#------------------------------------------------------------------------------ #$Date: 2017-01-17 03:49:32 +0200 (Tue, 17 Jan 2017) $ #$Revision: 190567 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/02/07/2020707.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2020707 _cell_angle_alpha 90.000 _cell_angle_beta 108.597 _cell_angle_gamma 90.000 _cell_length_a 13.2762 _cell_length_b 12.6138 _cell_length_c 10.1742 _exptl_crystal_F_000 696.00 _reflns_d_resolution_high 0.8172 _cod_data_source_file fn3226H2sup3.hkl _cod_data_source_block H2 _shelx_title ' twin4a in P2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 186.47 _shelx_f_squared_multiplier 1.000 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 4527.61 3706.75 134.69 o 2 0 0 336.80 248.16 7.73 o 3 0 0 21095.82 19734.17 610.97 o 4 0 0 545.77 568.96 17.69 o 5 0 0 2072.60 2040.67 74.15 o 6 0 0 0.64 -0.04 0.17 o 7 0 0 11.26 12.88 0.47 o 8 0 0 1.92 1.28 0.31 o 9 0 0 376.59 401.74 11.33 o 10 0 0 615.65 624.03 17.52 o 11 0 0 16.19 19.09 0.53 o 12 0 0 250.96 264.26 4.79 o 13 0 0 110.71 112.67 2.73 o 14 0 0 5.22 3.81 0.31 o 15 0 0 285.77 277.26 7.25 o 1 1 0 6773.58 5018.98 296.81 o 2 1 0 11.35 8.62 0.30 o 3 1 0 11290.23 11523.11 271.95 o 4 1 0 2816.49 2703.94 63.85 o 5 1 0 67.02 87.05 2.19 o 6 1 0 144.89 156.16 2.51 o 7 1 0 1.89 0.95 0.18 o 8 1 0 48.25 44.12 0.86 o 9 1 0 128.32 124.37 2.44 o 10 1 0 55.08 65.90 1.48 o 11 1 0 212.90 212.80 2.84 o 12 1 0 28.28 30.40 0.53 o 13 1 0 33.84 38.44 0.81 o 14 1 0 142.69 147.11 2.61 o 15 1 0 9.34 8.70 0.28 o 0 2 0 14171.14 13036.44 404.79 o 1 2 0 2044.39 1991.47 47.74 o 2 2 0 23.49 15.90 0.46 o 3 2 0 657.29 692.15 16.35 o 4 2 0 159.35 128.38 3.14 o 5 2 0 158.01 150.35 4.13 o 6 2 0 533.12 533.70 8.81 o 7 2 0 648.08 764.17 11.97 o 8 2 0 491.69 504.21 7.95 o 9 2 0 462.75 501.90 9.98 o 10 2 0 10.29 11.28 0.46 o 11 2 0 45.90 50.24 0.80 o 12 2 0 62.52 65.88 1.00 o 13 2 0 11.00 12.66 0.42 o 14 2 0 0.62 0.75 0.17 o 15 2 0 180.44 173.68 3.02 o 1 3 0 1357.20 1443.70 34.61 o 2 3 0 27.21 20.35 0.68 o 3 3 0 88.33 108.60 2.99 o 4 3 0 828.70 854.19 22.51 o 5 3 0 531.35 572.81 10.93 o 6 3 0 234.51 242.62 3.99 o 7 3 0 19.31 20.25 0.49 o 8 3 0 150.54 169.55 2.92 o 9 3 0 35.85 39.24 0.96 o 10 3 0 74.51 78.66 1.39 o 11 3 0 3.15 4.98 0.22 o 12 3 0 9.87 10.20 0.29 o 13 3 0 2.85 4.15 0.24 