#------------------------------------------------------------------------------ #$Date: 2016-08-27 04:13:54 +0300 (Sat, 27 Aug 2016) $ #$Revision: 186037 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/02/05/2020575.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2020575 _cell_angle_alpha 90.000 _cell_angle_beta 118.346 _cell_angle_gamma 90.000 _cell_length_a 12.0330 _cell_length_b 4.0256 _cell_length_c 11.5992 _exptl_crystal_F_000 232.00 _reflns_d_resolution_high 0.8156 _cod_data_source_file sk3636Isup2.hkl _cod_data_source_block I _shelx_title ' mhtr33_12 in P2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 67.74 _shelx_f_squared_multiplier 1.000 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 4 0 0 394.33 379.60 3.75 o 5 0 0 1119.01 1102.56 5.60 o 6 0 0 1048.51 1121.12 5.20 o 7 0 0 14.09 28.56 1.21 o 8 0 0 23.41 28.91 1.44 o 9 0 0 8.47 18.28 1.40 o 10 0 0 0.00 10.44 1.22 o 11 0 0 12.71 16.61 0.73 o 12 0 0 19.76 20.57 2.82 o 1 1 0 240.96 256.47 2.96 o 2 1 0 712.26 662.61 11.20 o 3 1 0 50.53 42.05 2.13 o 4 1 0 295.92 304.65 8.66 o 5 1 0 74.83 82.18 5.37 o 6 1 0 199.81 203.75 14.65 o 7 1 0 72.40 73.94 1.82 o 8 1 0 26.36 28.43 0.86 o 9 1 0 299.11 282.16 23.18 o 10 1 0 38.16 32.41 1.71 o 11 1 0 8.60 9.24 0.67 o 12 1 0 0.05 0.45 0.67 o 0 2 0 369.53 329.80 11.21 o 1 2 0 110.74 109.43 2.62 o 2 2 0 19.86 18.30 0.76 o 3 2 0 571.84 567.98 4.99 o 4 2 0 108.93 110.31 2.97 o 5 2 0 15.91 17.38 0.88 o 6 2 0 108.99 105.79 2.07 o 7 2 0 45.99 38.41 2.24 o 8 2 0 140.15 133.22 4.12 o 9 2 0 437.57 381.15 44.98 o 10 2 0 205.45 192.48 13.49 o 11 2 0 8.26 9.63 0.87 o 1 3 0 134.24 132.80 9.10 o 2 3 0 12.55 10.85 0.75 o 3 3 0 46.77 44.41 2.72 o 4 3 0 3.54 4.63 0.62 o 5 3 0 42.10 47.75 1.58 o 6 3 0 1.04 2.12 0.51 o 7 3 0 21.08 20.92 1.03 o 8 3 0 15.70 14.95 1.02 o 9 3 0 0.00 -0.15 0.75 o 10 3 0 10.80 11.77 0.92 o 0 4 0 163.84 177.05 7.14 o 1 4 0 0.06 0.46 0.57 o 2 4 0 0.55 1.12 0.51 o 3 4 0 8.99 9.35 0.64 o 4 4 0 0.04 0.57 0.54 o 5 4 0 153.20 172.92 1.76 o 6 4 0 2.33 3.59 0.65 o 7 4 0 26.74 29.33 0.74 o -13 1 1 17.87 20.63 1.68 o -12 1 1 11.29 11.81 1.33 o -11 1 1 42.94 44.32 1.12 o -10 1 1 4.73 3.16 0.59 o -9 1 1 380.74 383.96 6.62 o -8 1 1 3.77 2.72 0.55 o -7 1 1 30.89 28.01 1.58 o -6 1 1 236.66 257.99 3.19 o -5 1 1 186.29 184.15 1.61 o -4 1 1 863.64 859.07 17.68 o -3 1 1 15.37 16.09 0.72 o -2 1 1 462.72 442.19 19.89 o -1 1 1 131.85 137.74 4.68 o 0 1 1 3636.64 3678.42 69.74 o 1 1 1 466.92 460.62 19.05 o 2 1 1 38.74 37.63 1.44 o 3 1 1 10.62 16.29 0.66 o 4 1 1 210.20 217.94 9.19 o 5 1 1 137.30 119.41 3.19 o 6 1 1 36.75 38.64 0.75 o 7 1 1 49.96 40.52 2.02 o 8 1 1 63.34 54.47 2.39 o 9 1 1 19.21 25.13 0.84 o 10 1 1 62.22 56.20 1.35 o 11 1 1 15.55 13.53 0.91 o 12 1 1 9.07 12.58 0.73 o -12 2 1 3.22 2.87 0.55 o -11 2 1 16.24 17.80 0.75 o -10 2 1 6.84 3.68 0.90 o -9 2 1 55.26 60.66 4.18 o -8 2 1 1.44 1.93 0.64 o -7 2 1 9.33 9.71 0.59 o -6 2 1 24.64 28.05 1.33 o -5 2 1 248.64 246.02 11.66 o -4 2 1 1.38 1.73 0.44 o -3 2 1 141.41 142.40 7.85 o -2 2 1 0.93 0.57 0.67 o -1 2 1 31.78 30.78 1.70 o 0 2 1 0.25 2.39 0.77 o 1 2 1 27.93 26.93 0.78 o 2 2 1 0.46 1.25 0.62 o 3 2 1 176.14 166.48 5.42 o 