data_2020435 _cell_angle_alpha 88.257 _cell_angle_beta 81.614 _cell_angle_gamma 80.184 _cell_length_a 10.0414 _cell_length_b 14.4893 _cell_length_c 15.6001 _exptl_crystal_F_000 1136.00 _reflns_d_resolution_high 0.8370 _cod_data_source_file fm3038IIsup3.hkl _cod_data_source_block II _shelx_title ' CF solution in P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 412.69 _shelx_f_squared_multiplier 1.000 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 413.84 419.27 14.46 o 2 0 0 910.84 1030.59 32.69 o 3 0 0 2975.37 2860.68 68.21 o 4 0 0 681.74 675.62 20.98 o 5 0 0 460.74 481.16 31.34 o 6 0 0 1589.41 1605.15 47.44 o 7 0 0 497.94 529.26 30.54 o 8 0 0 2993.65 3098.57 79.60 o 9 0 0 231.91 368.80 170.76 o 10 0 0 2553.98 2547.78 172.56 o 11 0 0 26.50 48.21 16.19 o -11 1 0 71.44 67.37 16.20 o -10 1 0 525.54 613.35 180.77 o -9 1 0 296.28 336.44 56.00 o -8 1 0 485.25 440.34 33.83 o -7 1 0 1.09 3.19 8.92 o -6 1 0 145.13 90.67 18.73 o -5 1 0 18.85 24.35 5.95 o -4 1 0 12485.07 12859.29 95.78 o -3 1 0 4354.94 4471.14 45.02 o -2 1 0 53851.60 59241.94 262.54 o -1 1 0 7.88 11.06 3.51 o 1 1 0 130.07 120.83 5.67 o 2 1 0 2077.43 2180.37 37.86 o 3 1 0 756.68 747.56 22.55 o 4 1 0 4.27 18.29 5.56 o 5 1 0 51.04 42.86 11.11 o 6 1 0 8976.84 9343.54 159.48 o 7 1 0 839.57 817.95 32.06 o 8 1 0 0.01 -5.64 13.63 o 9 1 0 568.91 663.69 43.66 o 10 1 0 1865.99 1833.57 72.32 o 11 1 0 52.27 93.56 49.43 o -11 2 0 2.78 15.78 13.85 o -10 2 0 3319.03 3299.75 327.62 o -9 2 0 5.20 99.81 50.70 o -8 2 0 2135.00 2329.02 69.21 o -7 2 0 188.89 207.13 31.17 o -6 2 0 1678.17 1866.47 82.32 o -5 2 0 359.91 357.53 20.99 o -4 2 0 12.18 -1.40 5.35 o -3 2 0 179.71 132.13 7.48 o -2 2 0 10498.69 11061.22 106.63 o -1 2 0 1622.17 1489.62 34.00 o 0 2 0 43260.25 37810.18 132.32 o 1 2 0 89.49 85.19 6.55 o 2 2 0 12271.41 12455.58 77.29 o 3 2 0 7157.24 6929.35 72.03 o 4 2 0 1674.24 1663.79 42.29 o 5 2 0 883.38 869.82 32.93 o 6 2 0 1508.18 1929.22 55.36 o 7 2 0 175.45 170.39 19.33 o 8 2 0 3775.98 3785.29 69.29 o 9 2 0 59.86 52.45 11.49 o 10 2 0 950.37 1383.54 83.36 o 11 2 0 1113.75 1151.26 51.42 o -11 3 0 296.14 239.08 28.42 o -10 3 0 276.08 258.70 29.18 o -9 3 0 288.13 344.83 36.40 o -8 3 0 630.10 536.21 38.78 o -7 3 0 324.28 408.37 46.20 