o 14 3 0 2.13 1.17 0.17 o 15 3 0 13.53 11.24 0.40 o 0 4 0 5621.82 5725.10 177.10 o 1 4 0 1295.00 1391.90 33.39 o 2 4 0 11.44 8.33 0.38 o 3 4 0 2060.87 1996.51 60.06 o 4 4 0 1202.17 1245.49 21.25 o 5 4 0 516.97 555.71 8.96 o 6 4 0 153.97 162.56 2.59 o 7 4 0 593.44 607.55 11.02 o 8 4 0 704.92 769.00 13.65 o 9 4 0 17.57 18.26 0.58 o 10 4 0 227.86 228.58 2.96 o 11 4 0 7.46 7.05 0.23 o 12 4 0 65.47 71.16 1.35 o 13 4 0 71.52 73.71 1.37 o 14 4 0 27.16 28.68 0.61 o 1 5 0 2513.83 2485.58 59.57 o 2 5 0 5221.55 5394.72 129.24 o 3 5 0 906.61 949.65 16.82 o 4 5 0 19.22 28.02 0.55 o 5 5 0 152.59 174.83 3.08 o 6 5 0 132.62 144.58 2.33 o 7 5 0 147.02 136.66 2.36 o 8 5 0 11.23 12.91 0.46 o 9 5 0 3.16 3.10 0.27 o 10 5 0 34.97 34.39 0.59 o 11 5 0 60.28 65.39 1.05 o 12 5 0 14.15 13.91 0.43 o 13 5 0 24.83 27.20 0.64 o 14 5 0 62.05 59.36 1.18 o 0 6 0 2499.40 2792.38 75.66 o 1 6 0 41.24 50.01 1.01 o 2 6 0 333.12 296.65 4.88 o 3 6 0 457.31 463.46 7.34 o 4 6 0 1.57 1.41 0.15 o 5 6 0 135.02 141.63 2.34 o 6 6 0 568.35 579.14 9.43 o 7 6 0 319.45 340.69 7.81 o 8 6 0 101.00 105.23 2.36 o 9 6 0 172.68 176.62 2.48 o 10 6 0 0.30 0.11 0.16 o 11 6 0 81.57 78.49 1.29 o 12 6 0 12.06 15.35 0.44 o 13 6 0 2.73 2.86 0.20 o 14 6 0 0.48 0.37 0.19 o 1 7 0 9.40 8.11 0.28 o 2 7 0 44.10 42.46 0.85 o 3 7 0 7.09 13.41 0.42 o 4 7 0 22.76 22.52 0.57 o 5 7 0 505.18 497.53 8.39 o 6 7 0 3.22 3.16 0.32 o 7 7 0 252.36 270.93 6.27 o 8 7 0 165.00 142.67 2.61 o 9 7 0 893.23 896.40 12.59 o 10 7 0 4.48 3.91 0.21 o 11 7 0 14.32 13.70 0.43 o 12 7 0 101.92 91.82 1.73 o 13 7 0 2.23 2.24 0.19 o 0 8 0 112.52 156.51 4.84 o 1 8 0 0.90 0.28 0.17 o 2 8 0 385.64 408.14 7.05 o 3 8 0 3.69 4.84 0.28 o 4 8 0 670.06 645.13 11.39 o 5 8 0 0.02 -0.06 0.22 o 6 8 0 1125.74 1185.08 29.50 o 7 8 0 30.03 27.11 0.55 o 8 8 0 251.79 228.04 3.67 o 9 8 0 934.41 914.87 13.42 o 10 8 0 87.61 97.75 2.01 o 11 8 0 0.38 0.26 0.18 o 12 8 0 22.35 19.91 0.51 o 13 8 0 10.61 10.77 0.52 o 1 9 0 509.04 445.02 11.26 o 2 9 0 31.25 31.79 0.93 o 3 9 0 683.21 668.26 16.10 o 4 9 0 29.79 28.34 1.10 o 5 9 0 500.35 479.65 11.63 o 6 9 0 426.16 440.75 6.61 o 7 9 0 6.42 4.73 0.24 o 8 9 0 127.97 112.97 1.81 o 9 9 0 27.60 26.19 0.68 o 10 9 0 7.09 8.00 0.33 o 11 9 0 8.15 9.61 0.36 o 12 9 0 38.31 31.29 0.87 o 1 10 0 6.88 8.49 0.55 o 2 10 0 109.59 90.55 2.75 o 3 10 0 0.95 1.16 0.27 o 4 10 