#------------------------------------------------------------------------------ #$Date: 2016-04-06 16:42:43 +0300 (Wed, 06 Apr 2016) $ #$Revision: 181874 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/02/04/2020442.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_2020442 _cell_angle_alpha 102.266 _cell_angle_beta 100.318 _cell_angle_gamma 91.603 _cell_length_a 12.0462 _cell_length_b 13.6264 _cell_length_c 22.8143 _exptl_crystal_F_000 1612.00 _reflns_d_resolution_high 0.7697 _cod_data_source_file sk3620IIsup3.hkl _cod_data_source_block II #BEGIN Tags that were not found in dictionaries: _shelx_title ' TSBB-30' _shelx_refln_list_code 4 _shelx_f_calc_maximum 515.14 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 4398.29 4199.88 75.94 o 3 0 0 822.88 767.99 23.81 o 4 0 0 22.86 35.29 13.53 o 5 0 0 8353.88 8296.97 121.42 o 6 0 0 2271.58 2108.43 52.26 o 7 0 0 1324.87 1374.92 53.25 o 8 0 0 2483.37 2486.04 74.23 o 9 0 0 96.30 98.75 34.46 o 10 0 0 51.54 83.76 47.11 o 11 0 0 426.22 541.13 64.08 o 12 0 0 153.20 -23.45 64.99 o 13 0 0 592.13 477.65 111.24 o 14 0 0 136.87 180.90 142.06 o 15 0 0 266.03 354.52 150.65 o -15 1 0 72.56 258.42 167.51 o -14 1 0 87.10 -106.25 106.25 o -13 1 0 213.12 184.13 108.77 o -12 1 0 224.61 268.17 65.01 o -11 1 0 141.78 149.61 60.94 o -10 1 0 421.81 388.89 50.06 o -9 1 0 3356.89 3425.89 103.87 o -8 1 0 8312.11 9095.53 185.66 o -7 1 0 10687.16 11288.67 176.88 o -6 1 0 9873.38 9937.09 200.18 o -5 1 0 6823.17 6589.63 112.37 o -4 1 0 68.27 72.82 15.28 o -3 1 0 474.22 500.66 23.00 o -2 1 0 6217.74 6486.87 111.31 o -1 1 0 20481.72 5213.78 3682.51 o 1 1 0 19560.97 13018.81 2187.41 o 2 1 0 1005.38 947.95 39.37 o 3 1 0 104.10 112.31 14.33 o 4 1 0 74.92 119.73 17.72 o 5 1 0 79.88 104.80 24.69 o 6 1 0 12963.88 13827.47 226.75 o 7 1 0 35.92 15.24 23.04 o 8 1 0 160.23 139.54 28.78 o 9 1 0 237.62 195.29 37.22 o 10 1 0 92.54 117.96 42.28 o 11 1 0 50.00 4.71 47.53 o 12 1 0 3507.09 3318.98 198.18 o 13 1 0 1948.13 1911.49 164.34 o 14 1 0 805.57 744.32 171.35 o 15 1 0 680.62 573.54 169.47 o -15 2 0 2075.21 2504.12 258.04 o -14 2 0 1058.58 1161.95 267.69 o -13 2 0 1171.34 1287.20 134.17 o -12 2 0 8.84 -32.27 90.04 o -11 2 0 26.01 11.05 54.52 o -10 2 0 4698.83 4811.91 158.52 o -9 2 0 4987.21 5057.77 125.47 o -8 2 0 3998.64 4269.09 98.68 o -7 2 0 2212.91 2285.47 61.64 o -6 2 0 1990.23 1985.17 54.70 o -5 2 0 1128.54 1125.97 38.02 o -4 2 0 35.46 54.40 16.14 o -3 2 0 1505.05 1552.98 36.72 o -2 2 0 2433.97 2369.60 45.38 o -1 2 0 33731.40 35062.87 513.21 o 0 2 0 2596.06 2731.62 54.37 