4 2 1 2.65 3.80 0.44 o 5 2 1 34.73 37.41 0.90 o 6 2 1 2.52 2.61 0.53 o 7 2 1 90.54 96.37 1.15 o 8 2 1 3.39 4.28 0.67 o 9 2 1 160.39 171.67 2.42 o 10 2 1 3.48 4.68 0.69 o 11 2 1 10.49 11.23 0.80 o -10 3 1 61.82 67.62 4.74 o -9 3 1 13.82 15.09 0.69 o -8 3 1 6.01 6.73 0.46 o -7 3 1 1.71 2.67 0.65 o -6 3 1 16.76 14.44 0.52 o -5 3 1 10.44 10.24 0.87 o -4 3 1 3.64 4.59 0.57 o -3 3 1 1.62 2.01 0.56 o -2 3 1 62.18 56.12 4.01 o -1 3 1 15.87 16.55 0.65 o 0 3 1 8.04 6.93 0.68 o 1 3 1 140.86 135.19 3.56 o 2 3 1 0.07 0.45 0.48 o 3 3 1 130.44 134.20 2.68 o 4 3 1 14.27 15.49 0.71 o 5 3 1 256.95 262.40 7.88 o 6 3 1 56.60 61.97 0.86 o 7 3 1 19.69 21.13 1.31 o 8 3 1 59.12 63.72 2.67 o 9 3 1 30.06 32.96 1.22 o -8 4 1 33.24 30.12 2.28 o -7 4 1 68.65 74.55 2.11 o -6 4 1 12.79 14.06 0.59 o -5 4 1 39.44 40.00 2.04 o -4 4 1 2.15 2.96 0.55 o -3 4 1 0.03 0.50 0.47 o -2 4 1 39.52 39.89 1.00 o -1 4 1 120.50 123.86 2.72 o 0 4 1 10.00 10.47 0.91 o 1 4 1 20.03 20.50 0.62 o 2 4 1 22.58 21.42 1.86 o 3 4 1 19.02 22.36 1.02 o 4 4 1 8.77 9.34 0.59 o 5 4 1 129.00 135.02 2.84 o 6 4 1 1.76 1.32 0.63 o 7 4 1 11.52 10.89 0.74 o -13 0 2 41.17 46.22 4.89 o -12 0 2 48.88 50.63 1.13 o -11 0 2 36.37 37.27 1.26 o -10 0 2 269.35 284.82 2.81 o -9 0 2 1319.83 935.63 4.63 o -8 0 2 135.98 125.27 2.06 o -7 0 2 24.97 27.20 1.55 o -6 0 2 23.74 27.75 1.43 o -5 0 2 0.43 0.55 1.06 o -4 0 2 245.21 255.29 9.42 o -3 0 2 671.61 600.46 11.83 o -2 0 2 3795.73 3766.11 20.58 o -1 0 2 542.93 555.30 8.14 o 0 0 2 1717.52 1738.05 187.08 o 1 0 2 26.91 27.88 1.97 o 2 0 2 651.25 668.43 5.90 o 3 0 2 1104.62 1297.57 7.06 o 4 0 2 338.68 368.08 3.73 o 5 0 2 893.40 992.63 5.55 o 6 0 2 46.62 52.73 1.86 o 7 0 2 0.49 0.42 0.79 o 8 0 2 1.94 1.60 0.74 o 9 0 2 78.73 55.35 0.98 o 10 0 2 118.70 119.82 2.24 o 11 0 2 2.89 1.68 0.71 o -13 1 2 6.25 6.11 0.82 o -12 1 2 3.36 2.35 0.61 o -11 1 2 200.81 197.79 15.99 o -10 1 2 23.64 19.90 1.87 o -9 1 2 429.96 436.80 4.04 o -8 1 2 19.28 20.51 1.01 o -7 1 2 80.32 90.66 1.06 o -6 1 2 360.88 363.12 4.09 o -5 1 2 169.34 164.30 12.29 o -4 1 2 849.55 839.36 16.47 o -3 1 2 847.25 691.53 19.82 o -2 1 2 1116.87 1050.71 64.66 o -1 1 2 4589.23 4401.09 397.08 o 0 1 2 4461.61 4313.70 297.95 o 1 1 2 256.29 247.04 8.50 o 2 1 2 286.83 250.76 6.37 o 3 1 2 53.70 52.16 1.16 o 4 1 2 22.15 20.52 0.85 o 5 1 2 656.50 631.00 21.70 o 6 1 2 61.57 62.88 1.85 o 7 1 2 7.75 5.66 0.55 o 8 1 2 172.57 154.92 6.87 o 9 1 2 2.27 1.82 0.59 o 10 1 2 27.87 22.27 1.05 o 11 1 2 12.97 11.28 0.58 o -12 2 2 2.75 3.81 0.62 o -11 2 2 100.97 98.16 6.87 o -10 2 2 60.90 54.69 4.11 o -9 2 2 1.77 1.61 0.64 o -8 2 2 7.09 8.82 0.73 o -7 2 2 1.53 1.94 0.52 o -6 2 2 407.76 413.77 21.90 o -5 2 2 68.91 71.27 3.99 o -4 2 2 215.35 205.77 5.37 o -3 2 2 27.82 27.97 0.87 o -2 2 2 12.77 12.26 0.75 o -1 2 2 648.08 706.69 16.67 o 0 2 2 110.80 106.42 3.91 o 1 2 2 827.77 816.40 24.38 o 2 2 2 12.67 13.95 0.56 o 3 2 2 9.21 8.62 0.54 o 4 2 2 13.36 10.97 0.64 o 5 2 2 2.21 2.33 0.50 o 6 2 2 10.66 10.57 0.72 o 7 2 2 0.22 0.72 0.68 o 8 2 2 241.28 238.12 7.89 o 9 2 2 22.86 23.40 3.05 o 10 2 2 0.86 1.65 0.81 o -11 3 2 27.18 26.13 1.18 o -10 3 2 5.11 6.88 0.81 o -9 3 2 63.22 63.35 2.18 o -8 3 2 