0 1.23 1.83 0.17 o 5 10 0 384.36 372.03 5.89 o 6 10 0 462.00 461.32 7.71 o 7 10 0 131.53 129.16 2.16 o 8 10 0 181.41 173.17 3.63 o 9 10 0 101.44 92.20 1.81 o 10 10 0 1.03 1.41 0.21 o 11 10 0 1.28 0.91 0.20 o 1 11 0 7.28 3.55 0.21 o 2 11 0 30.45 33.53 0.69 o 3 11 0 6.96 10.37 0.38 o 4 11 0 31.75 27.07 0.57 o 5 11 0 181.98 183.65 2.79 o 6 11 0 49.68 54.89 0.99 o 7 11 0 76.77 73.96 1.50 o 8 11 0 145.72 143.77 3.03 o 9 11 0 28.58 28.21 0.81 o 10 11 0 6.21 5.09 0.29 o 0 12 0 15.87 15.91 0.62 o 1 12 0 263.39 236.88 3.94 o 2 12 0 0.85 0.22 0.16 o 3 12 0 6.91 7.13 0.27 o 4 12 0 363.58 363.15 7.36 o 5 12 0 0.01 0.31 0.19 o 6 12 0 150.77 151.21 3.57 o 7 12 0 174.34 145.38 3.28 o 8 12 0 199.99 194.37 4.51 o 9 12 0 101.29 95.05 2.61 o 1 13 0 20.41 15.18 0.48 o 2 13 0 39.62 41.60 0.92 o 3 13 0 3.75 5.17 0.29 o 4 13 0 2.65 2.55 0.25 o 5 13 0 133.20 146.66 3.43 o 6 13 0 64.15 60.20 1.86 o 7 13 0 204.83 192.35 4.45 o 8 13 0 56.53 56.65 3.83 o 0 14 0 0.83 0.40 0.30 o 1 14 0 68.60 60.73 1.71 o 2 14 0 1.38 0.61 0.19 o 3 14 0 40.42 40.85 1.12 o 4 14 0 3.50 5.22 0.32 o 5 14 0 36.38 34.30 1.10 o 6 14 0 104.50 100.88 6.68 o 1 15 0 5.87 6.69 0.63 o 2 15 0 0.12 -0.20 0.31 o -15 1 1 30.77 35.74 0.82 o -14 1 1 1.89 2.88 0.48 o -13 1 1 47.82 47.78 1.02 o -12 1 1 21.46 20.85 0.51 o -11 1 1 126.93 132.01 2.10 o -10 1 1 251.33 273.57 6.86 o -9 1 1 184.03 189.75 3.66 o -8 1 1 1300.35 1456.34 25.37 o -7 1 1 72.67 67.43 1.39 o -6 1 1 439.89 525.17 15.52 o -5 1 1 1507.92 859.06 46.23 o -4 1 1 1284.40 1369.33 51.97 o -3 1 1 713.51 890.39 47.82 o -2 1 1 503.31 559.59 12.26 o -1 1 1 1521.91 1406.27 33.09 o 0 1 1 1425.21 1354.50 31.88 o 1 1 1 573.80 579.25 12.68 o 2 1 1 1128.76 1253.34 27.41 o 3 1 1 376.43 373.36 9.67 o 4 1 1 193.31 173.21 5.39 o 5 1 1 383.18 349.94 9.09 o 6 1 1 112.33 97.94 2.37 o 7 1 1 821.87 834.09 18.56 o 8 1 1 127.93 122.59 3.75 o 9 1 1 350.80 378.70 9.19 o 10 1 1 157.84 171.38 3.23 o 11 1 1 22.30 22.84 0.52 o 12 1 1 55.15 56.63 1.17 o 13 1 1 1.19 2.06 0.44 o 14 1 1 21.95 25.47 0.66 o -15 2 1 54.24 48.17 1.02 o -14 2 1 159.35 182.77 3.47 o -13 2 1 43.88 45.30 0.99 o -12 2 1 9.83 7.58 0.42 o -11 2 1 266.05 282.67 3.89 o -10 2 1 294.62 333.67 6.72 o -9 2 1 747.01 797.97 13.97 o -8 2 1 335.91 378.45 7.21 o -7 2 1 3119.93 3570.52 72.77 o -6 2 1 520.58 545.44 20.57 o -5 2 1 1491.75 1616.14 