#------------------------------------------------------------------------------ #$Date: 2016-04-06 16:42:43 +0300 (Wed, 06 Apr 2016) $ #$Revision: 181874 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/02/04/2020441.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_2020441 _cell_angle_alpha 102.352 _cell_angle_beta 95.258 _cell_angle_gamma 104.153 _cell_length_a 10.1883 _cell_length_b 12.9209 _cell_length_c 23.0447 _exptl_crystal_F_000 1336.00 _reflns_d_resolution_high 0.7103 _cod_data_source_file sk3620Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' TSBB-28 (L0223)' _shelx_refln_list_code 4 _shelx_f_calc_maximum 327.57 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 17.77 9.58 3.12 o 2 0 0 30752.93 31055.04 512.19 o 3 0 0 31.48 37.05 5.99 o 4 0 0 29496.70 29260.92 408.55 o 5 0 0 85.87 74.03 10.96 o 6 0 0 5872.11 5832.69 101.36 o 7 0 0 15.21 21.11 15.55 o 8 0 0 15983.14 17072.35 396.66 o 9 0 0 2.97 62.33 36.69 o 10 0 0 1970.68 2192.73 110.46 o 11 0 0 45.06 2.05 59.59 o 12 0 0 47.18 48.56 97.29 o 13 0 0 37.56 28.37 137.25 o -13 1 0 1448.20 1197.09 322.85 o -12 1 0 236.87 231.53 69.45 o -11 1 0 56.43 52.34 104.69 o -10 1 0 15.83 28.69 34.80 o -9 1 0 2233.46 2214.32 98.03 o -8 1 0 28.36 37.49 18.82 o -7 1 0 3713.70 3799.35 83.79 o -6 1 0 55.67 48.91 16.02 o -5 1 0 2977.77 3050.72 54.67 o -4 1 0 17.89 13.04 7.01 o -3 1 0 8948.03 6107.94 995.26 o -2 1 0 483.09 365.98 70.33 o -1 1 0 3176.62 1265.17 434.17 o 1 1 0 15213.79 14512.50 503.32 o 2 1 0 10.52 14.00 4.20 o 3 1 0 512.51 328.49 79.38 o 4 1 0 180.23 156.41 17.97 o 5 1 0 28.89 112.11 20.53 o 6 1 0 76.12 80.94 23.02 o 7 1 0 5004.96 5393.32 178.77 o 8 1 0 548.59 468.40 44.08 o 9 1 0 772.97 818.08 66.20 o 10 1 0 57.09 44.98 55.53 o 11 1 0 2569.38 2972.90 182.79 o 12 1 0 480.31 426.08 252.92 o 13 1 0 14.31 7.17 98.28 o -14 2 0 36.62 -99.43 141.98 o -13 2 0 9.32 11.98 104.72 o -12 2 0 2515.32 2670.69 304.07 o -11 2 0 3.49 -84.18 114.08 o -10 2 0 63.18 60.31 24.83 o -9 2 0 13.48 9.95 18.45 o -8 2 0 10451.22 11100.26 230.86 o -7 2 0 41.48 2.44 18.82 o -6 2 0 4067.62 3998.15 80.38 o -5 2 0 454.03 414.33 26.06 o -4 2 0 12465.80 11964.33 197.33 o -3 2 0 1559.25 1466.79 40.13 o -2 2 0 26307.37 23227.82 943.60 o -1 2 0 1312.59 1285.54 23.80 o 0 2 0 15912.25 15800.25 289.17 o 1 2 0 432.06 429.54 16.70 o 2 2 0 43362.50 43234.11 957.20 o 3 2 0 953.21 1057.93 36.69 o 4 2 0 4293.02 4449.58 101.67 o 5 2 0 136.54 203.33 25.23 