12.04 12.17 1.01 o -7 3 2 0.32 0.01 0.60 o -6 3 2 4.81 4.62 0.59 o -5 3 2 20.12 22.99 0.79 o -4 3 2 52.55 50.77 3.08 o -3 3 2 7.60 5.86 0.52 o -2 3 2 5.17 5.18 0.54 o -1 3 2 257.00 251.10 11.29 o 0 3 2 42.71 40.52 1.74 o 1 3 2 27.10 27.41 0.80 o 2 3 2 134.02 123.93 4.55 o 3 3 2 20.02 20.12 0.86 o 4 3 2 4.49 4.81 0.48 o 5 3 2 252.59 255.05 9.19 o 6 3 2 20.51 21.19 1.06 o 7 3 2 54.07 58.16 1.21 o 8 3 2 190.10 196.79 10.47 o 9 3 2 12.86 13.43 0.78 o -8 4 2 0.49 0.74 0.67 o -7 4 2 15.81 17.59 2.32 o -6 4 2 0.06 0.60 0.53 o -5 4 2 3.63 4.53 0.49 o -4 4 2 37.79 40.57 2.30 o -3 4 2 12.94 12.12 0.54 o -2 4 2 3.82 3.75 0.51 o -1 4 2 0.05 0.43 0.56 o 0 4 2 9.41 7.91 0.63 o 1 4 2 0.09 0.84 0.54 o 2 4 2 1.75 1.36 0.53 o 3 4 2 71.10 72.97 1.04 o 4 4 2 62.43 62.17 2.85 o 5 4 2 114.99 109.27 6.13 o 6 4 2 6.77 7.93 0.74 o -13 1 3 10.57 12.40 0.72 o -12 1 3 0.04 0.08 0.59 o -11 1 3 123.90 132.07 9.72 o -10 1 3 136.67 123.94 12.76 o -9 1 3 177.44 181.76 3.07 o -8 1 3 72.50 67.01 2.05 o -7 1 3 12.65 13.93 0.72 o -6 1 3 442.51 477.57 4.36 o -5 1 3 34.41 33.13 2.01 o -4 1 3 224.99 235.75 12.75 o -3 1 3 166.46 162.52 2.33 o -2 1 3 796.36 816.69 37.41 o -1 1 3 1923.34 1852.84 48.19 o 0 1 3 129.02 119.22 2.55 o 1 1 3 492.63 522.90 10.46 o 2 1 3 102.22 87.92 1.30 o 3 1 3 180.54 185.61 5.43 o 4 1 3 0.53 0.19 0.65 o 5 1 3 76.58 76.99 4.52 o 6 1 3 0.00 0.58 0.66 o 7 1 3 23.48 21.84 1.00 o 8 1 3 30.46 27.36 1.85 o 9 1 3 70.74 63.17 3.34 o 10 1 3 0.29 1.21 0.54 o -13 2 3 17.77 18.64 0.98 o -12 2 3 6.76 7.77 0.90 o -11 2 3 0.73 1.55 0.49 o -10 2 3 1.90 1.61 0.54 o -9 2 3 0.44 0.38 0.57 o -8 2 3 16.26 18.00 0.92 o -7 2 3 69.28 79.10 2.64 o -6 2 3 105.46 96.02 1.15 o -5 2 3 173.02 187.05 3.65 o -4 2 3 11.29 10.07 1.03 o -3 2 3 17.12 12.10 0.76 o -2 2 3 103.85 103.70 2.18 o -1 2 3 168.92 147.44 5.54 o 0 2 3 424.20 394.85 11.07 o 1 2 3 39.73 38.42 0.78 o 2 2 3 7.32 7.47 0.52 o 3 2 3 11.61 10.44 0.52 o 4 2 3 61.57 61.55 2.99 o 5 2 3 3.72 3.40 0.52 o 6 2 3 161.90 165.57 8.44 o 7 2 3 45.55 45.70 3.43 o 8 2 3 10.17 11.46 0.85 o 9 2 3 2.31 3.85 0.80 o 10 2 3 1.17 1.48 0.98 o -11 3 3 20.82 20.03 1.20 o -10 3 3 0.09 0.18 0.62 o -9 3 3 3.41 3.79 0.56 o -8 3 3 30.59 27.18 0.70 o -7 3 3 7.07 7.28 0.59 o -6 3 3 3.10 4.09 0.63 o -5 3 3 49.21 45.00 2.42 o -4 3 3 7.75 6.87 0.53 o -3 3 3 23.25 21.89 1.02 o -2 3 3 45.02 40.52 1.85 o -1 3 3 167.96 161.93 5.03 o 0 3 3 19.76 22.89 0.96 o 1 3 3 2.92 2.98 0.55 o 2 3 3 8.43 8.25 0.50 o 3 3 3 165.10 157.34 8.47 o 4 3 3 252.48 266.76 5.42 o 5 3 3 87.96 86.89 3.01 o 6 3 3 3.25 4.19 0.56 o 7 3 3 17.49 18.28 2.97 o 8 3 3 176.37 165.73 13.45 o -8 4 3 8.51 8.39 1.04 o -7 4 3 0.16 0.56 0.56 o -6 4 3 36.01 38.53 1.75 o -5 4 3 22.17 22.76 1.24 o -4 4 3 122.96 128.83 3.47 o -3 4 3 19.08 21.43 0.79 o -2 4 3 32.60 33.04 1.92 o -1 4 3 6.55 6.14 0.47 o 0 4 3 4.01 4.13 0.58 o 1 4 3 9.93 11.01 0.89 o 2 4 3 8.94 8.80 0.60 o 3 4 3 0.26 1.32 0.56 o 4 4 3 12.47 11.87 1.44 o 5 4 3 13.99 14.29 0.79 o -14 0 4 32.50 33.86 1.90 o -13 0 4 41.91 32.06 9.84 o -12 0 4 131.03 100.17 1.79 o -11 0 4 488.65 518.83 3.73 o -10 0 4 1279.52 1373.01 5.95 o -9 0 4 207.31 207.82 2.73 o -8 0 4 98.87 91.39 1.55 o -7 0 4 266.09 