#------------------------------------------------------------------------------ #$Date: 2016-06-25 04:21:35 +0300 (Sat, 25 Jun 2016) $ #$Revision: 183915 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/02/05/2020541.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2020541 _cell_angle_alpha 93.079 _cell_angle_beta 92.995 _cell_angle_gamma 118.475 _cell_length_a 13.3716 _cell_length_b 13.5971 _cell_length_c 17.7021 _exptl_crystal_F_000 1248.00 _reflns_d_resolution_high 0.6869 _cod_data_source_file sk3627mol-3sup4.hkl _cod_data_source_block mol-3 _shelx_title ' mol-3 in P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 292.09 _shelx_f_squared_multiplier 1.000 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 4233.46 3139.16 280.29 o 2 0 0 665.98 691.17 18.55 o 3 0 0 6151.83 6412.32 87.43 o 4 0 0 744.39 686.63 26.95 o 5 0 0 323.79 398.63 25.13 o 6 0 0 11889.42 11576.94 143.48 o 7 0 0 6309.49 6414.92 106.99 o 8 0 0 47.60 12.59 19.19 o 9 0 0 1765.64 1762.69 106.12 o 10 0 0 2976.00 2895.77 82.91 o 11 0 0 342.97 358.41 39.99 o 12 0 0 775.49 840.98 112.29 o 13 0 0 1232.66 1183.34 138.17 o 14 0 0 109.29 -17.88 37.81 o 15 0 0 1816.81 1841.74 155.97 o 16 0 0 1090.18 1423.04 157.25 o -17 1 0 937.88 1015.83 142.94 o -16 1 0 1772.14 1627.89 152.02 o -15 1 0 14.84 -25.81 25.81 o -14 1 0 2242.67 2149.57 155.61 o -13 1 0 3714.28 3564.65 192.31 o -12 1 0 163.28 203.19 50.21 o -11 1 0 565.15 606.50 62.16 o -10 1 0 70.57 90.38 37.59 o -9 1 0 1627.82 1595.15 59.77 o -8 1 0 6989.22 6943.31 118.77 o -7 1 0 3607.08 3501.93 77.47 o -6 1 0 10609.49 11462.56 142.39 o -5 1 0 10739.05 10986.35 124.34 o -4 1 0 279.73 200.36 15.71 o -3 1 0 257.45 256.35 14.76 o -2 1 0 893.19 884.08 14.78 o -1 1 0 32888.11 31464.69 2815.10 o 0 1 0 5095.27 5312.11 49.33 o 1 1 0 1679.59 1738.12 18.81 o 2 1 0 8676.07 9341.68 68.70 o 3 1 0 3414.03 3538.99 39.64 o 4 1 0 3002.34 3268.68 66.35 o 5 1 0 3751.44 3615.67 65.59 o 6 1 0 5064.71 5065.85 85.62 o 7 1 0 2.45 -16.49 32.03 o 8 1 0 2377.12 2412.56 103.48 o 9 1 0 4755.11 4730.08 98.74 o 10 1 0 152.01 162.05 28.77 o 11 1 0 1156.33 1054.47 120.94 o 12 1 0 2367.07 2108.68 147.91 o 13 1 0 422.34 506.43 97.28 o 14 1 0 806.35 680.84 105.53 o 15 1 0 353.82 378.53 88.07 o 16 1 0 239.97 194.70 72.53 o -17 2 0 635.32 741.63 127.90 o -16 2 0 450.84 470.49 94.52 o -15 2 0 283.77 393.36 97.61 o -14 2 0 1781.60 1521.08 133.57 o -13 2 0 828.88 842.19 106.66 o -12 2 0 2621.03 2422.71 87.65 o -11 2 0 1786.07 1717.46 69.58 o -10 2 0 1284.98 1301.29 77.16 o -9 2 0 36.05 22.00 18.28 o -8 2 0 6022.44 5883.02 110.42 o -7 2 0 8736.49 9387.37 136.75 o -6 2 0 410.03 406.18 31.62 o -5 2 0 14334.05 14620.43 128.29 o -4 2 0 16918.23 