o -6 3 0 1045.21 1123.21 66.75 o -5 3 0 341.57 357.05 22.38 o -4 3 0 14289.09 14669.37 228.24 o -3 3 0 795.62 815.89 58.94 o -2 3 0 583.48 488.48 17.71 o -1 3 0 2167.83 2102.43 32.56 o 0 3 0 3796.38 3599.20 36.86 o 1 3 0 137.17 134.42 6.34 o 2 3 0 56999.30 58099.75 192.78 o 3 3 0 4.15 10.39 2.27 o 4 3 0 95.55 68.11 7.45 o 5 3 0 245.82 277.23 33.75 o 6 3 0 7512.76 7753.41 234.62 o 7 3 0 65.81 58.56 12.53 o 8 3 0 45.50 39.41 9.40 o 9 3 0 145.02 84.15 14.80 o 10 3 0 516.43 679.46 54.09 o 11 3 0 60.76 28.44 18.54 o -10 4 0 398.76 376.23 27.96 o -9 4 0 62.09 12.29 60.42 o -8 4 0 2813.10 2865.11 88.40 o -7 4 0 599.53 641.95 33.55 o -6 4 0 1991.52 2035.81 93.05 o -5 4 0 69.49 77.12 12.07 o -4 4 0 87.94 164.29 15.36 o -3 4 0 34.32 20.91 11.01 o -2 4 0 15536.72 15758.81 135.43 o -1 4 0 1059.72 1100.83 22.23 o 0 4 0 320.65 353.11 13.66 o 1 4 0 9300.67 8955.56 111.07 o 2 4 0 170309.92 161029.80 501.43 o 3 4 0 446.76 432.60 9.97 o 4 4 0 114.62 142.87 7.03 o 5 4 0 1594.42 1550.46 46.15 o 6 4 0 2303.23 2457.88 82.79 o 7 4 0 485.76 486.23 32.32 o 8 4 0 2019.29 1977.38 52.93 o 9 4 0 151.74 92.16 19.04 o 10 4 0 2346.20 2083.03 118.65 o 11 4 0 514.80 1071.28 441.64 o -10 5 0 799.53 720.30 40.79 o -9 5 0 266.52 266.77 36.94 o -8 5 0 1005.22 839.14 120.89 o -7 5 0 230.87 228.16 20.76 o -6 5 0 370.36 391.01 43.08 o -5 5 0 133.70 120.54 23.45 o -4 5 0 4363.23 4127.22 77.09 o -3 5 0 1103.13 1267.21 45.18 o -2 5 0 9095.36 10069.50 98.69 o -1 5 0 126.06 145.86 8.68 o 0 5 0 12331.82 13253.01 183.04 o 1 5 0 520.81 448.25 11.14 o 2 5 0 1832.05 2052.38 25.49 o 3 5 0 1069.94 1056.62 17.97 o 4 5 0 245.66 240.22 17.39 o 5 5 0 398.08 415.17 25.12 o 6 5 0 1571.41 1550.05 53.29 o 7 5 0 1.19 -13.21 13.21 o 8 5 0 739.47 687.12 31.75 o 9 5 0 32.02 2.25 17.40 o 10 5 0 59.71 47.03 13.72 o 11 5 0 320.81 784.21 373.78 o -10 6 0 252.21 226.52 29.22 o -9 6 0 234.90 237.74 33.35 o -8 6 0 7573.09 7651.78 193.28 o -7 6 0 107.89 125.75 23.76 o -6 6 0 3471.65 3935.31 80.24 o -5 6 0 10.82 24.15 11.48 o -4 6 0 253.08 247.64 30.40 o -3 6 0 668.75 642.36 42.29 o -2 6 0 12003.56 14491.77 177.40 o -1 6 0 461.45 488.32 21.61 o 0 6 0 5459.78 5154.68 71.14 o 1 6 0 30.73 27.98 3.54 o 2 6 0 28240.35 28925.52 126.51 o 3 6 0 1896.71 1876.16 