o 6 2 0 8373.84 8774.87 188.24 o 7 2 0 24.46 4.74 24.93 o 8 2 0 1874.74 2029.42 90.32 o 9 2 0 69.87 -44.08 44.08 o 10 2 0 105.94 143.69 64.37 o 11 2 0 455.23 536.17 102.70 o 12 2 0 3018.97 3256.12 389.38 o 13 2 0 29.73 -84.63 198.78 o -14 3 0 9.84 46.45 332.44 o -13 3 0 191.87 153.91 152.68 o -12 3 0 474.84 371.26 126.53 o -11 3 0 981.26 417.94 180.60 o -10 3 0 143.71 98.49 24.27 o -9 3 0 8.26 15.63 18.14 o -8 3 0 312.74 347.01 23.52 o -7 3 0 6058.73 6007.93 114.91 o -6 3 0 2.11 17.19 11.47 o -5 3 0 12168.36 12340.78 266.80 o -4 3 0 4428.27 4838.73 98.78 o -3 3 0 25.66 24.55 12.57 o -2 3 0 1848.53 1667.17 35.35 o -1 3 0 27224.50 26640.60 491.75 o 0 3 0 89.04 87.00 9.10 o 1 3 0 25.32 24.75 11.27 o 2 3 0 99.36 73.57 17.24 o 3 3 0 28669.64 29118.76 659.49 o 4 3 0 2991.14 3196.86 122.66 o 5 3 0 4837.73 5725.77 126.26 o 6 3 0 42.85 0.97 29.14 o 7 3 0 4715.55 4507.10 136.85 o 8 3 0 80.27 13.13 43.04 o 9 3 0 647.05 638.27 69.13 o 10 3 0 277.55 290.79 75.41 o 11 3 0 407.74 285.69 114.84 o 12 3 0 1.67 75.15 116.25 o -14 4 0 575.01 471.77 254.72 o -13 4 0 1.22 -113.24 113.24 o -12 4 0 124.85 130.21 108.87 o -11 4 0 18.66 -26.18 56.58 o -10 4 0 2806.54 3312.07 218.55 o -9 4 0 183.88 198.00 39.14 o -8 4 0 17.96 24.06 32.08 o -7 4 0 1214.39 1353.76 57.41 o -6 4 0 3875.02 3781.78 81.71 o -5 4 0 78.41 87.76 20.09 o -4 4 0 26568.57 26645.30 499.37 o -3 4 0 604.71 624.48 20.43 o -2 4 0 3930.97 3817.56 68.26 o -1 4 0 82.38 64.27 10.98 o 0 4 0 20760.02 20746.43 359.77 o 1 4 0 438.22 423.50 45.51 o 2 4 0 3.36 17.69 20.22 o 3 4 0 794.39 730.02 41.49 o 4 4 0 22146.96 23171.28 659.73 o 5 4 0 65.84 45.48 15.54 o 6 4 0 2266.52 2190.10 87.02 o 7 4 0 255.59 163.11 62.46 o 8 4 0 1350.67 1391.87 111.37 o 9 4 0 183.68 -8.33 65.15 o 10 4 0 1365.41 1254.14 115.29 o 11 4 0 148.77 101.08 121.27 o 12 4 0 3.73 76.52 108.96 o -14 5 0 0.12 -74.73 142.68 o -13 5 0 1749.35 1654.96 180.87 o -12 5 0 384.26 449.83 145.81 o -11 5 0 64.82 145.16 53.81 o -10 5 0 15.21 29.95 62.36 o -9 5 0 4178.28 4462.51 173.64 o -8 5 0 0.25 -37.30 37.30 o -7 5 0 308.55 296.29 28.38 o -6 5 0 0.60 42.43 22.02 o -5 5 0 14290.12 14217.41 272.46 o -4 5 0 938.11 987.90 29.26 o -3 5 0 14324.24 14690.26 244.14 o -2 5 0 13.83 24.77 10.03 o -1 5 0 1248.21 1212.92 38.75 o 0 5 0 62.83 49.86 13.11 o 1 5 0 15980.80 16440.38 428.39 o 2 5 0 70.89 22.81 24.48 o 3 5 0 654.77 750.24 40.91 o 4 5 0 22.96 13.28 23.17 o 5 5 0 8366.54 8792.29 188.97 o 6 5 0 30.15 