o 1 2 0 677.27 659.39 17.02 o 2 2 0 111.00 115.04 12.23 o 3 2 0 426.84 425.93 26.09 o 4 2 0 1479.78 1398.43 42.54 o 5 2 0 9755.84 10116.99 197.19 o 6 2 0 15390.45 16333.93 264.54 o 7 2 0 7461.56 7787.54 146.54 o 8 2 0 2162.72 1910.25 72.32 o 9 2 0 6.40 -25.12 37.19 o 10 2 0 212.72 177.61 51.94 o 11 2 0 2522.02 2777.49 177.52 o 12 2 0 2939.93 3048.21 184.07 o 13 2 0 1333.13 1338.24 148.10 o 14 2 0 704.33 616.92 134.72 o 15 2 0 31.97 -44.17 153.60 o -15 3 0 1870.97 1628.47 366.42 o -14 3 0 546.02 510.24 116.70 o -13 3 0 725.73 623.09 126.58 o -12 3 0 125.75 109.55 55.19 o -11 3 0 256.37 216.55 121.75 o -10 3 0 1895.23 1810.73 91.08 o -9 3 0 50.59 -0.95 29.09 o -8 3 0 732.52 632.40 44.36 o -7 3 0 411.47 459.37 33.83 o -6 3 0 922.21 899.65 39.07 o -5 3 0 840.01 957.09 39.15 o -4 3 0 953.33 1170.09 55.80 o -3 3 0 2346.96 2511.77 49.99 o -2 3 0 7387.14 7358.70 150.11 o -1 3 0 11884.04 12127.07 187.19 o 0 3 0 13737.58 13140.49 197.95 o 1 3 0 5728.84 5618.71 87.87 o 2 3 0 25.20 30.64 11.22 o 3 3 0 1818.64 1672.19 52.61 o 4 3 0 7499.24 7268.83 132.18 o 5 3 0 11622.04 10929.21 180.72 o 6 3 0 34766.39 39025.40 596.17 o 7 3 0 3260.52 3236.36 86.54 o 8 3 0 599.91 550.47 44.12 o 9 3 0 158.15 102.71 47.74 o 10 3 0 452.94 476.34 58.96 o 11 3 0 464.13 380.53 61.97 o 12 3 0 463.73 370.49 87.69 o 13 3 0 161.76 213.81 97.21 o 14 3 0 14.60 23.98 136.00 o -15 4 0 148.50 -11.16 140.07 o -14 4 0 75.53 212.23 114.11 o -13 4 0 66.70 80.97 82.91 o -12 4 0 12.11 -20.54 74.60 o -11 4 0 202.38 192.47 67.03 o -10 4 0 10.22 3.11 41.54 o -9 4 0 3.84 -39.07 39.07 o -8 4 0 918.32 981.00 49.53 o -7 4 0 574.59 478.30 35.04 o -6 4 0 1681.95 1928.89 72.67 o -5 4 0 1160.43 1264.60 42.12 o -4 4 0 13726.86 14838.56 196.54 o -3 4 0 25006.37 25837.95 346.60 o -2 4 0 40101.09 42531.79 628.94 o -1 4 0 12240.23 12419.11 192.94 o 0 4 0 8331.51 7731.57 134.03 o 1 4 0 1071.50 893.51 22.17 o 2 4 0 1362.21 1534.23 35.30 o 3 4 0 9317.55 9518.92 227.15 o 4 4 0 4833.62 4868.88 93.15 o 5 4 0 8171.13 8802.05 167.78 o 6 4 0 8456.92 8493.78 154.73 o 7 4 0 145.46 162.10 31.62 o 8 4 0 85.21 86.22 32.98 o 9 4 0 24.27 -14.79 42.83 o 10 4 0 6.72 -32.56 42.73 o 11 4 0 69.80 79.19 58.11 o 12 4 0 521.33 379.09 88.53 o 13 4 0 214.92 180.53 106.11 o 14 4 0 69.82 80.22 130.77 o -15 5 0 382.54 218.29 248.47 o -14 5 0 564.03 801.41 129.19 o -13 5 0 98.60 144.66 92.44 o -12 5 0 64.11 -21.23 69.16 o -11 5 0 406.21 332.63 70.75 o -10 5 0 2159.69 2411.62 101.96 o -9 5 0 6022.34 6242.19 195.85 o -8 5 0 3176.96 3208.10 86.90 o -7 5 0 6521.09 6789.02 131.56 o -6 5 0 