data_2020331 _cell_angle_alpha 112.087 _cell_angle_beta 94.380 _cell_angle_gamma 90.486 _cell_length_a 11.2516 _cell_length_b 15.0606 _cell_length_c 18.3213 _exptl_crystal_F_000 1630.00 _reflns_d_resolution_high 0.8001 _cod_data_source_file lg3178III_vCM14087twin5sup4.hkl _cod_data_source_block III_vCM14087twin5 _shelx_title ' twin CM14087 in P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 364.58 _shelx_f_squared_multiplier 1.000 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 248.54 397.55 41.87 o 3 0 0 9123.93 10109.67 222.98 o 4 0 0 51152.41 57194.42 1096.48 o 5 0 0 283.69 896.97 96.39 o 6 0 0 10113.76 10736.21 269.07 o 7 0 0 9616.92 9783.47 460.50 o 8 0 0 6587.15 6962.85 397.99 o 9 0 0 7064.33 7154.25 502.43 o 10 0 0 99.25 39.57 226.46 o 11 0 0 2691.85 2246.67 394.81 o 12 0 0 5661.35 5223.15 659.27 o 13 0 0 4026.44 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119.31 o -2 3 0 3949.17 4143.80 135.26 o -1 3 0 984.38 1522.73 71.92 o 0 3 0 30433.93 30456.27 674.31 o 1 3 0 1499.13 1686.07 73.04 o 2 3 0 3009.02 3448.50 100.59 o 3 3 0 18400.91 17744.17 364.44 o 4 3 0 5097.42 5463.36 244.99 o 5 3 0 4012.37 4417.05 190.09 o 6 3 0 1720.07 1785.46 156.57 o 7 3 0 1723.09 1897.03 176.94 o 8 3 0 9014.37 8613.30 459.81 o 9 3 0 1386.90 1599.54 330.42 o 10 3 0 3557.84 3508.34 461.60 o 11 3 0 160.81 297.42 250.36 o 12 3 0 553.37 -77.14 549.03 o 13 3 0 780.57 643.72 590.72 o -12 4 0 455.27 834.45 276.00 o -11 4 0 648.12 793.40 396.58 o -10 4 0 2404.02 2945.56 364.19 o -9 4 0 420.50 366.95 416.20 o -8 4 0 822.34 868.76 216.22 o -7 4 0 2214.01 2202.55 256.92 o -6 4 0 2352.70 2324.18 192.91 o -5 4 0 579.11 584.12 99.19 o -4 4 0 23177.84 24040.69 549.94 o -3 4 0 2242.34 2366.51 151.93 o -2 4 0 529.78 458.06 119.16 o -1 4 0 9881.36 9879.33 197.00 o 0 4 0 5708.46 6702.01 151.33 o 1 4 0 19829.16 18349.61 341.51 o 2 4 0 2361.74 2567.19 143.30 o 3 4 0 5144.71 5145.33 137.93 o 4 4 0 8330.20 8800.29 221.67 o 5 4 0 8911.61 8778.30 264.24 o 6 4 0 768.26 681.44 195.47 o 7 4 0 1212.92 1216.80 168.63 o 8 4 0 2707.43 3308.96 321.00 o 9 4 0 1552.87 1183.93 210.61 o 10 4 0 783.45 534.59 400.86 o 11 4 0 423.61 664.27 256.55 o 12 4 0 866.45 591.69 608.93 o 13 4 0 840.11 773.45 509.51 o -12 5 0 828.52 698.90 275.59 o -11 5 0 746.17 855.91 439.01 o -10 5 0 2962.56 2891.88 330.02 o -9 5 0 7949.51 8093.77 501.49 o -8 5 0 48.21 -102.81 166.09 o -7 5 0 1206.57 1175.08 266.35 o -6 5 0 5804.14 5746.54 223.88 o -5 5 0 17329.43 16532.08 614.98 o -4 5 0 