0 572.53 952.23 263.32 o 15 13 0 2026.85 2688.86 443.55 o 16 13 0 0.42 -306.11 306.11 o 17 13 0 40.77 315.50 479.52 o 0 14 0 17327.99 18609.47 565.96 o 1 14 0 1510.51 1674.78 121.51 o 2 14 0 172.45 78.94 52.42 o 3 14 0 44.21 121.39 63.94 o 4 14 0 6406.39 5971.00 215.94 o 5 14 0 6668.82 5775.14 206.72 o 6 14 0 191.45 231.33 141.51 o 7 14 0 491.96 364.84 204.05 o 8 14 0 20.59 -148.93 148.93 o 9 14 0 3914.95 4595.16 304.21 o 10 14 0 3351.92 3480.03 284.45 o 11 14 0 10.61 27.40 187.72 o 12 14 0 2190.79 2686.44 323.98 o 13 14 0 0.38 -136.40 211.12 o 14 14 0 874.91 769.90 315.99 o 15 14 0 119.76 87.02 256.43 o 16 14 0 0.47 -273.73 345.77 o 1 15 0 2481.48 2756.89 195.28 o 2 15 0 7168.20 7585.51 271.91 o 3 15 0 4352.39 4003.08 204.18 o 4 15 0 381.12 446.90 193.47 o 5 15 0 7267.39 6467.48 264.16 o 6 15 0 377.97 502.72 151.47 o 7 15 0 35.81 -94.23 136.69 o 8 15 0 1297.98 1105.44 196.40 o 9 15 0 1064.43 980.00 203.79 o 10 15 0 1886.76 2039.24 250.89 o 11 15 0 81.18 -110.94 190.39 o 12 15 0 15.48 -53.85 201.76 o 13 15 0 54.48 141.19 225.50 o 14 15 0 277.24 165.41 239.07 o 15 15 0 1353.39 1546.44 394.80 o 16 15 0 70.12 170.27 308.43 o 0 16 0 17616.25 17541.81 1067.33 o 1 16 0 1.15 178.64 88.70 o 2 16 0 2353.83 2308.51 302.61 o 3 16 0 67.86 140.14 126.81 o 4 16 0 556.06 595.33 174.18 o 5 16 0 27.10 245.14 173.77 o 6 16 0 75.97 -24.96 137.20 o 7 16 0 1593.12 1260.64 324.25 o 8 16 0 958.12 1277.28 305.58 o 9 16 0 135.26 -81.01 172.47 o 10 16 0 731.84 991.67 218.16 o 11 16 0 52.67 -15.62 195.43 o 12 16 0 887.99 759.55 290.55 o 13 16 0 583.67 649.17 253.18 o 14 16 0 122.55 120.51 244.26 o 15 16 0 15.08 -231.52 256.64 o 1 17 0 497.00 722.54 223.75 o 2 17 0 2127.84 2198.29 295.97 o 3 17 0 729.56 952.24 160.02 o 4 17 0 2306.58 1779.39 191.32 o 5 17 0 7.32 177.11 174.88 o 6 17 0 272.02 55.21 242.03 o 7 17 0 1481.55 1185.16 242.22 o 8 17 0 1081.46 862.85 247.68 o 9 17 0 271.51 349.91 228.27 o 10 17 0 352.71 -83.95 232.92 o 11 17 0 148.40 73.72 276.30 o 12 17 0 94.87 -15.62 267.05 o 13 17 0 14.60 -272.41 272.41 o 14 17 0 93.54 -114.90 335.64 o 15 17 0 94.33 -28.42 324.04 o 0 18 0 11312.48 10738.87 813.43 o 1 18 0 1694.85 1722.40 274.60 o 2 18 0 2888.95 3415.84 370.31 o 3 18 0 599.57 566.96 155.64 o 4 18 0 3.82 124.65 142.40 o 5 18 0 12.40 587.37 197.80 o 6 18 0 303.10 193.85 190.72 o 7 18 0 401.71 441.94 344.71 o 8 18 0 1.07 -200.14 200.14 o 9 18 0 4.15 -203.55 203.55 o 10 18 0 36.45 210.43 252.08 o 11 18 0 22.94 82.25 257.20 o 12 18 0 190.86 436.30 286.67 o 13 18 0 4.05 5.46 287.15 o 14 18 0 1.68 -133.18 306.44 o 1 19 0 1967.88 1702.16 687.15 o 2 19 0 2922.55 2659.62 781.43 o 3 19 0 39.38 -127.02 127.02 o 4 19 0 2644.32 2390.78 257.77 o 5 19 0 1264.02 1627.99 242.58 o 6 19 0 234.49 -134.97 201.89 o 7 19 0 1443.02 2008.26 284.53 o 8 19 0 1357.83 1137.63 370.44 o 9 19 0 2.13 169.99 238.43 o 10 19 0 182.06 288.63 248.63 o 11 19 0 91.90 -16.07 274.30 o 12 19 0 64.29 319.03 292.46 o 13 19 0 299.99 191.78 300.88 o 14 19 0 12.74 88.30 303.98 o 0 20 0 67.25 570.73 356.04 o 1 20 0 5331.45 6269.48 459.55 o 2 20 0 113.48 -90.89 352.31 o 3 20 0 8.19 -81.13 225.23 o 4 20 0 272.82 336.51 183.90 o 5 20 0 1642.13 1778.07 255.65 o 6 20 0 1527.80 1902.03 296.70 o 7 20 0 447.11 358.41 339.11 o 8 20 0 340.48 341.86 236.44 o 9 20 0 45.79 0.18 232.39 o 10 20 0 67.84 134.89 256.70 o 11 20 0 1271.55 1765.28 579.40 o 12 20 0 520.00 441.64 646.21 o 13 20 0 1.29 142.63 303.78 o 1 21 0 131.24 12.65 241.26 o 2 21 0 158.88 369.89 255.03 o 3 21 0 287.98 319.32 319.10 o 4 21 0 418.00 674.21 421.12 o 5 21 0 1172.11 1143.84 240.03 o 6 21 0 0.60 16.56 346.44 o 7 21 0 532.61 168.37 379.51 o 8 21 0 634.78 490.21 254.70 o 9 21 0 476.95 580.65 270.32 o 10 21 0 127.51 343.48 347.11 o 11 21 0 167.32 462.81 315.10 o 12 21 0 13.86 620.48 306.27 o 0 22 0 2206.98 3128.64 515.79 o 1 22 0 471.58 680.75 373.91 o 2 22 0 1026.30 618.78 275.50 o 3 22 0 321.95 649.94 404.05 o 4 22 0 566.23 721.15 433.65 o 5 22 0 2439.99 2457.00 269.78 o 6 22 0 1792.18 1646.24 266.00 o 7 22 0 304.77 579.79 235.86 o 8 22 0 120.56 121.96 234.22 o 9 22 0 86.81 924.33 279.15 o 10 22 0 380.57 692.66 286.87 o 11 22 0 31.63 115.09 271.98 o 1 23 0 111.52 -114.54 253.85 o 2 23 0 1.35 -255.06 255.06 o 3 23 0 8.02 378.98 398.98 o 4 23 0 1256.53 1000.39 454.45 o 5 23 0 228.45 -120.01 395.51 o 6 23 0 59.27 202.96 410.45 o 7 23 0 104.83 -84.04 211.99 o 8 23 0 11.67 -8.01 233.76 o 9 23 0 575.65 963.14 280.40 o 10 23 0 503.89 548.51 274.41 o 11 23 0 42.56 305.34 289.82 o 0 24 0 1732.36 1557.25 493.66 o 1 24 0 753.40 1263.06 343.65 o 2 24 0 19.75 -233.63 367.78 o 3 24 0 1.36 -34.94 412.58 o 4 24 0 566.81 722.22 462.19 o 5 24 0 1847.60 1572.72 529.13 o 6 24 0 6.02 -226.43 408.05 o 7 24 0 41.98 33.07 407.25 o 8 24 0 26.72 -32.03 306.44 o 9 24 0 22.78 53.47 240.52 o 10 24 0 437.41 642.64 590.74 o 1 25 0 67.06 -7.99 309.90 o 2 25 0 101.14 -132.82 425.92 o 3 25 0 23.77 602.74 446.99 o 4 25 0 198.86 -386.45 386.45 o 5 25 0 637.35 793.69 485.12 o 6 25 0 187.22 259.50 425.38 o 7 25 0 579.47 209.89 449.12 o 8 25 0 138.82 79.48 467.79 o 0 26 0 1143.04 2067.44 548.87 o 1 26 0 2.87 23.74 450.45 o 2 26 0 90.78 71.74 447.79 o 3 26 0 40.85 458.72 496.06 o 4 26 0 159.55 951.85 547.80 o 5 26 0 1254.18 2099.98 596.87 o 6 26 0 40.20 955.85 523.53 o 7 26 0 508.17 687.55 507.26 o 1 27 0 7.80 16.00 444.32 o 2 27 0 677.29 1489.24 580.34 o 3 27 0 1095.84 882.24 525.13 o 4 27 0 25.90 -150.68 471.79 o 5 27 0 29.40 38.14 478.72 o 1 28 0 2.81 631.81 547.00 o -19 1 1 0.55 20.41 344.27 o -18 1 1 15.16 -284.15 284.15 o -17 1 1 212.13 517.17 307.11 o -16 1 1 79.36 448.60 406.58 o -15 1 1 803.48 799.26 289.42 o -14 1 1 232.26 519.34 261.85 o -13 1 1 224.20 360.87 197.10 o -12 1 1 1043.54 1541.61 188.31 o -11 1 1 217.30 364.39 118.46 o -10 1 1 1550.87 1439.32 187.76 o -9 1 1 4059.57 4020.56 163.08 o -8 1 1 46.77 -47.57 68.42 o -7 1 1 1.24 -64.31 64.31 o -6 1 1 1723.55 2200.76 82.25 o -5 1 1 242.71 28.24 47.81 o -4 1 1 30104.46 26767.15 495.13 o -3 1 1 909.70 689.36 43.67 o -2 1 1 1740.22 1894.01 59.11 o -1 1 1 283.77 263.82 21.41 o 1 1 1 4855.31 5317.47 123.88 o 2 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