18.25 -2.53 21.40 o -5 5 0 951.99 952.26 35.57 o -4 5 0 24335.52 26418.36 339.64 o -3 5 0 7254.10 7430.48 106.89 o -2 5 0 8116.30 8637.96 165.93 o -1 5 0 4148.79 4179.31 74.17 o 0 5 0 268.08 275.29 15.32 o 1 5 0 156.82 138.24 12.90 o 2 5 0 200.58 159.62 14.86 o 3 5 0 612.90 559.83 25.18 o 4 5 0 313.11 386.22 26.04 o 5 5 0 8.86 26.62 33.74 o 6 5 0 443.97 384.64 36.08 o 7 5 0 280.82 199.74 38.75 o 8 5 0 4.78 32.04 36.94 o 9 5 0 731.42 752.43 64.87 o 10 5 0 1236.63 1303.24 85.33 o 11 5 0 2497.92 2659.15 142.10 o 12 5 0 2264.85 2231.67 193.27 o 13 5 0 642.66 633.71 167.34 o 14 5 0 177.86 -169.98 169.98 o -14 6 0 126.16 230.42 242.44 o -13 6 0 9.85 1.73 102.66 o -12 6 0 939.90 822.82 116.81 o -11 6 0 2252.22 2309.59 190.02 o -10 6 0 2123.13 2046.88 121.99 o -9 6 0 3077.76 3235.53 164.02 o -8 6 0 2016.89 1895.61 75.06 o -7 6 0 140.47 112.21 28.82 o -6 6 0 7.96 9.86 20.24 o -5 6 0 707.91 821.36 38.73 o -4 6 0 1025.73 906.67 32.50 o -3 6 0 746.53 685.00 30.71 o -2 6 0 18.87 -5.66 16.48 o -1 6 0 412.12 418.23 21.77 o 0 6 0 474.31 511.99 21.91 o 1 6 0 444.20 440.15 28.54 o 2 6 0 1604.00 1637.43 41.23 o 3 6 0 5053.38 5099.75 94.84 o 4 6 0 7116.19 7341.60 119.22 o 5 6 0 2096.84 1967.88 74.50 o 6 6 0 4262.47 4167.28 106.02 o 7 6 0 628.09 587.87 58.59 o 8 6 0 375.76 404.71 47.65 o 9 6 0 2491.80 2800.16 130.23 o 10 6 0 2144.05 2231.01 121.46 o 11 6 0 2181.01 2173.10 146.28 o 12 6 0 784.62 801.76 126.49 o 13 6 0 271.16 295.77 107.83 o 14 6 0 3.27 395.34 257.52 o -14 7 0 80.00 -99.01 110.06 o -13 7 0 245.92 205.26 121.74 o -12 7 0 327.53 280.16 170.51 o -11 7 0 1332.86 1214.63 90.29 o -10 7 0 26.34 -34.44 52.84 o -9 7 0 115.54 85.99 40.20 o -8 7 0 95.27 71.58 32.02 o -7 7 0 0.43 63.91 30.13 o -6 7 0 34.83 37.66 24.75 o -5 7 0 417.15 449.04 29.77 o -4 7 0 4459.81 4309.69 85.15 o -3 7 0 7308.24 7438.99 117.66 o -2 7 0 2033.75 2201.20 52.05 o -1 7 0 9204.13 9788.25 146.59 o 0 7 0 157.03 172.67 17.61 o 1 7 0 7871.04 8300.20 128.74 o 2 7 0 15967.26 17021.66 242.62 o 3 7 0 2901.28 2708.55 59.36 o 4 7 0 23795.37 25490.39 364.07 o 5 7 0 5844.08 5930.70 123.93 o 6 7 0 518.02 549.54 53.43 o 7 7 0 93.20 60.75 30.58 o 8 7 0 403.05 374.03 70.33 o 9 7 0 495.32 466.85 53.36 o 10 7 0 2047.66 1873.62 112.40 o 11 7 0 222.12 122.07 73.40 o 12 7 0 21.93 38.32 99.91 o 13 7 0 59.44 50.07 131.61 o -14 8 0 0.77 -95.96 198.17 o -13 8 0 15.43 -92.76 111.33 o -12 8 0 17.47 -112.92 112.92 o -11 8 0 5.83 79.06 94.38 o -10 8 0 818.72 780.58 81.54 o -9 8 0 3821.93 3589.45 126.38 o -8 8 0 772.25 759.60 56.48 o -7 8 0 4.59 -28.76 28.76 o -6 