48.15 16.49 o 7 5 0 1875.26 1649.80 94.24 o 8 5 0 425.54 362.75 79.76 o 9 5 0 940.24 1037.19 158.63 o 10 5 0 58.55 69.82 85.54 o 11 5 0 736.22 548.53 136.31 o 12 5 0 77.76 6.61 117.32 o -14 6 0 281.88 466.89 176.93 o -13 6 0 7.62 -100.48 127.02 o -12 6 0 2840.23 3140.82 282.36 o -11 6 0 24.61 -4.44 53.60 o -10 6 0 92.52 -11.32 48.18 o -9 6 0 5.36 13.01 41.87 o -8 6 0 4421.89 4622.01 131.39 o -7 6 0 138.12 61.51 32.64 o -6 6 0 1774.63 1872.44 66.80 o -5 6 0 439.18 444.82 25.63 o -4 6 0 16005.58 16104.21 239.17 o -3 6 0 29.72 17.52 12.15 o -2 6 0 11703.37 11820.34 182.44 o -1 6 0 1182.25 1574.65 40.58 o 0 6 0 6.00 37.45 17.74 o 1 6 0 263.86 263.68 26.70 o 2 6 0 20264.91 21733.57 447.64 o 3 6 0 482.43 452.20 53.53 o 4 6 0 37.68 34.21 23.91 o 5 6 0 8.99 33.80 25.47 o 6 6 0 4932.83 5015.55 128.18 o 7 6 0 502.26 288.50 81.16 o 8 6 0 2682.70 2690.95 152.35 o 9 6 0 212.99 274.50 98.23 o 10 6 0 1020.77 1023.79 159.21 o 11 6 0 70.79 38.54 148.39 o -14 7 0 28.21 -2.13 154.11 o -13 7 0 234.77 299.47 144.25 o -12 7 0 101.54 14.24 69.04 o -11 7 0 3160.21 3257.34 159.12 o -10 7 0 281.79 186.21 45.95 o -9 7 0 50.38 78.93 44.61 o -8 7 0 2.48 -2.19 33.83 o -7 7 0 5204.91 5340.57 154.76 o -6 7 0 136.32 112.26 14.12 o -5 7 0 2088.91 2240.93 93.97 o -4 7 0 706.53 741.04 27.62 o -3 7 0 15232.38 16188.72 276.93 o -2 7 0 5065.54 5545.70 96.67 o -1 7 0 19087.97 19545.48 334.48 o 0 7 0 1484.38 1617.94 51.22 o 1 7 0 2999.27 3131.46 102.86 o 2 7 0 415.48 360.25 37.33 o 3 7 0 5136.27 5533.51 149.57 o 4 7 0 673.59 721.40 54.49 o 5 7 0 37.32 47.31 33.02 o 6 7 0 66.26 137.34 31.37 o 7 7 0 1812.34 1965.55 126.40 o 8 7 0 0.08 -28.01 65.43 o 9 7 0 615.22 662.09 106.86 o 10 7 0 427.92 501.29 194.59 o 11 7 0 359.32 71.12 241.34 o -14 8 0 469.84 285.74 173.55 o -13 8 0 14.59 5.82 126.16 o -12 8 0 991.91 798.55 119.22 o -11 8 0 61.56 37.94 78.15 o -10 8 0 2768.95 2945.75 148.10 o -9 8 0 16.88 14.94 42.11 o -8 8 0 369.19 393.33 47.37 o -7 8 0 278.45 219.77 64.13 o -6 8 0 7759.89 7941.49 150.71 o -5 8 0 31.97 32.80 16.29 o -4 8 0 1732.87 1721.55 42.15 o -3 8 0 509.65 451.14 29.66 o -2 8 0 11165.73 11625.65 187.12 o -1 8 0 636.16 665.50 35.83 o 0 8 0 13910.02 15226.69 276.43 o 1 8 0 1013.90 1002.07 55.65 o 2 8 0 2372.50 2495.48 88.17 o 3 8 0 65.32 -1.09 44.03 o 4 8 0 2654.25 2825.79 188.43 o 5 8 0 592.52 567.35 70.12 o 6 8 0 21.60 12.62 37.57 o 7 8 0 138.61 134.61 99.93 o 8 8 0 2498.21 2147.72 169.64 o 9 8 0 18.99 22.09 