#------------------------------------------------------------------------------ #$Date: 2017-07-25 12:03:35 +0300 (Tue, 25 Jul 2017) $ #$Revision: 199078 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/02/07/2020787.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2020787 _cell_angle_alpha 90.000 _cell_angle_beta 99.079 _cell_angle_gamma 90.000 _cell_length_a 10.5376 _cell_length_b 21.5025 _cell_length_c 19.9462 _exptl_crystal_F_000 1944.00 _reflns_d_resolution_high 0.7202 _cod_data_source_file ov3091Isup2.hkl _cod_data_source_block I _shelx_title ' 160427_SRE040105a in P21/n # 14' _shelx_refln_list_code 4 _shelx_f_calc_maximum 386.65 _shelx_f_squared_multiplier 1.000 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 31721.03 33649.81 273.83 o 4 0 0 14346.71 14673.12 120.95 o 6 0 0 2269.37 2486.65 57.29 o 8 0 0 1295.14 1539.88 121.79 o 10 0 0 229.36 179.26 53.21 o 12 0 0 19.82 -44.59 53.90 o 2 1 0 12467.66 12811.95 74.21 o 3 1 0 268.64 330.73 14.36 o 4 1 0 2019.09 2069.47 47.78 o 5 1 0 72.31 37.55 9.07 o 6 1 0 594.89 573.62 29.63 o 7 1 0 758.85 625.32 63.72 o 8 1 0 746.23 677.23 33.23 o 9 1 0 150.94 148.37 18.70 o 10 1 0 12.84 -25.55 25.55 o 11 1 0 36.89 5.89 23.63 o 12 1 0 386.23 467.31 62.19 o 13 1 0 10.81 23.77 35.19 o 2 2 0 18873.14 19317.76 225.05 o 3 2 0 0.04 7.99 5.66 o 4 2 0 13666.91 13071.73 141.62 o 5 2 0 874.22 676.89 24.23 o 6 2 0 3499.95 3246.96 73.71 o 7 2 0 88.52 66.64 16.91 o 8 2 0 338.47 353.34 28.21 o 9 2 0 855.96 868.53 42.99 o 10 2 0 404.06 352.33 49.01 o 11 2 0 5.16 -18.33 21.69 o 12 2 0 62.66 60.40 29.81 o 13 2 0 53.90 68.05 28.76 o 1 3 0 1334.50 1238.76 42.96 o 2 3 0 435.21 506.41 13.06 o 3 3 0 575.94 477.23 19.75 o 4 3 0 667.77 771.11 25.38 o 5 3 0 6372.67 6180.84 76.58 o 6 3 0 9023.21 8934.03 131.74 o 7 3 0 2184.20 1772.50 107.73 o 8 3 0 459.32 509.38 34.27 o 9 3 0 171.31 246.25 27.41 o 10 3 0 220.16 221.54 69.73 o 11 3 0 266.78 306.69 50.20 o 12 3 0 246.43 281.04 50.42 o 13 3 0 176.13 233.28 47.62 o 0 4 0 52.69 66.11 14.94 o 1 4 0 21698.81 21831.57 633.54 o 2 4 0 7256.22 7148.31 58.24 o 3 4 0 461.90 353.43 11.58 o 4 4 0 5968.63 5887.77 96.15 o 5 4 0 801.05 1029.65 33.42 o 6 4 0 2395.11 2304.03 60.52 o 7 4 0 143.19 128.95 20.49 o 8 4 0 2197.39 2267.47 76.33 o 9 4 0 7.22 1.46 14.00 o 10 4 0 1241.64 1285.40 90.75 o 11 4 0 24.08 25.03 23.68 o 12 4 0 31.38 32.34 34.97 o 13 4 0 90.09 77.95 43.20 o 1 5 0 712.68 693.21 34.48 o 2 5 0 3345.04 2916.79 59.46 o 3 5 0 3900.58 4172.95 44.21 o 4 5 0 1032.89 834.64 22.46 o 5 5 0 4769.54 4641.66 75.78 o 6 5 0 1747.43 1599.21 57.62 o 7 5 0 1931.67 2268.97 64.83 o 8 5 0 807.33 873.45 49.42 o 9 5 0 123.79 98.75 19.25 o 10 5 0 503.72 498.96 58.55 o 11 5 0 411.43 448.28 60.33 o 12 5 0 694.52 803.97 82.31 o 13 5 0 118.57 177.55 53.04 o 0 6 0 1973.19 1761.43 83.09 o 1 6 0 926.32 1044.50 44.65 o 2 6 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100.00 o 2 14 0 241.58 312.58 32.30 o 3 14 0 1406.17 1338.16 58.09 o 4 14 0 3648.34 4093.16 102.18 o 5 14 0 89.34 50.82 