61.32 o -4 2 1 1905.27 1893.23 41.42 o -3 2 1 5777.26 6757.93 362.15 o -2 2 1 4467.15 4457.32 114.38 o -1 2 1 855.70 802.00 17.56 o 0 2 1 22.91 22.72 0.60 o 1 2 1 1354.64 1488.87 36.31 o 2 2 1 4.23 4.50 0.21 o 3 2 1 1463.70 967.31 52.00 o 4 2 1 1086.35 925.83 35.18 o 5 2 1 675.89 663.40 24.50 o 6 2 1 1967.76 1990.36 40.61 o 7 2 1 529.84 587.25 12.89 o 8 2 1 963.54 1033.62 22.58 o 9 2 1 190.41 209.68 4.65 o 10 2 1 416.05 458.27 6.44 o 11 2 1 7.28 5.35 0.38 o 12 2 1 40.37 42.79 0.95 o 13 2 1 107.30 124.82 2.26 o 14 2 1 34.44 31.45 0.80 o -15 3 1 31.02 32.39 0.92 o -14 3 1 0.42 -0.21 0.42 o -13 3 1 24.14 22.56 0.64 o -12 3 1 50.77 52.06 0.90 o -11 3 1 7.97 6.64 0.39 o -10 3 1 252.03 256.94 5.23 o -9 3 1 60.62 63.22 1.46 o -8 3 1 981.33 1088.26 24.14 o -7 3 1 664.58 728.40 17.30 o -6 3 1 2699.75 3103.26 99.76 o -5 3 1 712.87 587.05 31.89 o -4 3 1 1993.86 2182.37 117.12 o -3 3 1 628.63 700.47 37.77 o -2 3 1 212.93 199.20 4.86 o -1 3 1 34.53 27.98 0.75 o 0 3 1 39.63 44.41 1.05 o 1 3 1 66.21 63.75 1.47 o 2 3 1 128.67 138.70 3.11 o 3 3 1 1273.98 1233.37 66.31 o 4 3 1 793.92 763.60 41.25 o 5 3 1 2321.65 2200.01 69.77 o 6 3 1 647.55 647.75 17.70 o 7 3 1 1024.94 1082.38 19.31 o 8 3 1 38.26 39.34 1.21 o 9 3 1 373.15 397.97 9.57 o 10 3 1 6.74 5.64 0.37 o 11 3 1 49.38 50.86 0.85 o 12 3 1 34.71 35.74 0.84 o 13 3 1 0.27 -0.43 0.43 o 14 3 1 20.46 20.75 0.60 o -15 4 1 72.59 76.53 2.57 o -14 4 1 64.90 72.09 1.79 o -13 4 1 22.76 24.94 0.69 o -12 4 1 84.12 89.45 1.41 o -11 4 1 67.37 63.58 1.06 o -10 4 1 108.31 110.66 2.96 o -9 4 1 194.33 200.98 5.06 o -8 4 1 818.93 847.48 16.41 o -7 4 1 201.42 219.48 6.16 o -6 4 1 246.99 261.18 7.26 o -5 4 1 1406.96 1295.58 53.03 o -4 4 1 66.54 88.39 5.33 o -3 4 1 833.06 971.14 52.26 o -2 4 1 99.58 93.67 2.59 o -1 4 1 433.47 457.52 11.05 o 0 4 1 478.94 424.17 22.87 o 1 4 1 1039.20 921.73 49.54 o 2 4 1 816.19 849.28 22.37 o 3 4 1 98.46 124.70 7.19 o 4 4 1 978.74 920.39 29.01 o 5 4 1 323.11 311.76 12.43 o 6 4 1 254.43 260.61 6.25 o 7 4 1 631.62 644.38 11.56 o 8 4 1 308.44 325.38 6.77 o 9 4 1 79.99 77.99 2.41 o 10 4 1 74.93 72.40 1.16 o 11 4 1 92.66 101.75 1.55 o 12 4 1 17.52 19.55 0.59 o 13 4 1 45.71 51.10 1.02 o 14 4 1 74.29 77.48 2.12 o -14 5 1 44.98 48.36 1.16 o -13 5 1 23.45 27.00 0.83 o -12 5 1 158.83 165.57 3.02 o -11 5 1 77.43 82.84 1.27 o -10 5 1 43.47 