90.72 o 10 8 0 574.64 455.89 411.95 o -13 9 0 781.50 515.15 146.62 o -12 9 0 4.66 14.50 67.29 o -11 9 0 933.74 910.86 94.70 o -10 9 0 208.13 139.70 57.78 o -9 9 0 4672.76 4738.55 185.32 o -8 9 0 28.21 11.22 35.48 o -7 9 0 218.00 142.87 36.51 o -6 9 0 77.42 53.18 20.45 o -5 9 0 9334.32 9705.52 198.88 o -4 9 0 7.56 -8.02 21.17 o -3 9 0 26.87 14.09 19.84 o -2 9 0 431.23 374.94 27.96 o -1 9 0 4616.23 4837.88 120.39 o 0 9 0 31.84 31.29 26.20 o 1 9 0 7559.32 7785.43 230.19 o 2 9 0 332.92 244.31 51.57 o 3 9 0 1787.89 1516.84 143.67 o 4 9 0 63.33 19.82 55.58 o 5 9 0 636.49 671.29 58.02 o 6 9 0 103.83 97.03 87.41 o 7 9 0 390.01 334.44 82.10 o 8 9 0 305.91 242.84 98.46 o 9 9 0 976.94 962.02 162.05 o -13 10 0 55.82 35.21 164.82 o -12 10 0 1005.15 854.54 119.31 o -11 10 0 17.76 13.26 58.08 o -10 10 0 21.44 63.85 76.69 o -9 10 0 200.82 126.49 66.47 o -8 10 0 8986.35 9653.29 290.47 o -7 10 0 204.51 239.83 43.24 o -6 10 0 2138.64 2094.88 74.98 o -5 10 0 1176.74 1237.58 49.24 o -4 10 0 9825.46 10455.84 239.70 o -3 10 0 141.88 97.00 31.37 o -2 10 0 6219.14 6331.85 186.71 o -1 10 0 497.90 457.24 56.56 o 0 10 0 4654.26 4722.12 133.89 o 1 10 0 1085.90 1082.98 76.74 o 2 10 0 11313.07 11714.52 426.12 o 3 10 0 48.71 45.42 122.67 o 4 10 0 462.38 272.59 65.51 o 5 10 0 17.29 -56.61 58.83 o 6 10 0 1483.51 1485.31 153.42 o 7 10 0 2.82 -76.45 181.04 o 8 10 0 103.53 14.29 126.74 o 9 10 0 89.21 152.53 158.69 o -13 11 0 294.63 148.51 105.27 o -12 11 0 0.60 26.00 80.69 o -11 11 0 196.20 114.01 69.62 o -10 11 0 1.11 1.83 55.42 o -9 11 0 57.26 6.46 52.98 o -8 11 0 112.51 117.81 55.79 o -7 11 0 4744.49 4391.51 458.62 o -6 11 0 156.59 104.75 47.95 o -5 11 0 132.91 101.53 37.14 o -4 11 0 109.19 82.89 33.00 o -3 11 0 1331.57 1283.68 68.16 o -2 11 0 7.56 29.00 25.27 o -1 11 0 755.32 686.21 53.04 o 0 11 0 2127.14 1972.47 101.21 o 1 11 0 1672.09 1708.28 151.43 o 2 11 0 351.50 401.83 115.83 o 3 11 0 2645.48 2513.43 180.67 o 4 11 0 1000.11 1015.41 98.20 o 5 11 0 178.21 162.40 66.92 o 6 11 0 120.51 94.44 141.80 o 7 11 0 727.01 505.35 113.49 o 8 11 0 314.02 -13.03 135.09 o -12 12 0 456.40 354.02 108.13 o -11 12 0 1.80 86.81 86.76 o -10 12 0 1576.79 1489.01 162.45 o -9 12 0 65.57 -5.73 81.09 o -8 12 0 85.82 61.08 53.34 o -7 12 0 5.59 -17.32 33.47 o -6 12 0 10027.75 10858.29 343.02 o -5 12 0 356.39 363.87 40.72 o -4 12 0 439.68 483.15 42.71 o -3 12 0 538.40 494.31 47.67 o -2 12 0 5555.37 5781.18 163.30 o -1 12 0 2.88 34.11 