273.99 9.87 o -6 0 4 917.91 1005.71 5.69 o -5 0 4 72.13 87.14 2.60 o -4 0 4 3642.78 3665.93 14.54 o -3 0 4 10.12 6.52 0.94 o -2 0 4 184.34 181.17 5.57 o -1 0 4 846.19 774.58 11.60 o 0 0 4 260.24 309.14 6.22 o 1 0 4 175.05 176.26 2.26 o 2 0 4 125.30 125.98 2.46 o 3 0 4 122.08 121.39 2.23 o 4 0 4 137.39 151.74 2.58 o 5 0 4 176.35 178.81 2.65 o 6 0 4 5.40 4.95 1.59 o 7 0 4 213.20 206.24 9.55 o 8 0 4 156.07 146.16 1.63 o 9 0 4 182.94 163.95 7.84 o 10 0 4 16.76 19.60 0.82 o -14 1 4 5.80 7.49 0.71 o -13 1 4 20.69 24.20 0.84 o -12 1 4 20.49 19.35 1.39 o -11 1 4 26.29 23.56 1.43 o -10 1 4 287.89 285.59 5.66 o -9 1 4 84.88 93.37 2.69 o -8 1 4 41.33 39.11 0.77 o -7 1 4 0.10 0.62 0.54 o -6 1 4 278.83 317.00 3.51 o -5 1 4 79.04 77.13 4.14 o -4 1 4 13.32 14.01 1.79 o -3 1 4 243.30 251.58 7.09 o -2 1 4 257.70 288.13 9.40 o -1 1 4 2.34 4.26 0.67 o 0 1 4 207.10 229.28 7.22 o 1 1 4 155.41 155.94 2.08 o 2 1 4 8.00 11.81 4.29 o 3 1 4 241.62 247.52 8.50 o 4 1 4 6.28 5.76 0.50 o 5 1 4 86.17 89.66 2.04 o 6 1 4 38.94 37.29 1.18 o 7 1 4 25.52 23.27 0.80 o 8 1 4 6.17 5.73 0.56 o 9 1 4 13.38 10.12 0.62 o 10 1 4 18.80 20.01 0.68 o -13 2 4 49.62 49.97 0.98 o -12 2 4 6.11 4.67 0.67 o -11 2 4 3.19 3.44 0.56 o -10 2 4 0.59 0.83 0.59 o -9 2 4 8.50 14.79 3.83 o -8 2 4 14.16 13.39 1.12 o -7 2 4 80.55 72.62 3.56 o -6 2 4 63.05 63.02 2.86 o -5 2 4 11.06 10.39 0.62 o -4 2 4 254.93 244.64 6.04 o -3 2 4 125.17 123.14 8.57 o -2 2 4 27.84 42.63 2.45 o -1 2 4 3140.78 3169.27 66.60 o 0 2 4 31.17 45.45 1.21 o 1 2 4 2.93 5.07 0.52 o 2 2 4 70.19 61.74 2.24 o 3 2 4 150.52 146.92 6.12 o 4 2 4 758.38 721.28 26.46 o 5 2 4 265.72 265.34 13.72 o 6 2 4 45.23 48.42 3.16 o 7 2 4 13.53 12.75 0.68 o 8 2 4 1.35 1.09 0.71 o 9 2 4 2.84 5.85 0.83 o -11 3 4 40.80 42.82 4.19 o -10 3 4 71.75 67.57 5.80 o -9 3 4 0.87 0.86 0.60 o -8 3 4 12.74 11.88 0.59 o -7 3 4 70.58 72.53 2.35 o -6 3 4 31.83 31.43 1.98 o -5 3 4 1.70 1.50 0.66 o -4 3 4 37.89 38.45 1.13 o -3 3 4 25.17 22.26 1.63 o -2 3 4 2.62 2.69 0.60 o -1 3 4 102.38 95.65 4.45 o 0 3 4 0.07 1.09 0.57 o 1 3 4 52.42 55.67 2.21 o 2 3 4 3.04 2.55 0.59 o 3 3 4 19.52 17.48 0.60 o 4 3 4 72.54 76.56 3.13 o 5 3 4 23.51 25.47 0.92 o 6 3 4 33.01 33.19 0.86 o 7 3 4 8.26 7.88 0.76 o -8 4 4 0.04 0.83 0.55 o -7 4 4 0.33 0.45 0.54 o -6 4 4 29.72 31.06 3.14 o -5 4 4 159.95 152.47 11.55 o -4 4 4 86.44 89.12 2.91 o -3 4 4 22.87 24.76 0.70 o -2 4 4 4.49 6.02 0.60 o -1 4 4 0.19 0.42 0.56 o 0 4 4 3.61 8.01 1.11 o 1 4 4 39.26 39.82 1.56 o 2 4 4 73.32 63.77 2.99 o 3 4 4 7.62 8.17 0.62 o 4 4 4 4.00 3.88 0.63 o -14 1 5 14.95 14.57 0.85 o -13 1 5 3.11 4.75 0.90 o -12 1 5 53.74 53.92 5.86 o -11 1 5 32.24 29.43 2.48 o -10 1 5 348.73 367.87 6.25 o -9 1 5 6.37 6.75 0.58 o -8 1 5 17.05 14.95 0.84 o -7 1 5 13.01 14.20 0.91 o -6 1 5 218.19 227.55 9.42 o -5 1 5 20.57 17.96 0.95 o -4 1 5 93.76 75.04 1.82 o -3 1 5 134.95 131.44 4.69 o -2 1 5 100.20 113.99 2.93 o -1 1 5 97.83 126.20 2.51 o 0 1 5 386.31 408.32 8.19 o 1 1 5 44.01 42.51 0.98 o 2 1 5 34.38 29.96 1.42 o 3 1 5 66.01 66.92 3.11 o 4 1 5 233.55 221.13 6.16 o 5 1 5 2.72 1.74 0.62 o 6 1 5 41.21 45.49 1.03 o 7 1 5 47.34 43.63 2.68 o 8 1 5 0.26 0.67 0.55 o 9 1 5 48.57 51.72 