37.79 o 4 6 0 248.04 206.33 11.81 o 5 6 0 2094.71 2156.07 58.79 o 6 6 0 1882.91 1949.44 61.39 o 7 6 0 958.82 947.75 46.90 o 8 6 0 572.62 496.62 28.48 o 9 6 0 1568.65 1437.58 150.85 o 10 6 0 2800.89 2628.22 191.81 o 11 6 0 485.70 884.85 295.38 o -9 7 0 279.96 265.91 34.13 o -8 7 0 1997.27 2090.83 99.84 o -7 7 0 184.87 218.00 35.41 o -6 7 0 911.01 965.79 49.06 o -5 7 0 61.47 28.95 12.21 o -4 7 0 786.57 855.26 38.15 o -3 7 0 271.91 236.28 18.86 o -2 7 0 10447.82 12126.07 129.18 o -1 7 0 130.95 151.96 13.32 o 0 7 0 761.46 666.49 41.45 o 1 7 0 1059.63 961.64 34.33 o 2 7 0 418.76 451.05 19.13 o 3 7 0 6161.27 6234.04 136.13 o 4 7 0 4495.19 4990.41 72.34 o 5 7 0 83.67 73.69 18.15 o 6 7 0 784.46 763.92 55.81 o 7 7 0 641.58 669.38 31.89 o 8 7 0 8635.61 8620.09 117.94 o 9 7 0 27.18 26.29 13.53 o 10 7 0 351.89 300.18 53.55 o 11 7 0 48.73 475.74 329.67 o -9 8 0 156.76 167.54 25.24 o -8 8 0 790.79 884.39 63.35 o -7 8 0 114.90 94.84 25.16 o -6 8 0 567.77 598.23 39.27 o -5 8 0 133.19 146.79 14.20 o -4 8 0 266.60 308.77 24.57 o -3 8 0 851.70 919.96 39.64 o -2 8 0 11108.20 13187.70 234.55 o -1 8 0 1301.39 1651.00 71.83 o 0 8 0 2779.66 2997.60 97.74 o 1 8 0 384.56 446.12 39.09 o 2 8 0 316.12 255.32 30.91 o 3 8 0 5487.05 5567.64 279.02 o 4 8 0 16586.95 16422.05 385.98 o 5 8 0 763.01 704.86 50.34 o 6 8 0 4.82 36.53 15.23 o 7 8 0 1243.29 1199.90 42.90 o 8 8 0 2021.65 1942.89 68.06 o 9 8 0 2.18 14.37 13.02 o 10 8 0 18.62 13.24 17.21 o 11 8 0 448.76 941.18 46.31 o -8 9 0 885.90 950.54 60.85 o -7 9 0 7.75 10.45 15.67 o -6 9 0 637.96 658.32 58.02 o -5 9 0 43.83 38.73 10.65 o -4 9 0 1293.74 1416.14 39.37 o -3 9 0 834.37 893.72 60.21 o -2 9 0 8436.41 9621.49 191.88 o -1 9 0 658.61 766.19 53.67 o 0 9 0 10891.12 12949.19 223.78 o 1 9 0 69.79 59.96 18.59 o 2 9 0 1603.82 1719.58 85.27 o 3 9 0 743.93 697.42 56.68 o 4 9 0 226.35 191.50 23.04 o 5 9 0 2073.16 1953.57 85.90 o 6 9 0 2836.06 2790.25 62.89 o 7 9 0 2362.25 2391.14 61.15 o 8 9 0 52.43 52.03 14.12 o 9 9 0 1.00 -14.31 14.31 o 10 9 0 232.47 188.44 20.44 o 11 9 0 322.75 754.66 38.53 o -8 10 0 128.26 139.77 22.11 o -7 10 0 1.97 -6.22 15.61 o -6 10 0 3693.26 3555.24 127.62 o -5 10 0 192.53 150.39 22.12 o -4 10 0 106.14 95.90 13.69 o -3 10 0 652.50 763.64 43.10 o -2 