46.80 0.85 o -9 5 1 377.75 397.26 8.31 o -8 5 1 122.80 130.49 3.64 o -7 5 1 25.10 31.93 1.01 o -6 5 1 571.53 601.59 13.67 o -5 5 1 2.04 -0.62 1.07 o -4 5 1 428.58 426.89 13.89 o -3 5 1 1890.44 2161.96 88.15 o -2 5 1 735.56 740.58 19.53 o -1 5 1 717.70 777.77 18.73 o 0 5 1 2440.44 2634.96 70.60 o 1 5 1 1561.61 1541.82 82.75 o 2 5 1 2807.04 2928.72 109.64 o 3 5 1 390.13 366.53 12.00 o 4 5 1 1.91 2.03 0.55 o 5 5 1 654.57 725.21 19.06 o 6 5 1 18.78 24.68 0.81 o 7 5 1 77.29 82.83 2.10 o 8 5 1 329.95 346.04 7.93 o 9 5 1 61.78 67.36 1.21 o 10 5 1 117.55 129.37 1.96 o 11 5 1 108.13 109.51 2.17 o 12 5 1 15.50 17.68 0.59 o 13 5 1 41.49 46.58 1.25 o 14 5 1 1.29 1.37 0.26 o -14 6 1 3.05 1.52 0.40 o -13 6 1 41.37 46.72 1.30 o -12 6 1 39.50 38.75 0.97 o -11 6 1 184.32 193.76 2.91 o -10 6 1 19.99 19.80 0.54 o -9 6 1 84.79 84.40 2.46 o -8 6 1 143.38 144.95 3.94 o -7 6 1 894.95 965.09 25.12 o -6 6 1 58.94 58.88 1.39 o -5 6 1 464.40 320.30 20.49 o -4 6 1 211.75 206.77 8.76 o -3 6 1 889.36 988.90 40.48 o -2 6 1 3360.87 3870.62 242.67 o -1 6 1 762.22 740.36 13.68 o 0 6 1 2402.80 2641.99 47.18 o 1 6 1 4309.07 4462.09 233.27 o 2 6 1 1048.27 1116.84 45.00 o 3 6 1 304.14 275.24 9.10 o 4 6 1 528.78 551.66 14.92 o 5 6 1 47.01 50.93 1.45 o 6 6 1 782.68 834.49 20.82 o 7 6 1 107.90 106.08 2.63 o 8 6 1 74.04 76.21 1.81 o 9 6 1 15.67 14.15 0.49 o 10 6 1 179.40 190.41 3.00 o 11 6 1 28.16 28.15 0.82 o 12 6 1 49.29 56.06 1.48 o 13 6 1 2.04 1.64 0.50 o -13 7 1 20.32 19.58 0.72 o -12 7 1 36.26 36.28 1.02 o -11 7 1 45.36 50.49 1.20 o -10 7 1 376.94 385.66 6.06 o -9 7 1 47.08 45.67 0.97 o -8 7 1 846.71 884.72 22.57 o -7 7 1 69.79 67.21 1.78 o -6 7 1 613.70 628.90 20.65 o -5 7 1 12.68 12.22 0.63 o -4 7 1 1041.43 1099.31 44.34 o -3 7 1 765.51 848.88 34.26 o -2 7 1 65.94 62.33 2.75 o -1 7 1 1515.93 1537.15 96.55 o 0 7 1 955.20 921.54 48.37 o 1 7 1 91.05 91.51 3.93 o 2 7 1 752.96 851.92 34.40 o 3 7 1 691.55 697.76 28.26 o 4 7 1 11.80 12.88 0.55 o 5 7 1 432.81 483.62 11.05 o 6 7 1 102.07 92.71 2.22 o 7 7 1 621.72 539.76 12.91 o 8 7 1 74.07 70.80 1.46 o 9 7 1 542.63 562.45 8.69 o 10 7 1 66.31 75.48 1.67 o 11 7 1 23.57 23.07 0.71 o 12 7 1 29.60 27.43 0.79 o 13 7 1 7.07 5.95 0.62 o -13 8 1 12.16 10.63 0.51 o -12 8 1 9.07 9.55 0.54 o -11 8 1 13.91 13.82 0.67 o -10 8 1 36.01 37.28 1.11 o -9 8 1 294.27 305.94 5.13 o -8 8 1 9.52 11.43 0.53 o -7 8 1 878.93 917.75 20.72 o -6 8 1 299.88 306.11 7.80 o -5 8 1 672.49 682.09 16.50 o -4 8 1 247.35 236.35 6.33 o -3 8 1 18.22 15.75 0.91 o -2 8 1 577.13 576.87 36.49 o -1 8 1 200.52 208.35 9.89 o 0 8 1 126.66 132.82 6.47 o 1 8 1 439.16 417.99 7.49 o 2 8 1 28.23 24.31 0.92 o 3 8 1 170.77 170.68 4.09 o 4 8 1 447.35 443.19 10.08 o 5 8 1 472.48 510.07 13.10 o 6 8 1 557.33 567.70 15.92 o 7 8 1 7.05 9.39 0.64 o 8 8 1 419.84 394.90 7.28 o 9 8 1 22.91 25.28 0.88 o 10 8 1 17.92 19.29 0.76 o 11 8 1 5.97 6.20 0.51 o 12 8 1 9.47 8.97 0.44 o -12 9 1 77.53 81.20 1.85 o -11 9 1 20.84 20.73 0.71 o -10 9 1 52.23 56.58 1.43 o -9 9 1 11.14 9.57 0.53 o -8 9 1 172.04 174.52 2.77 o -7 9 1 25.04 28.03 0.70 o -6 9 1 791.26 782.66 14.16 o -5 9 1 434.21 470.95 13.45 o -4 9 1 387.75 390.14 10.19 o -3 9 1 1031.78 1040.52 25.91 o -2 9 1 282.54 279.62 7.11 o -1 9 1 255.18 245.54 6.82 o 0 9 1 401.27 388.25 10.65 o 1 9 1 439.20 436.14 12.24 o 2 9 1 847.85 857.08 21.81 o 3 9 1 386.13 385.38 9.94 o 4 9 1 415.42 443.83 15.60 o 5 9 1 561.59 576.29 12.59 o 6 9 1 28.75 36.15 0.98 o 7 9 1 222.56 230.09 4.42 o 8 9 1 15.81 13.93 0.62 o 9 9 1 69.75 75.61 1.83 o 10 9 1 32.62 31.02 0.92 o 11 9 1 54.42 59.99 1.40 o -11 10 1 98.39 107.94 2.41 o -10 10 1 90.59 100.22 2.29 o -9 10 1 122.32 126.95 2.73 o -8 10 1 12.21 10.58 0.61 o -7 10 1 259.03 270.08 4.64 o -6 10 1 23.53 23.68 0.63 o -5 10 1 126.41 132.95 2.38 o -4 10 1 56.43 58.34 1.30 o -3 10 1 85.47 88.13 2.86 o -2 10 1 208.68 221.07 7.48 o -1 10 1 395.32 373.64 12.42 o 0 10 1 327.35 316.25 10.56 o 1 10 1 328.08 349.86 11.65 o 2 10 1 99.85 96.54 2.96 o 3 10 1 79.77 83.55 1.86 o 4 10 1 158.41 164.37 2.66 o 5 10 1 36.14 37.11 0.80 o 6 10 1 349.92 379.28 7.43 o 7 10 1 9.94 8.91 0.63 o 8 10 1 166.66 167.89 3.55 o 9 10 1 69.87 76.03 1.78 o 10 10 1 68.31 74.18 1.70 o 11 10 1 4.94 6.36 0.72 o -10 11 1 10.80 8.67 0.52 o -9 11 1 12.36 12.36 0.54 o -8 11 1 30.92 34.20 1.21 o -7 11 1 19.09 18.21 0.69 o -6 11 1 17.16 17.79 0.64 o -5 11 1 95.62 89.20 1.81 o -4 11 1 345.48 338.24 7.00 o -3 11 1 13.67 11.40 0.63 o -2 11 1 139.42 140.97 3.41 o -1 11 1 44.01 47.22 1.19 o 0 11 1 60.49 67.54 1.59 o 1 11 1 103.31 109.51 2.30 o 2 11 1 10.00 7.45 0.53 o 3 11 1 427.09 424.14 7.99 o 4 11 1 77.24 72.23 1.55 o 5 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