1.92 o -13 2 5 4.86 6.84 1.39 o -12 2 5 0.01 0.46 0.57 o -11 2 5 0.14 -0.08 0.69 o -10 2 5 20.99 23.45 0.73 o -9 2 5 13.71 13.25 3.03 o -8 2 5 1.01 0.47 0.82 o -7 2 5 27.72 28.58 1.85 o -6 2 5 11.20 10.92 0.63 o -5 2 5 1.17 0.22 0.69 o -4 2 5 4.58 3.18 0.67 o -3 2 5 415.40 400.22 20.54 o -2 2 5 97.16 100.48 1.60 o -1 2 5 303.95 279.66 4.05 o 0 2 5 1.58 2.47 0.57 o 1 2 5 17.19 17.98 0.67 o 2 2 5 46.00 44.43 1.40 o 3 2 5 43.87 44.44 1.31 o 4 2 5 172.10 165.86 6.30 o 5 2 5 19.72 18.98 0.94 o 6 2 5 6.81 5.91 0.60 o 7 2 5 4.84 5.63 0.77 o 8 2 5 34.94 38.60 2.24 o -11 3 5 13.98 11.18 0.96 o -10 3 5 23.77 21.85 2.17 o -9 3 5 14.30 13.42 1.43 o -8 3 5 5.60 6.80 0.54 o -7 3 5 105.12 116.39 3.22 o -6 3 5 30.46 29.32 1.51 o -5 3 5 464.00 466.97 12.77 o -4 3 5 0.58 2.49 0.71 o -3 3 5 0.00 -0.08 0.77 o -2 3 5 20.27 19.00 0.80 o -1 3 5 424.80 427.27 13.30 o 0 3 5 39.56 36.76 0.81 o 1 3 5 41.94 36.98 1.07 o 2 3 5 7.90 7.18 0.58 o 3 3 5 13.36 13.29 0.73 o 4 3 5 55.91 57.05 2.02 o 5 3 5 12.18 13.29 0.62 o 6 3 5 32.47 32.03 1.04 o -8 4 5 10.82 10.60 1.07 o -7 4 5 0.03 0.83 0.67 o -6 4 5 39.90 38.00 1.76 o -5 4 5 34.90 35.43 0.95 o -4 4 5 24.21 23.77 0.65 o -3 4 5 0.09 0.43 0.66 o -2 4 5 28.57 27.12 1.90 o -1 4 5 6.62 7.71 0.62 o 0 4 5 0.98 0.81 0.67 o 1 4 5 20.16 21.08 1.22 o 2 4 5 9.19 9.71 0.77 o 3 4 5 2.43 3.66 0.61 o -14 0 6 27.44 26.53 9.51 o -13 0 6 43.07 37.17 1.13 o -12 0 6 141.72 116.33 18.75 o -11 0 6 83.99 91.58 2.10 o -10 0 6 0.15 1.05 0.92 o -9 0 6 76.18 77.54 7.97 o -8 0 6 57.96 70.18 1.33 o -7 0 6 199.79 202.01 4.41 o -6 0 6 814.98 926.20 33.88 o -5 0 6 2.37 2.71 1.00 o -4 0 6 10.01 11.09 1.00 o -3 0 6 16.49 16.06 0.97 o -2 0 6 812.30 892.94 20.91 o -1 0 6 65.67 57.99 1.19 o 0 0 6 753.03 800.67 37.75 o 1 0 6 17.55 16.66 0.80 o 2 0 6 1.41 2.73 0.78 o 3 0 6 80.93 84.28 1.36 o 4 0 6 71.99 81.44 1.26 o 5 0 6 74.55 76.99 1.09 o 6 0 6 81.10 87.55 3.41 o 7 0 6 84.86 85.69 2.10 o 8 0 6 9.26 10.67 1.48 o -14 1 6 2.90 2.28 0.72 o -13 1 6 26.92 30.78 2.40 o -12 1 6 227.80 244.84 3.99 o -11 1 6 2.74 2.67 0.64 o -10 1 6 253.87 247.71 9.52 o -9 1 6 0.01 0.40 0.60 o -8 1 6 34.41 31.38 0.81 o -7 1 6 6.92 9.15 0.75 o -6 1 6 163.73 160.74 3.47 o -5 1 6 410.84 400.83 13.93 o -4 1 6 185.94 188.47 3.52 o -3 1 6 1.80 2.29 0.70 o -2 1 6 804.04 828.78 15.80 o -1 1 6 89.09 103.04 1.72 o 0 1 6 4.06 5.77 0.64 o 1 1 6 153.86 137.39 6.86 o 2 1 6 33.41 36.96 0.79 o 3 1 6 104.98 112.71 2.06 o 4 1 6 722.51 733.77 21.84 o 5 1 6 5.92 5.62 0.58 o 6 1 6 4.41 4.06 0.62 o 7 1 6 113.62 96.85 5.21 o 8 1 6 7.98 8.03 0.70 o -13 2 6 9.75 8.85 1.02 o -12 2 6 18.24 16.42 2.29 o -11 2 6 137.71 120.74 16.75 o -10 2 6 383.08 399.87 56.34 o -9 2 6 51.79 43.60 3.96 o -8 2 6 0.49 1.72 0.79 o -7 2 6 1.33 1.20 0.61 o -6 2 6 12.85 14.99 0.85 o -5 2 6 324.68 328.05 6.25 o -4 2 6 23.88 23.74 0.78 o -3 2 6 32.92 37.27 1.22 o -2 2 6 21.51 25.98 0.67 o -1 2 6 30.00 37.14 1.28 o 0 2 6 9.59 7.66 0.55 o 1 2 6 33.52 33.11 1.17 o 2 2 6 236.65 223.41 7.78 o 3 2 6 16.41 15.16 1.10 o 4 2 6 242.30 241.86 7.15 o 5 2 6 2.85 3.28 0.48 o 6 2 6 5.93 6.19 0.59 o 7 2 6 6.54 6.77 0.65 o -11 3 6 14.91 11.87 1.22 o -10 3 6 3.18 2.33 0.66 o -9 3 6 9.93 11.62 