37.46 o 0 12 0 3895.96 3675.92 219.17 o 1 12 0 312.79 477.50 116.07 o 2 12 0 3438.44 3638.92 224.54 o 3 12 0 5.01 31.05 71.99 o 4 12 0 2515.57 3093.58 336.25 o 5 12 0 292.16 346.77 106.44 o 6 12 0 22.97 -39.90 96.67 o 7 12 0 87.17 18.40 112.47 o -12 13 0 323.37 346.29 175.42 o -11 13 0 380.27 163.26 79.26 o -10 13 0 73.77 40.55 76.58 o -9 13 0 327.80 291.90 77.01 o -8 13 0 163.23 179.43 43.06 o -7 13 0 141.49 107.34 48.80 o -6 13 0 173.27 180.46 58.47 o -5 13 0 3426.20 3989.32 181.74 o -4 13 0 815.10 858.68 66.92 o -3 13 0 551.17 521.64 54.93 o -2 13 0 4.46 38.56 45.67 o -1 13 0 554.10 611.45 86.58 o 0 13 0 19.18 -10.09 70.29 o 1 13 0 1379.02 1536.10 165.65 o 2 13 0 230.69 288.85 115.50 o 3 13 0 783.79 777.97 104.65 o 4 13 0 1.99 80.03 101.78 o 5 13 0 2137.92 2039.06 258.17 o 6 13 0 294.34 336.08 149.28 o -11 14 0 11.33 -13.80 151.21 o -10 14 0 824.62 870.00 140.42 o -9 14 0 34.79 43.63 74.66 o -8 14 0 2054.83 2030.39 218.50 o -7 14 0 0.43 2.21 80.00 o -6 14 0 148.38 121.08 67.17 o -5 14 0 162.28 143.29 65.30 o -4 14 0 4112.04 4496.21 214.02 o -3 14 0 124.73 90.23 66.50 o -2 14 0 400.14 291.90 124.80 o -1 14 0 121.53 22.12 86.56 o 0 14 0 1835.42 2055.99 220.42 o 1 14 0 13.30 144.10 127.57 o 2 14 0 507.29 641.12 114.18 o 3 14 0 256.12 221.21 96.77 o 4 14 0 135.04 279.84 211.57 o 5 14 0 110.13 -67.32 191.20 o -10 15 0 52.83 -171.34 171.34 o -9 15 0 711.17 490.26 207.38 o -8 15 0 6.07 -58.04 58.04 o -7 15 0 735.35 1021.59 161.31 o -6 15 0 103.78 70.01 231.95 o -5 15 0 31.62 -24.17 80.09 o -4 15 0 0.29 -51.97 72.62 o -3 15 0 2444.13 2837.75 173.95 o -2 15 0 3.91 80.94 118.58 o -1 15 0 381.92 349.10 138.49 o 0 15 0 366.48 45.90 96.94 o 1 15 0 1353.37 1666.96 164.16 o 2 15 0 68.65 177.53 136.72 o 3 15 0 433.15 268.65 151.58 o 4 15 0 119.10 -214.57 266.91 o -9 16 0 151.97 117.50 127.38 o -8 16 0 500.91 444.14 129.44 o -7 16 0 0.01 -68.54 68.54 o -6 16 0 967.47 1105.28 164.83 o -5 16 0 2.89 -90.35 90.35 o -4 16 0 4.83 -13.30 71.77 o -3 16 0 194.54 87.28 87.59 o -2 16 0 1538.86 1470.42 136.29 o -1 16 0 209.99 262.29 97.08 o 0 16 0 484.68 433.03 123.69 o 1 16 0 18.51 70.33 120.99 o 2 16 0 245.95 54.47 159.47 o -7 17 0 91.21 131.50 105.28 o -6 17 0 39.61 140.61 121.27 o -5 17 0 953.59 933.71 144.06 o -4 17 0 311.73 357.21 133.30 o -3 17 0 84.77 2.85 86.02 o -2 17 0 9.66 95.79 97.42 o -1 17 0 1645.14 1621.72 203.21 o 0 17 0 61.13 49.06 113.97 o 0 -17 1 0.36 6.33 118.73 o 1 -17 1 221.84 480.35 