25.72 o 6 14 0 2163.67 1509.04 130.49 o 7 14 0 642.32 543.25 44.56 o 8 14 0 360.90 342.27 78.52 o 9 14 0 227.69 223.98 62.85 o 10 14 0 231.26 228.59 72.75 o 11 14 0 49.84 158.04 70.98 o 1 15 0 6.88 15.38 15.14 o 2 15 0 2530.40 2676.70 93.31 o 3 15 0 406.97 388.40 28.85 o 4 15 0 688.96 701.40 43.77 o 5 15 0 17.95 -13.84 13.84 o 6 15 0 609.04 489.15 50.33 o 7 15 0 219.11 234.79 25.57 o 8 15 0 175.61 166.31 40.93 o 9 15 0 246.20 310.16 80.11 o 10 15 0 37.10 1.56 35.63 o 0 16 0 5445.26 5301.66 176.41 o 1 16 0 1732.40 1732.60 77.96 o 2 16 0 1851.58 1892.26 107.71 o 3 16 0 1190.13 1119.64 49.67 o 4 16 0 134.29 61.06 13.94 o 5 16 0 46.70 16.04 9.80 o 6 16 0 510.72 494.24 71.07 o 7 16 0 967.18 1129.79 99.23 o 8 16 0 277.16 244.50 47.43 o 9 16 0 479.28 553.49 100.54 o 10 16 0 180.95 186.42 56.69 o 1 17 0 1572.46 1769.91 100.00 o 2 17 0 6.08 0.49 18.91 o 3 17 0 717.10 709.92 42.16 o 4 17 0 40.75 24.10 14.06 o 5 17 0 124.29 97.42 15.23 o 6 17 0 645.14 736.71 74.13 o 7 17 0 80.93 134.83 56.34 o 8 17 0 56.50 81.84 27.67 o 9 17 0 45.15 73.64 54.85 o 10 17 0 193.97 227.76 72.44 o 0 18 0 11.56 15.25 30.58 o 1 18 0 44.93 28.05 22.43 o 2 18 0 437.60 460.22 55.50 o 3 18 0 136.47 124.53 21.98 o 4 18 0 802.76 764.86 44.01 o 5 18 0 13.91 -2.44 16.81 o 6 18 0 44.58 7.51 39.06 o 7 18 0 235.18 266.56 69.46 o 8 18 0 458.97 491.75 68.40 o 9 18 0 143.27 209.03 64.30 o 10 18 0 129.45 163.35 69.20 o 1 19 0 691.07 680.95 66.12 o 2 19 0 292.74 252.90 44.58 o 3 19 0 373.27 399.49 37.87 o 4 19 0 289.64 219.39 35.16 o 5 19 0 6.78 -43.26 43.26 o 6 19 0 792.91 996.85 135.90 o 7 19 0 175.60 146.90 55.08 o 8 19 0 30.71 62.47 42.96 o 9 19 0 36.21 19.24 28.74 o 0 20 0 839.36 813.84 103.05 o 1 20 0 69.37 4.78 26.61 o 2 20 0 330.95 323.55 50.34 o 3 20 0 5.25 -0.83 26.75 o 4 20 0 65.45 25.90 20.91 o 5 20 0 334.06 381.03 87.50 o 6 20 0 294.33 352.34 84.36 o 7 20 0 1.62 24.31 47.15 o 8 20 0 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2 1 574.69 720.08 79.78 o 13 2 1 4.06 -7.21 24.50 o -13 3 1 109.44 171.13 45.68 o -12 3 1 58.34 56.15 27.62 o -11 3 1 132.23 174.84 41.28 o -10 3 1 79.29 76.53 27.22 o -9 3 1 3287.70 3866.17 96.69 o -8 3 1 19.97 27.43 16.87 o -7 3 1 208.63 186.45 21.92 o -6 3 1 1280.08 1084.18 37.16 o -5 3 1 2193.23 2310.85 46.24 o -4 3 1 99.49 96.22 11.25 o -3 3 1 654.36 627.98 21.79 o -2 3 1 118.27 183.00 9.34 o 1 3 1 16020.49 15757.15 280.72 o 2 3 1 12.64 6.83 3.93 o 3 3 1 1926.23 1856.35 37.21 o 4 3 1 6231.77 7079.14 127.97 o 5 3 1 14611.60 14406.89 157.18 o 6 3 1 145.60 92.27 14.76 o 7 3 1 1862.63 1656.43 87.23 o 8 3 1 384.42 306.99 28.67 o 9 3 1 1060.87 1122.21 66.47 o 10 3 1 45.29 30.25 30.77 o 11 3 1 91.21 111.72 37.92 o 12 3 1 0.91 28.09 41.41 o 13 3 1 58.54 142.02 66.77 o -14 4 1 30.83 80.92 54.17 o -13 4 1 58.17 46.18 32.73 o -12 4 1 551.12 679.77 74.06 o -11 4 1 546.03 613.55 111.80 o -10 4 1 45.50 38.82 35.91 o -9 4 1 498.81 536.43 50.50 o -8 4 1 10.12 -1.72 14.20 o -7 4 1 4671.26 4940.13 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