#------------------------------------------------------------------------------ #$Date: 2017-02-22 04:19:09 +0200 (Wed, 22 Feb 2017) $ #$Revision: 192430 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/02/07/2020719.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2020719 _cell_angle_alpha 90.000 _cell_angle_beta 99.734 _cell_angle_gamma 90.000 _cell_length_a 13.0725 _cell_length_b 12.3992 _cell_length_c 30.0047 _exptl_crystal_F_000 2128.00 _reflns_d_resolution_high 0.8409 _cod_data_source_file wq3130Isup2.hkl _cod_data_source_block I _shelx_title ' ab13g3_a.res in P2(1)/n' _shelx_refln_list_code 4 _shelx_f_calc_maximum 426.65 _shelx_f_squared_multiplier 1.000 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 1302.50 1508.10 84.18 o 4 0 0 507.06 523.04 50.88 o 6 0 0 1875.48 1932.63 145.65 o 8 0 0 23862.27 28090.00 823.09 o 10 0 0 17805.83 17390.00 840.22 o 12 0 0 130.59 97.88 56.78 o 14 0 0 108.17 122.40 91.57 o 2 1 0 4720.16 4793.22 446.61 o 3 1 0 782.98 913.93 88.36 o 4 1 0 12197.80 13220.11 463.58 o 5 1 0 19911.16 23697.96 389.41 o 6 1 0 997.80 984.87 64.47 o 7 1 0 85.97 47.98 21.55 o 8 1 0 4503.32 4203.72 243.99 o 9 1 0 1.48 18.06 27.87 o 10 1 0 13.54 -2.26 42.99 o 11 1 0 92.46 107.34 45.54 o 12 1 0 331.33 347.06 86.67 o 13 1 0 568.37 430.49 108.75 o 14 1 0 1214.94 1045.64 218.30 o 15 1 0 853.86 855.50 212.91 o 0 2 0 65.37 67.49 11.66 o 1 2 0 23664.78 23264.34 456.89 o 2 2 0 15531.10 15873.89 436.28 o 3 2 0 31480.43 31180.76 1564.39 o 4 2 0 20277.21 19837.57 916.83 o 5 2 0 9312.39 10347.99 821.24 o 6 2 0 3673.77 3492.36 129.55 o 7 2 0 19.85 57.98 22.28 o 8 2 0 2880.96 2701.33 198.12 o 9 2 0 1771.26 1925.47 179.59 o 10 2 0 2719.36 2748.02 225.60 o 11 2 0 1961.45 2245.17 219.04 o 12 2 0 113.40 182.96 74.76 o 13 2 0 3219.26 3299.80 303.36 o 14 2 0 857.72 928.72 177.62 o 15 2 0 486.14 295.05 70.18 o 1 3 0 724.70 784.11 30.31 o 2 3 0 14173.94 15436.61 350.06 o 3 3 0 3659.93 3695.26 194.22 o 4 3 0 6037.84 6361.33 362.17 o 5 3 0 249.23 296.27 37.26 o 6 3 0 404.21 630.13 66.07 o 7 3 0 54.94 140.69 30.51 o 8 3 0 8405.90 8015.85 409.56 o 9 3 0 2103.42 2097.39 221.55 o 10 3 0 1165.79 1191.57 151.89 o 11 3 0 343.15 423.99 99.06 o 12 3 0 74.33 52.33 67.24 o 13 3 0 10.14 13.42 39.69 o 14 3 0 215.02 170.62 57.49 o 15 3 0 15.81 31.09 13.57 o 0 4 0 12068.24 11049.13 285.56 o 1 4 0 7535.96 7266.75 284.81 o 2 4 0 10733.88 10644.95 198.42 o 3 4 0 5378.95 5388.85 146.67 o 4 4 0 3567.18 3740.14 199.21 o 5 4 0 9.01 55.72 40.40 o 6 4 0 2567.62 3155.02 411.38 o 7 4 0 3012.91 3434.61 972.80 o 8 4 0 6862.17 7105.49 1793.10 o 9 4 0 1151.74 1412.05 701.59 o 10 4 0 4138.49 4026.18 328.26 o 11 4 0 1785.21 1882.59 197.21 o 12 4 0 784.17 810.16 160.53 o 13 4 0 233.28 303.80 76.94 o 14 4 0 1106.02 1275.77 182.65 o 1 5 0 1195.15 1329.63 50.23 o 2 5 0 2173.30 2441.18 72.93 o 3 5 0 310.87 346.88 31.25 o 4 5 0 9002.60 10314.50 352.28 o 5 5 0 5530.51 5539.96 434.62 o 6 5 0 170.19 288.44 66.11 o 7 5 0 384.04 496.45 407.67 o 8 5 0 373.93 444.15 283.20 o 9 5 0 282.79 274.73 70.58 o 10 5 0 478.91 581.09 126.73 o 11 5 0 1233.82 1193.81 152.37 o 12 5 0 2250.16 2407.53 243.81 o 13 5 0 817.43 760.52 132.80 o 14 5 0 856.29 1074.71 207.52 o 0 6 0 3968.35 4225.47 124.20 o 1 6 0 17294.34 15817.38 521.35 o 2 6 0 678.98 716.36 41.65 o 3 6 0 30631.85 32332.34 800.64 o 4 6 0 8092.50 8428.39 187.50 o 5 6 0 7752.81 7751.90 323.26 o 6 6 0 739.19 829.21 112.90 o 7 6 0 4719.75 5072.00 588.30 o 8 6 0 107.65 187.66 