8 0 1932.18 2027.17 63.80 o -5 8 0 4067.81 4502.75 95.81 o -4 8 0 6875.09 7363.77 147.55 o -3 8 0 9865.15 10387.86 168.79 o -2 8 0 4586.61 4729.69 86.19 o -1 8 0 1149.83 1284.36 41.27 o 0 8 0 410.70 348.13 20.96 o 1 8 0 5697.60 5461.56 98.05 o 2 8 0 7899.89 7886.55 131.27 o 3 8 0 1769.18 1639.68 67.07 o 4 8 0 3723.23 3948.80 121.24 o 5 8 0 960.34 987.65 32.96 o 6 8 0 90.57 84.00 35.99 o 7 8 0 974.68 902.82 70.34 o 8 8 0 20.99 71.48 37.79 o 9 8 0 2062.45 2042.60 96.77 o 10 8 0 644.88 607.98 103.02 o 11 8 0 989.44 744.47 126.92 o 12 8 0 329.39 357.50 135.57 o 13 8 0 21.23 73.82 194.64 o -13 9 0 251.22 218.28 177.96 o -12 9 0 1060.93 1031.76 142.06 o -11 9 0 1877.96 2398.70 299.27 o -10 9 0 2536.95 2571.42 146.62 o -9 9 0 2181.28 2016.50 97.78 o -8 9 0 233.76 272.94 48.50 o -7 9 0 220.86 155.29 39.66 o -6 9 0 1488.76 1518.78 73.25 o -5 9 0 6222.93 6447.41 150.71 o -4 9 0 1999.33 2115.80 68.26 o -3 9 0 215.84 265.68 29.63 o -2 9 0 2794.86 2975.41 69.86 o -1 9 0 67.48 84.49 22.32 o 0 9 0 272.26 229.36 31.00 o 1 9 0 47.60 58.58 15.66 o 2 9 0 7.98 -11.15 17.32 o 3 9 0 127.67 36.58 36.85 o 4 9 0 155.90 199.51 39.94 o 5 9 0 90.84 109.75 46.33 o 6 9 0 177.17 131.93 58.90 o 7 9 0 77.86 -8.34 27.04 o 8 9 0 3709.15 3439.14 151.09 o 9 9 0 984.78 1045.03 128.48 o 10 9 0 1688.79 1621.64 348.06 o 11 9 0 1565.25 1399.85 139.07 o 12 9 0 225.16 138.53 144.74 o -13 10 0 897.35 358.62 376.23 o -12 10 0 1068.40 887.28 176.16 o -11 10 0 1293.01 1205.64 256.52 o -10 10 0 974.19 894.01 153.35 o -9 10 0 513.25 398.80 83.13 o -8 10 0 226.73 200.03 44.78 o -7 10 0 162.87 53.03 38.97 o -6 10 0 1666.71 1604.61 136.79 o -5 10 0 5610.13 5543.24 126.90 o -4 10 0 8689.33 9370.39 181.45 o -3 10 0 71.02 50.71 27.16 o -2 10 0 22.90 48.19 26.97 o -1 10 0 9.06 10.99 26.10 o 0 10 0 212.96 173.81 31.83 o 1 10 0 2449.66 2464.10 53.83 o 2 10 0 9586.42 10354.15 209.46 o 3 10 0 3685.80 3852.25 116.96 o 4 10 0 2009.33 1936.38 80.34 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392.32 o -9 12 0 22.72 83.49 154.92 o -7 12 0 1472.94 1417.74 177.55 o -6 12 0 3278.58 3337.89 152.54 o -5 12 0 3793.49 3900.39 143.93 o -4 12 0 1025.12 1119.23 68.31 o -3 12 0 1766.10 1730.33 125.40 o -2 12 0 306.27 332.00 43.37 o -1 12 0 359.16 389.20 54.52 o 0 12 0 7203.87 7541.50 210.89 o 1 12 0 1608.10 1659.39 102.70 o 2 12 0 1557.21 1444.23 74.33 o 3 12 0 300.15 259.78 57.46 o 4 12 0 0.07 -40.68 69.55 o 5 12 0 46.44 -0.27 67.40 o 6 12 0 0.42 6.05 107.06 o 7 12 0 54.68 102.36 144.75 o 8 12 0 327.55 569.19 156.71 o 9 12 0 201.47 104.59 115.86 o 10 12 0 