17072.85 132.86 o -3 2 0 15282.33 16452.34 100.63 o -2 2 0 3640.66 3948.93 32.25 o -1 2 0 358.53 407.06 16.19 o 0 2 0 1637.35 1857.39 84.85 o 1 2 0 4956.29 4878.79 44.14 o 2 2 0 27788.77 28868.40 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14.17 o 1 5 0 2436.56 2557.93 59.19 o 2 5 0 20954.08 21960.28 217.95 o 3 5 0 7591.19 7777.86 198.78 o 4 5 0 1146.33 1318.04 85.81 o 5 5 0 1156.26 1096.59 92.12 o 6 5 0 3345.15 3264.55 147.97 o 7 5 0 1924.26 1736.83 120.00 o 8 5 0 1324.02 1482.89 115.33 o 9 5 0 4093.50 4174.95 194.61 o 10 5 0 154.24 125.86 62.34 o 11 5 0 347.42 422.49 94.28 o 12 5 0 971.55 832.12 118.93 o 13 5 0 117.40 220.45 67.65 o 14 5 0 120.74 102.05 66.16 o -19 6 0 19.72 187.49 74.42 o -18 6 0 186.27 357.97 101.36 o -17 6 0 1753.64 1917.48 154.45 o -16 6 0 513.78 453.95 86.30 o -15 6 0 208.91 180.63 42.06 o -14 6 0 4569.07 4328.20 179.93 o -13 6 0 971.87 1120.17 83.44 o -12 6 0 857.07 850.99 66.26 o -11 6 0 4203.57 4445.45 120.10 o -10 6 0 6373.11 6073.14 134.47 o -9 6 0 938.34 866.88 117.81 o -8 6 0 2929.11 2926.31 84.75 o -7 6 0 491.48 384.95 37.48 o -6 6 0 2129.58 2134.96 131.13 o -5 6 0 6329.51 5940.22 123.72 o -4 6 0 9918.24 9554.25 137.50 o -3 6 0 2383.32 2681.88 68.40 o -2 6 0 2876.78 2692.93 67.85 o -1 6 0 6449.52 6507.14 144.43 o 0 6 0 279.82 328.11 70.97 o 1 6 0 4666.54 4302.54 111.68 o 2 6 0 4745.89 4573.10 189.84 o 3 6 0 20.26 8.13 22.58 o 4 6 0 4346.83 4300.98 81.80 o 5 6 0 3659.29 3640.39 155.51 o 6 6 0 9.72 50.54 33.28 o 7 6 0 579.26 538.93 81.07 o 8 6 0 3945.50 3813.71 183.38 o 9 6 0 277.80 316.61 71.29 o 10 6 0 218.47 296.03 68.78 o 11 6 0 1742.72 1956.10 150.06 o 12 6 0 430.32 509.72 105.10 o 13 6 0 47.36 232.58 68.58 o -19 7 0 324.63 321.48 105.49 o -18 7 0 900.20 1242.55 149.13 o -17 7 0 281.93 323.14 84.77 o -16 7 0 95.82 105.04 39.32 o -15 7 0 2312.38 2250.22 101.52 o -14 7 0 2237.12 2252.78 97.76 o -13 7 0 1097.56 1122.24 128.73 o -12 7 0 4244.98 4295.74 124.17 o -11 7 0 2985.96 2946.33 100.40 o -10 7 0 567.31 523.35 50.97 o -9 7 0 2931.59 2912.19 90.90 o -8 7 0 5667.18 5863.32 240.46 o -7 7 0 196.88 248.92 32.81 o -6 7 0 1896.28 1803.08 65.24 o -5 7 0 10930.02 11277.18 287.60 o -4 7 0 547.00 557.16 42.24 o -3 7 0 16876.55 16533.88 200.22 o -2 7 0 15907.29 15962.18 195.15 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1027.12 1073.48 120.19 o 5 10 0 3288.46 3571.30 185.66 o 6 10 0 68.14 45.03 48.42 o 7 10 0 263.84 255.82 74.38 o 8 10 0 3960.50 4049.19 217.92 o 9 10 0 585.95 547.85 108.37 o -19 11 0 158.36 50.76 43.28 o -18 11 0 1383.10 1510.63 106.15 o -17 11 0 561.30 609.26 145.38 o -16 11 0 528.70 518.62 67.92 o -15 11 0 1690.19 1762.11 98.05 o -14 11 0 1512.84 1540.92 88.82 o -13 11 