0.62 o -8 3 6 40.21 39.25 0.83 o -7 3 6 0.02 0.46 0.56 o -6 3 6 9.39 11.66 0.69 o -5 3 6 348.28 298.72 12.96 o -4 3 6 9.95 10.54 0.73 o -3 3 6 186.98 174.21 9.07 o -2 3 6 173.52 164.44 7.39 o -1 3 6 133.98 131.29 7.00 o 0 3 6 0.00 5.94 0.97 o 1 3 6 71.55 69.12 1.49 o 2 3 6 0.10 0.37 0.51 o 3 3 6 0.04 0.64 0.50 o 4 3 6 77.27 77.16 3.52 o 5 3 6 16.54 17.51 0.76 o -8 4 6 2.58 2.98 0.68 o -7 4 6 113.22 119.15 4.45 o -6 4 6 5.59 6.52 0.62 o -5 4 6 47.84 47.05 1.50 o -4 4 6 2.45 3.26 0.66 o -3 4 6 10.92 10.17 0.61 o -2 4 6 44.45 40.38 2.34 o -1 4 6 115.78 113.32 5.32 o 0 4 6 31.00 30.10 1.56 o 1 4 6 20.47 20.73 1.12 o 2 4 6 3.61 3.61 0.60 o -14 1 7 1.77 2.16 1.00 o -13 1 7 5.05 6.69 0.72 o -12 1 7 80.62 94.42 3.22 o -11 1 7 44.13 37.46 2.66 o -10 1 7 41.75 49.39 2.35 o -9 1 7 70.43 60.78 3.60 o -8 1 7 26.21 28.65 2.30 o -7 1 7 57.39 57.75 2.18 o -6 1 7 17.09 20.50 0.75 o -5 1 7 149.89 151.14 1.60 o -4 1 7 0.00 0.05 0.50 o -3 1 7 44.34 45.12 0.81 o -2 1 7 196.97 211.94 5.42 o -1 1 7 45.01 46.28 0.76 o 0 1 7 25.21 27.79 0.86 o 1 1 7 9.40 9.12 0.68 o 2 1 7 132.44 124.98 2.20 o 3 1 7 168.05 168.60 4.35 o 4 1 7 108.98 111.32 6.29 o 5 1 7 35.71 36.84 1.86 o 6 1 7 1.57 0.80 0.54 o 7 1 7 45.74 50.03 1.44 o -13 2 7 0.26 0.75 0.81 o -12 2 7 77.73 76.86 6.90 o -11 2 7 0.28 0.78 0.60 o -10 2 7 95.71 88.62 14.96 o -9 2 7 3.96 5.22 0.64 o -8 2 7 3.57 3.06 0.72 o -7 2 7 26.71 25.40 0.78 o -6 2 7 101.75 103.33 1.95 o -5 2 7 107.80 108.11 4.29 o -4 2 7 91.99 91.40 1.96 o -3 2 7 38.98 41.38 0.69 o -2 2 7 3.60 2.64 0.58 o -1 2 7 11.90 12.00 0.61 o 0 2 7 17.56 15.24 0.69 o 1 2 7 26.61 23.67 0.52 o 2 2 7 0.05 0.94 0.53 o 3 2 7 22.05 20.78 1.05 o 4 2 7 6.62 6.45 0.57 o 5 2 7 0.45 1.20 0.78 o 6 2 7 20.11 21.13 0.63 o -11 3 7 62.41 60.69 3.36 o -10 3 7 11.76 12.91 0.87 o -9 3 7 5.95 5.97 0.58 o -8 3 7 0.27 0.35 0.69 o -7 3 7 162.48 170.02 1.26 o -6 3 7 16.00 15.88 0.88 o -5 3 7 107.54 115.13 1.20 o -4 3 7 4.21 4.89 0.72 o -3 3 7 175.85 163.77 7.90 o -2 3 7 125.35 123.92 1.89 o -1 3 7 118.79 106.77 2.94 o 0 3 7 88.50 87.11 1.98 o 1 3 7 1.30 0.98 0.49 o 2 3 7 29.10 29.67 1.03 o 3 3 7 11.94 10.08 0.51 o 4 3 7 8.58 8.64 0.81 o -7 4 7 8.52 9.81 0.72 o -6 4 7 32.37 29.78 1.05 o -5 4 7 0.09 0.19 0.52 o -4 4 7 3.00 2.68 0.71 o -3 4 7 9.44 9.22 0.66 o -2 4 7 82.20 70.02 1.78 o -1 4 7 3.00 3.88 0.56 o 0 4 7 32.61 30.16 1.70 o -14 0 8 80.84 95.51 2.35 o -13 0 8 3.03 1.32 1.50 o -12 0 8 9.87 9.43 1.96 o -11 0 8 1.09 1.44 1.15 o -10 0 8 6.10 3.21 0.82 o -9 0 8 50.44 42.98 1.34 o -7 0 8 14.14 14.09 1.95 o -6 0 8 0.00 0.16 0.83 o -5 0 8 105.50 114.84 1.68 o -4 0 8 24.26 25.38 0.94 o -3 0 8 247.75 237.07 29.81 o -2 0 8 845.01 922.19 10.82 o -1 0 8 213.70 203.67 15.73 o 0 0 8 59.25 65.23 2.09 o 1 0 8 2.82 2.81 0.84 o 2 0 8 218.23 225.15 6.85 o 3 0 8 1203.62 1289.68 12.31 o 4 0 8 275.09 301.31 8.52 o 5 0 8 141.13 142.79 1.55 o 6 0 8 7.71 9.42 0.77 o -14 1 8 23.80 27.28 1.35 o -13 1 8 7.03 8.30 1.02 o -12 1 8 58.01 56.87 2.68 o -11 1 8 110.85 94.55 2.41 o -10 1 8 5.46 7.66 0.80 o -9 1 8 4.31 3.42 0.64 o -8 1 8 0.15 0.03 0.61 o -7 1 8 76.30 74.68 4.32 o -6 1 8 276.97 265.72 19.91 o -5 1 8 131.16 124.05 5.96 o -4 1 8 28.56 