10 0 10.82 30.89 14.70 o -1 10 0 19.58 22.56 12.38 o 0 10 0 2320.29 2874.22 116.62 o 1 10 0 6.66 8.38 12.86 o 2 10 0 2145.59 2270.65 106.66 o 3 10 0 12.02 -3.39 15.75 o 4 10 0 8493.95 7917.23 205.78 o 5 10 0 24.19 18.61 11.24 o 6 10 0 1390.71 1370.01 45.32 o 7 10 0 327.33 284.26 27.40 o 8 10 0 2862.00 2869.60 80.34 o 9 10 0 56.44 79.67 29.71 o 10 10 0 75.00 44.46 14.03 o -7 11 0 5.07 2.09 10.32 o -6 11 0 34.95 30.66 22.32 o -5 11 0 340.77 308.61 29.24 o -4 11 0 81.34 65.51 25.30 o -3 11 0 255.65 295.93 30.72 o -2 11 0 3024.40 3387.29 135.10 o -1 11 0 238.82 310.42 43.63 o 0 11 0 3617.24 4431.10 156.74 o 1 11 0 8.45 19.77 18.25 o 2 11 0 2187.09 2274.16 114.21 o 3 11 0 13.26 13.45 11.34 o 4 11 0 3734.80 3837.85 115.77 o 5 11 0 1717.48 1753.93 62.85 o 6 11 0 45.22 39.42 14.09 o 7 11 0 5.02 -2.02 16.12 o 8 11 0 8.24 8.00 9.72 o 9 11 0 856.39 739.19 56.80 o 10 11 0 706.06 598.32 36.53 o -7 12 0 157.40 113.63 17.58 o -6 12 0 380.43 331.04 25.07 o -5 12 0 45.54 26.19 12.27 o -4 12 0 0.17 19.33 11.23 o -3 12 0 6.88 -2.86 9.16 o -2 12 0 444.62 460.85 50.41 o -1 12 0 371.10 409.01 51.24 o 0 12 0 3040.68 3586.51 148.03 o 1 12 0 308.66 361.04 49.73 o 2 12 0 136.88 196.20 60.71 o 3 12 0 22.31 44.23 16.46 o 4 12 0 90.21 61.88 13.43 o 5 12 0 4858.25 5007.88 133.93 o 6 12 0 64.37 50.07 20.35 o 7 12 0 1.37 -11.60 11.60 o 8 12 0 0.79 11.99 10.48 o 9 12 0 118.84 76.04 48.49 o -6 13 0 40.26 17.68 10.10 o -5 13 0 495.32 428.01 45.06 o -4 13 0 195.12 189.53 35.84 o -3 13 0 3.67 -1.93 20.38 o -2 13 0 2639.63 3054.18 142.75 o -1 13 0 180.97 202.01 39.67 o 0 13 0 3111.92 3557.06 151.88 o 1 13 0 3365.90 3714.75 109.23 o 2 13 0 1315.97 1352.09 71.64 o 3 13 0 110.82 125.58 34.22 o 4 13 0 1140.35 1198.52 97.63 o 5 13 0 1177.16 1198.56 95.90 o 6 13 0 611.37 624.15 68.59 o 7 13 0 22.60 7.42 13.83 o 8 13 0 198.46 225.40 36.83 o 9 13 0 187.45 156.67 26.55 o -5 14 0 293.85 277.01 32.01 o -4 14 0 193.80 160.72 28.55 o -3 14 0 35.27 30.72 18.78 o -2 14 0 105.67 67.60 25.01 o -1 14 0 303.55 378.84 51.08 o 0 14 0 47.76 54.27 23.27 o 1 14 0 130.70 159.09 24.86 o 2 14 0 1284.02 1399.97 104.12 o 3 14 0 226.72 205.11 41.17 o 4 14 0 28.02 28.02 20.51 o 5 14 0 75.22 74.34 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