Crystallography Open Database

Information card for entry 2020604

2020603 << 2020604 >> 2020605

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Structure parameters

Chemical name	<i>catena</i>-Poly[[silver(I)-(μ-5-{[tris(pyrazol-1-yl)methoxy]methyl-κ^2^<i>N</i>,<i>N</i>'}-2,2'-bipyridine-κ^2^<i>N</i>,<i>N</i>')] diethyl ether hemisolvate]
Formula	C24 H25 Ag B F4 N8 O1.5
Calculated formula	C24 H25 Ag B F4 N8 O1.5
Title of publication	Silver(I) and rhenium(I) metal complexes of a 2,2'-bipyridine-functionalized third-generation tris(pyrazolyl)methane ligand
Authors of publication	Semeniuc, Radu F.; Reger, Daniel L.; Smith, Mark D.
Journal of publication	Acta Crystallographica Section C
Year of publication	2016
Journal volume	72
Journal issue	11
Pages of publication	826 - 831
a	20.4544 ± 0.0006 Å
b	11.9881 ± 0.0004 Å
c	21.4952 ± 0.0007 Å
α	90°
β	93.493 ± 0.001°
γ	90°
Cell volume	5261 ± 0.3 Å³
Cell temperature	150 ± 2 K
Ambient diffraction temperature	150 ± 2 K
Number of distinct elements	7
Space group number	15
Hermann-Mauguin space group symbol	C 1 2/c 1
Hall space group symbol	-C 2yc
Residual factor for all reflections	0.0596
Residual factor for significantly intense reflections	0.048
Weighted residual factors for significantly intense reflections	0.1209
Weighted residual factors for all reflections included in the refinement	0.1296
Goodness-of-fit parameter for all reflections included in the refinement	1.043
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	Yes

Version history

Revision	Date	Message	Files
188940 (current)	2016-12-06	cif/ Updating files of 2020604, 2020605 Original log message: Adding full bibliography for 2020604--2020605.cif.	2020604.cif 2020604.hkl
186992	2016-10-07	cif/ hkl/ Adding structures of 2020604, 2020605 via cif-deposit CGI script.	2020604.cif 2020604.hkl