4068.48 4645.83 183.30 o -3 5 0 1001.33 1067.66 159.29 o -2 5 0 13187.89 12973.10 283.63 o -1 5 0 28722.07 28690.83 482.74 o 0 5 0 1578.59 1574.09 87.48 o 1 5 0 63.14 91.91 102.68 o 2 5 0 1371.42 1545.42 111.12 o 3 5 0 242.45 367.75 75.38 o 4 5 0 11126.18 10726.04 258.56 o 5 5 0 1482.74 1481.85 174.08 o 6 5 0 1448.27 1309.58 196.75 o 7 5 0 1645.92 1758.52 182.61 o 8 5 0 11151.12 10873.23 565.15 o 9 5 0 2242.54 2612.11 344.38 o 10 5 0 1824.51 1077.41 371.68 o 11 5 0 2.11 180.94 353.25 o 12 5 0 1599.94 1900.27 739.66 o 13 5 0 394.84 1036.80 522.23 o -12 6 0 891.59 1744.25 709.76 o -11 6 0 1496.25 1195.83 466.90 o -10 6 0 191.29 331.24 329.72 o -9 6 0 2164.10 2549.62 372.37 o -8 6 0 192.90 274.45 178.56 o -7 6 0 1170.99 1251.93 299.03 o -6 6 0 1016.12 1310.68 185.08 o -5 6 0 1196.66 1079.83 191.06 o -4 6 0 17730.25 17640.00 382.17 o -3 6 0 2278.63 1878.08 269.41 o -2 6 0 3243.06 3087.41 133.58 o -1 6 0 10995.11 11343.65 235.53 o 0 6 0 337.85 311.62 72.01 o 1 6 0 16415.05 19476.05 389.31 o 2 6 0 5437.69 5491.27 157.96 o 3 6 0 5693.29 5701.83 267.16 o 4 6 0 2284.20 2336.87 129.85 o 5 6 0 424.29 249.21 193.12 o 6 6 0 10588.71 11121.29 334.67 o 7 6 0 6999.09 6978.48 459.30 o 8 6 0 3055.04 2908.83 293.10 o 9 6 0 2101.82 2053.04 366.18 o 10 6 0 9213.34 9012.33 504.60 o 11 6 0 1574.00 1195.07 693.01 o 12 6 0 394.28 254.23 394.84 o -12 7 0 2136.75 3458.63 701.43 o -11 7 0 955.38 1117.21 671.86 o -10 7 0 7439.97 7430.96 494.33 o -9 7 0 3663.40 3406.67 359.15 o -8 7 0 11129.54 9744.62 544.10 o -7 7 0 422.98 396.09 166.07 o -6 7 0 2028.22 2257.60 254.39 o -5 7 0 12463.52 12489.05 316.51 o -4 7 0 12243.68 11839.46 286.23 o -3 7 0 188.02 207.65 87.41 o -2 7 0 15872.36 16286.26 363.54 o -1 7 0 19114.77 18409.81 371.62 o 0 7 0 6520.13 5617.89 187.97 o 1 7 0 1244.29 1222.15 98.10 o 2 7 0 260.12 128.39 124.93 o 3 7 0 12061.40 11982.81 303.30 o 4 7 0 593.65 728.30 103.56 o 5 7 0 4646.07 4539.10 262.29 o 6 7 0 2454.73 2523.18 221.41 o 7 7 0 6948.48 6825.46 443.39 o 8 7 0 2453.72 2655.92 279.08 o 9 7 0 981.61 1034.36 385.31 o 10 7 0 361.79 469.26 351.11 o 11 7 0 196.08 1212.30 652.57 o 12 7 0 444.53 395.34 397.81 o -11 8 0 501.23 417.37 359.27 o -10 8 0 1166.35 1082.34 565.41 o -9 8 0 671.25 624.23 226.68 o -8 8 0 1585.82 1459.79 374.67 o -7 8 0 259.10 43.05 155.09 o -6 8 0 748.78 1239.30 227.78 o -5 8 0 4245.44 4265.49 187.73 o -4 8 0 3063.33 2931.71 266.38 o -3 8 0 20921.77 20185.26 435.90 o -2 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