#------------------------------------------------------------------------------ #$Date: 2016-10-07 04:53:11 +0300 (Fri, 07 Oct 2016) $ #$Revision: 186993 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/02/06/2020606.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2020606 _cell_angle_alpha 77.203 _cell_angle_beta 80.890 _cell_angle_gamma 89.522 _cell_length_a 13.1754 _cell_length_b 13.6724 _cell_length_c 19.5709 _exptl_crystal_F_000 1400.00 _reflns_d_resolution_high 0.7500 _cod_data_source_file yp3119Ix2CH3CNsup2.hkl _cod_data_source_block Ix2CH3CN _shelx_title ' 10mz370_0m in P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 223.41 _shelx_f_squared_multiplier 1.000 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 11122.08 9033.04 360.52 o 3 0 0 194.98 183.02 22.79 o 4 0 0 492.24 568.30 47.99 o 5 0 0 2836.16 2869.94 142.81 o 6 0 0 698.37 716.63 85.89 o 7 0 0 9833.61 9455.66 377.89 o 8 0 0 540.11 586.17 50.95 o 9 0 0 212.73 202.40 48.29 o 10 0 0 1029.69 1193.41 130.21 o 11 0 0 278.65 283.42 106.92 o 12 0 0 1026.06 1031.32 138.40 o 13 0 0 0.02 -10.04 36.95 o 14 0 0 64.20 -20.58 43.57 o 15 0 0 227.47 197.58 52.16 o 16 0 0 624.32 506.20 68.62 o 17 0 0 71.92 -46.94 64.30 o -17 1 0 8.37 -63.75 63.75 o -16 1 0 505.03 352.09 65.01 o -15 1 0 296.54 198.74 51.91 o -14 1 0 6.24 14.01 41.21 o -13 1 0 898.84 869.18 135.03 o -12 1 0 926.71 745.19 123.99 o -11 1 0 261.44 446.46 72.39 o -10 1 0 391.40 489.33 57.58 o -9 1 0 88.91 52.26 47.34 o -8 1 0 5864.92 5929.32 243.51 o -7 1 0 375.56 449.88 44.58 o -6 1 0 5979.54 6663.02 270.72 o -5 1 0 204.95 271.97 33.63 o -4 1 0 5807.87 5818.03 234.93 o -3 1 0 31839.57 32592.16 1299.08 o -2 1 0 7060.25 6937.10 277.70 o -1 1 0 34847.22 34354.27 1369.61 o 0 1 0 1331.71 1045.53 53.61 o 1 1 0 49912.74 50198.26 2528.04 o 2 1 0 2321.02 2072.29 144.47 o 3 1 0 9562.62 9625.53 451.28 o 4 1 0 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