82.56 o 9 6 0 151.46 308.86 219.11 o 10 6 0 17.03 10.41 163.32 o 11 6 0 3443.49 3971.85 969.92 o 12 6 0 166.45 267.69 89.88 o 13 6 0 2351.38 2235.70 599.38 o 1 7 0 3318.54 3435.94 260.36 o 2 7 0 132.54 144.98 27.29 o 3 7 0 855.32 967.80 64.31 o 4 7 0 4039.23 4434.75 151.37 o 5 7 0 3140.04 2852.87 195.19 o 6 7 0 701.32 614.55 73.20 o 7 7 0 616.72 631.97 80.75 o 8 7 0 117.70 165.14 55.03 o 9 7 0 7092.28 7222.89 937.47 o 10 7 0 867.13 867.35 146.09 o 11 7 0 198.23 192.99 113.48 o 12 7 0 558.19 599.27 203.25 o 13 7 0 1981.06 2155.51 319.88 o 0 8 0 1745.80 1286.31 81.40 o 1 8 0 3680.35 3173.02 100.39 o 2 8 0 143.46 177.49 31.05 o 3 8 0 55.20 36.71 10.58 o 4 8 0 1500.34 1571.04 93.94 o 5 8 0 16.94 7.20 14.78 o 6 8 0 5.01 23.43 25.44 o 7 8 0 2527.85 2755.87 190.43 o 8 8 0 1828.52 2313.10 254.58 o 9 8 0 3935.47 4193.42 246.03 o 10 8 0 50.46 49.92 36.23 o 11 8 0 311.07 166.15 71.69 o 12 8 0 65.53 135.89 62.93 o 1 9 0 18.18 12.55 9.37 o 2 9 0 947.85 1038.78 72.90 o 3 9 0 34.71 91.71 28.26 o 4 9 0 293.57 271.73 45.62 o 5 9 0 793.79 808.84 73.73 o 6 9 0 1487.33 1391.20 105.66 o 7 9 0 1278.37 1269.51 129.33 o 8 9 0 18.52 44.13 39.72 o 9 9 0 5.32 -2.20 19.75 o 10 9 0 408.48 349.64 64.52 o 11 9 0 81.14 80.00 31.96 o 12 9 0 236.39 147.07 70.71 o 0 10 0 777.11 715.39 68.78 o 1 10 0 13910.17 12630.23 351.45 o 2 10 0 233.38 250.18 37.22 o 3 10 0 146.89 161.15 34.45 o 4 10 0 3259.52 3482.23 191.71 o 5 10 0 2211.03 2203.07 168.32 o 6 10 0 547.39 571.22 80.20 o 7 10 0 2360.37 2578.07 190.68 o 8 10 0 791.38 809.08 109.90 o 9 10 0 4628.62 4966.73 365.51 o 10 10 0 125.25 162.29 49.16 o 11 10 0 1057.88 1283.06 206.17 o 1 11 0 69.10 47.93 25.61 o 2 11 0 385.86 398.75 61.20 o 3 11 0 64.67 48.33 26.37 o 4 11 0 255.69 310.90 62.28 o 5 11 0 276.93 308.42 68.80 o 6 11 0 77.83 74.57 40.93 o 7 11 0 222.34 262.99 69.04 o 8 11 0 1113.17 1051.44 134.05 o 9 11 0 743.52 646.10 104.19 o 10 11 0 90.35 27.51 26.95 o 0 12 0 4607.40 3641.90 359.09 o 1 12 0 388.96 309.82 57.21 o 2 12 0 469.78 473.69 65.43 o 3 12 0 1577.41 1403.21 117.73 o 4 12 0 3590.28 3740.55 375.03 o 5 12 0 37.41 75.63 48.27 o 6 12 0 1386.32 1320.87 137.22 o 7 12 0 426.18 400.36 79.14 o 8 12 0 1042.41 1116.08 145.32 o 1 13 0 102.51 167.47 93.20 o 2 13 0 566.72 699.07 168.37 o 3 13 0 76.47 112.99 74.29 o 4 13 0 509.86 547.09 143.29 o 5 13 0 379.97 366.41 108.41 o 6 13 0 50.98 91.35 65.79 o 7 13 0 411.85 461.22 122.48 o 0 14 0 1620.33 1677.37 294.73 o 1 14 0 2.26 15.10 20.14 o 2 14 0 85.98 123.84 72.29 o 3 14 0 19.81 39.84 58.77 o 4 14 0 1104.27 1376.10 254.20 o -15 0 1 1674.59 1120.89 330.97 o -13 0 1 832.17 538.81 215.06 o -11 0 1 1542.42 1362.62 266.61 o -9 0 1 2636.53 2982.85 300.32 o -7 0 1 9249.22 11247.25 502.31 o -5 0 1 834.64 698.28 67.27 o -3 0 1 11023.90 11170.13 298.88 o 3 0 1 61151.17 65124.09 1467.18 o 5 0 1 16109.75 16936.18 1035.17 o 7 0 1 9541.79 10817.98 496.99 o 9 0 1 2193.91 2928.59 288.06 o 11 0 1 4106.47 3779.08 451.74 o 13 0 1 66.56 31.37 70.12 o 15 0 1 274.48 55.88 57.32 o -15 1 1 30.88 67.43 49.53 o -14 1 1 1067.14 856.42 188.41 o -13 1 1 1013.73 928.98 177.43 o -12 1 1 1563.73 1492.30 272.02 o -11 1 1 672.34 855.06 141.79 o -10 1 1 19.38 36.55 23.80 o -9 1 1 8861.55 8891.00 387.85 o -8 1 1 881.27 774.19 106.43 o -7 1 1 45.67 44.50 17.09 o -6 1 1 6000.93 6108.66 305.88 o -5 1 1 225.52 268.93 32.81 o -4 1 1 8029.17 7935.00 240.47 o -3 1 1 6047.10 6092.17 275.48 o -2 1 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