0 86.19 144.55 41.21 o -12 11 0 339.14 404.81 54.91 o -11 11 0 3677.55 3504.09 118.95 o -10 11 0 125.06 156.99 36.14 o -9 11 0 6080.36 5671.78 143.70 o -8 11 0 5248.00 5015.20 132.25 o -7 11 0 544.55 572.23 55.20 o -6 11 0 268.32 241.07 66.03 o -5 11 0 1424.72 1396.89 69.06 o -4 11 0 296.69 346.66 84.87 o -3 11 0 6711.68 6477.48 337.64 o -2 11 0 101.53 134.61 35.52 o -1 11 0 737.94 642.88 54.04 o 0 11 0 877.52 924.08 58.40 o 1 11 0 2472.69 2530.72 125.87 o 2 11 0 360.62 441.99 85.96 o 3 11 0 429.26 435.30 85.08 o 4 11 0 1041.25 977.19 122.48 o 5 11 0 152.44 169.31 69.89 o 6 11 0 368.25 222.38 81.19 o 7 11 0 1793.55 1950.89 158.49 o 8 11 0 340.67 419.29 90.98 o -19 12 0 390.84 474.62 71.75 o -18 12 0 310.62 378.03 65.72 o -17 12 0 46.43 60.15 73.57 o -16 12 0 1298.64 1262.79 99.72 o -15 12 0 1935.40 1986.90 115.91 o -14 12 0 379.28 342.83 55.10 o -13 12 0 1445.05 1469.47 166.11 o -12 12 0 1417.30 1513.39 118.06 o -11 12 0 59.92 43.52 48.68 o -10 12 0 3140.25 2908.18 176.16 o -9 12 0 3494.43 3261.73 217.49 o -8 12 0 5.31 50.10 30.45 o -7 12 0 767.43 737.76 99.10 o -6 12 0 9927.68 9658.49 188.39 o -5 12 0 3765.70 3528.92 119.80 o -4 12 0 42.88 40.22 26.35 o -3 12 0 3968.39 3673.53 113.92 o -2 12 0 2202.61 2126.03 86.15 o -1 12 0 1018.48 1132.52 71.76 o 0 12 0 4199.11 4256.03 119.07 o 1 12 0 2157.38 2222.68 144.14 o 2 12 0 22.99 -3.38 41.40 o 3 12 0 610.79 681.43 102.50 o 4 12 0 3473.67 3630.50 196.24 o 5 12 0 83.97 52.54 55.23 o 6 12 0 1223.45 1043.42 134.52 o 7 12 0 429.58 633.20 115.56 o -18 13 0 312.58 219.33 59.12 o -17 13 0 312.13 371.92 62.92 o -16 13 0 1554.64 1568.13 104.37 o -15 13 0 389.49 287.74 54.30 o -14 13 0 1544.80 1583.34 94.44 o -13 13 0 807.42 859.00 80.09 o -12 13 0 1142.60 1210.17 79.93 o -11 13 0 1060.15 1149.48 87.44 o -10 13 0 3037.87 2872.76 150.13 o -9 13 0 514.20 494.52 57.08 o -8 13 0 1641.46 1605.47 132.33 o -7 13 0 2417.70 2404.11 98.82 o -6 13 0 487.67 448.72 64.33 o -5 13 0 128.01 106.26 32.48 o -4 13 0 5095.23 4941.67 137.83 o -3 13 0 3059.66 2728.40 102.53 o -2 13 0 443.64 345.72 47.59 o -1 13 0 3676.85 3832.76 118.38 o 0 13 0 427.38 417.89 88.36 o 1 13 0 0.35 -43.41 43.41 o 2 13 0 786.87 841.13 119.63 o 3 13 0 1285.19 1225.85 146.00 o 4 13 0 2.94 -16.99 53.95 o 5 13 0 1442.30 1514.53 168.31 o 6 13 0 1534.12 1596.93 148.43 o -18 14 0 583.63 665.76 130.63 o -17 14 0 3064.59 3221.35 193.90 o -16 14 0 283.66 335.16 60.60 o -15 14 0 202.52 240.44 90.27 o -14 14 0 1044.84 1021.45 90.33 o -13 14 0 122.88 128.99 42.70 o -12 14 0 5.36 -18.50 27.91 o -11 14 0 875.80 835.15 77.98 o -10 14 0 1853.09 1717.82 106.52 o -9 14 0 245.70 166.24 40.38 o -8 14 0 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