121.89 o 2 -17 1 1395.64 1193.87 212.50 o 3 -17 1 9.51 -11.38 94.34 o 4 -17 1 337.58 371.09 143.67 o 5 -17 1 113.86 106.21 95.36 o 6 -17 1 833.00 1224.71 159.14 o 7 -17 1 0.28 -36.97 121.16 o -2 -16 1 150.91 167.66 112.37 o -1 -16 1 806.14 825.74 140.87 o 0 -16 1 322.16 374.82 164.90 o 1 -16 1 40.16 123.67 141.31 o 2 -16 1 174.51 183.09 80.66 o 3 -16 1 1782.18 1633.11 189.89 o 4 -16 1 47.51 -35.01 100.31 o 5 -16 1 890.85 1027.48 161.91 o 6 -16 1 126.93 291.52 150.84 o 7 -16 1 673.55 914.18 117.65 o 8 -16 1 39.03 10.60 106.56 o 9 -16 1 509.16 406.46 108.99 o -4 -15 1 792.49 372.59 323.65 o -3 -15 1 536.67 794.49 147.47 o -2 -15 1 101.41 79.89 92.12 o -1 -15 1 82.21 23.24 110.29 o 0 -15 1 1951.43 2567.20 304.47 o 1 -15 1 90.14 -15.69 203.98 o 2 -15 1 45.33 48.07 73.74 o 3 -15 1 118.57 91.62 64.69 o 4 -15 1 2119.42 2238.70 155.45 o 5 -15 1 5.00 5.75 99.09 o 6 -15 1 1095.96 988.64 104.25 o 7 -15 1 291.57 272.56 87.87 o 8 -15 1 609.05 572.14 76.84 o 9 -15 1 18.41 -74.67 116.97 o 10 -15 1 900.90 912.26 311.65 o -5 -14 1 459.30 92.29 137.65 o -4 -14 1 213.83 95.11 163.82 o -3 -14 1 1434.74 1635.61 191.23 o -2 -14 1 313.54 415.66 132.61 o -1 -14 1 146.49 70.66 122.58 o 0 -14 1 374.45 417.55 100.58 o 1 -14 1 2130.48 2245.14 169.52 o 2 -14 1 39.34 -58.68 58.68 o 3 -14 1 62.92 131.48 52.69 o 4 -14 1 609.23 569.74 102.13 o 5 -14 1 2477.70 2614.56 158.83 o 6 -14 1 18.55 -3.25 51.55 o 7 -14 1 794.14 831.13 80.21 o 8 -14 1 911.65 984.11 80.85 o 9 -14 1 325.09 352.81 86.12 o 10 -14 1 62.30 134.61 130.41 o 11 -14 1 586.11 454.46 136.57 o -6 -13 1 254.97 248.52 191.48 o -5 -13 1 157.64 57.67 162.37 o -4 -13 1 623.13 903.39 123.10 o -3 -13 1 50.45 -121.46 121.46 o -2 -13 1 2984.45 3595.34 255.06 o -1 -13 1 895.60 802.09 144.44 o 0 -13 1 57.82 47.57 92.50 o 1 -13 1 27.38 46.21 99.32 o 2 -13 1 4538.06 4651.95 177.10 o 3 -13 1 158.30 111.52 43.28 o 4 -13 1 472.84 447.74 61.23 o 5 -13 1 271.51 223.17 49.76 o 6 -13 1 2593.73 2509.58 214.42 o 7 -13 1 0.57 47.36 47.36 o 8 -13 1 1732.29 1776.15 169.76 o 9 -13 1 88.56 29.61 57.54 o 10 -13 1 567.84 630.92 94.67 o 11 -13 1 5.99 37.53 70.51 o 12 -13 1 1028.27 609.84 126.00 o -7 -12 1 388.89 289.92 184.64 o -6 -12 1 35.64 -50.61 108.45 o -5 -12 1 337.41 351.60 229.35 o -4 -12 1 1332.44 1386.88 180.40 o -3 -12 1 1468.60 1063.45 156.78 o -2 -12 1 6.12 120.51 149.04 o -1 -12 1 2437.97 2966.90 201.42 o 0 -12 1 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