27.75 0.92 o -3 1 8 0.01 0.68 0.56 o -2 1 8 77.56 74.05 2.34 o -1 1 8 10.68 14.72 0.67 o 0 1 8 19.65 20.18 0.71 o 1 1 8 42.13 40.33 1.94 o 2 1 8 77.93 74.90 2.01 o 3 1 8 5.75 4.57 0.57 o 4 1 8 17.11 16.26 0.89 o 5 1 8 11.22 12.35 0.62 o 6 1 8 43.16 41.84 0.91 o -13 2 8 31.57 25.17 3.22 o -12 2 8 64.87 62.14 7.03 o -11 2 8 260.08 276.22 6.15 o -10 2 8 1.26 1.32 0.77 o -9 2 8 0.74 0.94 0.69 o -8 2 8 28.18 28.54 0.89 o -7 2 8 437.98 403.77 12.91 o -6 2 8 129.56 121.16 4.62 o -5 2 8 570.15 578.60 9.52 o -4 2 8 15.99 14.67 0.81 o -3 2 8 18.73 16.49 0.56 o -2 2 8 0.51 1.41 0.49 o -1 2 8 8.46 10.02 0.53 o 0 2 8 111.07 103.69 3.87 o 1 2 8 15.94 14.21 0.58 o 2 2 8 9.21 9.23 0.52 o 3 2 8 28.39 29.28 0.66 o 4 2 8 36.32 36.46 1.00 o 5 2 8 0.29 0.64 0.57 o -11 3 8 79.25 83.58 1.74 o -10 3 8 35.13 35.81 0.87 o -9 3 8 2.48 1.89 0.58 o -8 3 8 7.15 9.08 0.58 o -7 3 8 44.40 46.18 2.43 o -6 3 8 0.54 0.79 0.56 o -5 3 8 0.09 -0.05 0.62 o -4 3 8 36.23 33.17 0.89 o -3 3 8 5.44 6.14 0.59 o -2 3 8 2.00 2.21 0.53 o -1 3 8 12.94 11.67 0.61 o 0 3 8 19.17 16.69 0.72 o 1 3 8 7.06 6.75 0.57 o 2 3 8 36.01 35.34 0.68 o 3 3 8 7.83 7.74 0.56 o -6 4 8 0.62 0.71 0.81 o -5 4 8 19.85 21.98 0.79 o -4 4 8 7.12 8.89 0.75 o -3 4 8 11.51 11.35 1.37 o -2 4 8 136.99 117.85 1.25 o -14 1 9 4.33 6.26 0.93 o -13 1 9 5.93 6.25 0.78 o -12 1 9 7.48 5.41 0.71 o -11 1 9 48.09 41.77 2.90 o -10 1 9 44.05 40.30 1.61 o -9 1 9 5.38 6.50 0.71 o -8 1 9 1.01 0.75 0.63 o -7 1 9 83.79 86.44 1.90 o -6 1 9 242.73 202.09 14.99 o -5 1 9 24.00 24.36 0.62 o -4 1 9 9.45 10.13 0.54 o -3 1 9 55.24 58.07 0.82 o -2 1 9 101.28 93.62 7.83 o -1 1 9 96.28 94.11 2.19 o 0 1 9 2.68 2.66 0.55 o 1 1 9 36.46 34.29 1.89 o 2 1 9 8.34 9.08 0.74 o 3 1 9 207.14 218.87 1.62 o 4 1 9 0.02 0.12 0.65 o 5 1 9 6.70 7.76 0.73 o -13 2 9 29.39 39.39 1.81 o -12 2 9 51.35 46.03 4.59 o -11 2 9 8.34 10.79 0.81 o -10 2 9 5.79 7.15 0.74 o -9 2 9 3.33 2.89 0.70 o -8 2 9 33.50 37.29 1.09 o -7 2 9 0.20 0.69 0.68 o -6 2 9 117.60 124.08 1.26 o -5 2 9 0.14 0.69 0.71 o -4 2 9 0.01 0.05 0.48 o -3 2 9 33.98 33.72 0.97 o -2 2 9 41.45 35.85 0.84 o -1 2 9 16.34 13.84 0.54 o 0 2 9 43.44 38.87 0.74 o 1 2 9 4.56 4.71 0.53 o 2 2 9 3.91 3.99 0.57 o 3 2 9 4.51 4.72 0.55 o 4 2 9 0.40 1.54 0.59 o -10 3 9 0.96 1.68 0.71 o -9 3 9 39.52 44.04 0.91 o -8 3 9 0.80 1.83 0.65 o -7 3 9 57.34 54.32 1.80 o -6 3 9 0.00 1.55 0.74 o -5 3 9 5.25 4.84 0.65 o -4 3 9 4.58 3.82 0.60 o -3 3 9 7.30 8.17 0.73 o -2 3 9 9.50 6.80 0.52 o -1 3 9 1.39 1.12 0.56 o 0 3 9 8.57 9.61 0.69 o 1 3 9 2.05 3.91 0.50 o -14 0 10 4.45 1.09 1.26 o -13 0 10 5.46 4.84 1.70 o -12 0 10 154.09 142.15 5.18 o -11 0 10 152.67 149.96 7.87 o -10 0 10 51.23 53.66 1.45 o -9 0 10 7.46 7.79 2.86 o -8 0 10 3.54 3.69 1.09 o -7 0 10 25.82 24.63 1.33 o -6 0 10 766.74 672.71 111.41 o -5 0 10 17.78 17.44 3.94 o -4 0 10 59.65 60.18 1.13 o -3 0 10 15.65 16.35 0.90 o -2 0 10 3.10 1.88 0.73 o -1 0 10 18.07 16.03 1.79 o 0 0 10 1.49 3.49 0.87 o 1 0 10 280.76 286.80 6.98 o 2 0 10 2.33 2.42 0.73 o 3 0 10 223.23 232.52 8.51 o 4 0 10 1.57 2.43 0.72 o -13 1 10 16.95 13.36 1.42 o -12 1 10 15.76 13.84 1.74 o -11 1 10 1.96 1.19 0.81 o -10 1 10 1.71 2.61 0.69 o -9 1 10 45.99 44.07 