62.44 -121.72 289.21 o -10 13 0 203.82 161.60 184.86 o -9 13 0 256.21 393.83 208.74 o -8 13 0 1053.58 872.34 170.97 o -7 13 0 1487.25 1888.18 270.60 o -6 13 0 2258.58 2058.71 262.00 o -5 13 0 2318.45 2372.87 156.69 o -4 13 0 349.72 269.98 61.45 o -3 13 0 4.17 113.83 43.12 o -2 13 0 52.15 51.62 45.50 o -1 13 0 87.39 65.95 66.62 o 0 13 0 510.36 454.36 49.01 o 1 13 0 605.98 433.43 88.22 o 2 13 0 423.48 339.41 148.38 o 3 13 0 129.16 54.64 67.54 o 4 13 0 0.36 16.47 87.09 o 5 13 0 28.58 3.27 92.77 o 6 13 0 1039.89 872.96 140.77 o 7 13 0 1735.84 1683.18 229.57 o 8 13 0 2153.26 2076.48 225.18 o 9 13 0 1004.62 970.38 287.70 o -9 14 0 17.72 -147.11 147.11 o -8 14 0 60.65 -196.66 202.70 o -7 14 0 169.29 119.21 196.66 o -6 14 0 539.26 651.26 147.91 o -5 14 0 59.01 46.19 97.09 o -4 14 0 39.32 65.20 94.10 o -3 14 0 0.05 -28.03 61.15 o -2 14 0 214.94 149.70 94.37 o -1 14 0 868.74 854.81 68.45 o 0 14 0 587.39 621.81 88.20 o 1 14 0 1426.01 1225.61 123.88 o 2 14 0 1663.44 1392.24 155.34 o 3 14 0 147.03 39.43 114.57 o 4 14 0 107.28 126.40 191.50 o 5 14 0 446.08 504.85 141.19 o 6 14 0 1454.98 1314.52 189.78 o 7 14 0 2507.51 2385.77 234.25 o 8 14 0 2322.47 1954.99 379.75 o -8 15 0 151.38 -0.51 186.29 o -7 15 0 1347.06 1236.70 471.29 o -6 15 0 407.97 637.78 258.53 o -5 15 0 358.11 271.68 148.77 o -4 15 0 135.15 240.50 170.76 o -3 15 0 225.66 236.10 117.69 o -2 15 0 1993.71 2028.01 309.33 o -1 15 0 2949.11 3361.47 287.45 o 0 15 0 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204.48 o -1 -16 1 412.82 473.49 187.60 o 0 -16 1 44.08 171.32 152.53 o 1 -16 1 0.42 -53.32 184.09 o 2 -16 1 70.85 -33.07 94.95 o 3 -16 1 190.66 -16.79 148.82 o 4 -16 1 3.73 -149.38 218.29 o 5 -16 1 133.25 -8.91 139.86 o 6 -16 1 11.41 15.80 157.83 o -6 -15 1 2.24 -99.62 133.37 o -5 -15 1 104.84 41.16 122.01 o -4 -15 1 285.41 116.50 169.81 o -3 -15 1 275.41 182.64 113.09 o -2 -15 1 16.44 48.84 93.83 o -1 -15 1 188.46 202.13 111.39 o 0 -15 1 168.09 192.97 88.64 o 1 -15 1 2.84 41.75 92.58 o 2 -15 1 253.08 280.66 128.76 o 3 -15 1 425.74 601.41 118.54 o 4 -15 1 2249.74 2354.26 196.70 o 5 -15 1 2307.79 1952.82 530.89 o 6 -15 1 174.36 -14.24 119.55 o 7 -15 1 249.17 197.80 131.71 o 8 -15 1 93.19 -49.89 173.89 o -8 -14 1 0.13 -166.70 166.70 o -7 -14 1 8.98 -110.91 110.91 o -6 -14 1 24.62 -83.03 106.27 o -5 -14 1 244.07 177.90 111.13 o -4 -14 1 202.12 95.65 112.01 o -3 -14 1 2250.71 2393.17 320.90 o -2 -14 1 297.68 360.11 171.26 o -1 -14 1 1595.62 1703.14 127.52 o 0 -14 1 237.38 265.74 83.59 o 1 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