0.98 o -8 1 10 111.16 107.95 4.15 o -7 1 10 49.46 46.70 3.81 o -6 1 10 418.68 408.71 11.55 o -5 1 10 8.27 9.33 0.58 o -4 1 10 6.61 7.36 0.65 o -3 1 10 168.55 178.44 3.08 o -2 1 10 14.87 12.96 0.59 o -1 1 10 0.60 1.28 0.53 o 0 1 10 144.39 146.63 1.16 o 1 1 10 28.84 29.95 0.90 o 2 1 10 21.11 22.67 0.66 o 3 1 10 280.83 284.76 7.70 o -12 2 10 9.17 9.12 0.83 o -11 2 10 0.01 0.77 0.78 o -10 2 10 25.24 25.84 1.33 o -9 2 10 1.94 1.90 0.77 o -8 2 10 61.23 67.58 3.28 o -7 2 10 142.56 145.14 2.88 o -6 2 10 2.04 1.89 0.64 o -5 2 10 2.35 2.11 0.55 o -4 2 10 5.56 5.09 0.57 o -3 2 10 51.04 52.32 0.73 o -2 2 10 81.98 71.84 2.73 o -1 2 10 26.51 24.71 1.28 o 0 2 10 0.93 1.25 0.54 o 1 2 10 0.76 1.86 0.56 o 2 2 10 25.31 24.95 0.85 o -9 3 10 41.32 45.87 1.42 o -8 3 10 0.77 0.59 0.65 o -7 3 10 29.07 29.91 0.82 o -6 3 10 26.02 25.01 1.02 o -5 3 10 34.65 34.02 0.83 o -4 3 10 1.88 2.94 0.82 o -3 3 10 0.56 0.96 0.61 o -2 3 10 6.23 4.54 0.61 o -1 3 10 26.49 23.34 1.54 o -13 1 11 1.03 1.03 0.83 o -12 1 11 52.42 45.27 6.14 o -11 1 11 0.02 0.42 0.70 o -10 1 11 20.75 19.88 1.71 o -9 1 11 6.37 5.37 0.67 o -8 1 11 109.86 108.81 8.86 o -7 1 11 11.97 12.06 0.74 o -6 1 11 182.96 172.11 13.12 o -5 1 11 2.76 2.74 0.59 o -4 1 11 1.22 1.09 0.59 o -3 1 11 58.53 56.68 1.74 o -2 1 11 13.42 11.14 0.68 o -1 1 11 22.95 22.78 0.76 o 0 1 11 6.27 5.26 0.56 o 1 1 11 83.13 83.17 1.56 o 2 1 11 21.85 23.18 0.95 o -11 2 11 15.96 22.16 0.87 o -10 2 11 2.04 2.66 0.85 o -9 2 11 23.70 26.56 0.89 o -8 2 11 5.30 6.39 0.84 o -7 2 11 1.45 1.10 0.68 o -6 2 11 0.86 1.82 0.65 o -5 2 11 8.49 7.29 0.60 o -4 2 11 2.42 2.14 0.50 o -3 2 11 46.15 45.89 1.91 o -2 2 11 28.86 21.70 0.71 o -1 2 11 23.21 24.09 0.84 o 0 2 11 1.67 2.90 0.64 o -7 3 11 13.90 13.98 0.87 o -6 3 11 6.98 7.29 1.17 o -5 3 11 2.47 6.37 1.31 o -4 3 11 10.80 10.72 0.69 o -12 0 12 106.57 92.09 15.09 o -11 0 12 42.39 40.69 13.88 o -10 0 12 6.18 5.26 1.20 o -9 0 12 3.25 2.78 0.93 o -8 0 12 589.45 605.65 27.76 o -7 0 12 203.59 165.95 42.01 o -6 0 12 459.92 474.42 4.45 o -5 0 12 39.74 42.08 1.06 o -4 0 12 23.38 26.72 1.21 o -3 0 12 28.60 29.48 1.05 o -2 0 12 21.83 23.06 0.90 o -1 0 12 137.30 143.27 10.55 o 0 0 12 37.53 40.85 1.23 o 1 0 12 4.51 4.94 1.28 o -12 1 12 43.06 40.59 2.61 o -11 1 12 1.19 1.27 0.82 o -10 1 12 0.12 -0.34 0.81 o -9 1 12 9.79 10.90 1.61 o -8 1 12 26.13 26.61 1.33 o -7 1 12 68.60 69.57 2.06 o -6 1 12 53.35 58.11 1.44 o -5 1 12 0.47 0.29 0.55 o -4 1 12 24.39 23.19 0.66 o -3 1 12 13.45 12.97 0.59 o -2 1 12 49.86 46.38 1.99 o -1 1 12 1.99 1.56 0.56 o 0 1 12 2.91 3.07 0.52 o -10 2 12 35.54 32.79 1.00 o -9 2 12 2.68 2.90 0.76 o -8 2 12 6.15 5.96 0.76 o -7 2 12 0.02 0.48 0.63 o -6 2 12 11.69 12.19 0.63 o -5 2 12 1.52 2.15 0.47 o -4 2 12 14.39 15.88 0.67 o -3 2 12 31.20 29.21 0.83 o -2 2 12 8.22 8.09 0.67 o -10 1 13 3.97 3.75 0.81 o -9 1 13 15.45 17.29 1.99 o -8 1 13 71.20 75.06 3.09 o -7 1 13 83.29 78.24 4.74 o -6 1 13 12.75 13.31 1.16 o -5 1 13 14.13 15.00 0.67 o -4 1 13 1.29 1.76 0.57 o -3 1 13 19.67 19.50 0.66 o -2 1 13 3.06 3.29 0.73 o -9 0 14 73.83 72.10 2.52 o -8 0 14 80.61 80.59 2.45 o -7 0 14 7.79 7.62 1.01 o -6 0 14 11.62 12.12 0.96 o -5 0 14 6.82 6.70 0.88 o