#------------------------------------------------------------------------------ #$Date: 2017-07-25 12:07:47 +0300 (Tue, 25 Jul 2017) $ #$Revision: 199093 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/02/08/2020806.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2020806 _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 9.9801 _cell_length_b 18.8540 _cell_length_c 26.1414 _exptl_crystal_F_000 1856.00 _reflns_d_resolution_high 0.8118 _cod_data_source_file sk3660Isup2.hkl _cod_data_source_block I _shelx_title ' ma65 in P212121' _shelx_refln_list_code 4 _shelx_f_calc_maximum 255.41 _shelx_f_squared_multiplier 1.000 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 4 0 0 3239.37 3855.47 129.56 o 6 0 0 55.30 57.80 64.34 o 8 0 0 372.31 374.35 54.59 o 10 0 0 635.94 611.40 69.88 o 12 0 0 20.96 15.47 56.48 o 1 1 0 8.60 105.80 99.62 o 2 1 0 16780.27 15784.41 1383.28 o 3 1 0 418.33 334.92 103.90 o 4 1 0 23.93 29.75 82.46 o 5 1 0 53.43 123.97 72.64 o 6 1 0 2.68 6.75 40.67 o 7 1 0 74.92 98.20 44.49 o 8 1 0 299.27 346.50 44.99 o 9 1 0 1.13 35.24 49.84 o 10 1 0 286.75 312.47 41.56 o 11 1 0 0.22 49.27 41.12 o 12 1 0 215.18 195.70 43.15 o 1 2 0 111.49 122.81 60.06 o 2 2 0 11535.85 11014.92 1550.05 o 3 2 0 206.27 196.38 66.05 o 4 2 0 1159.65 1076.13 90.07 o 5 2 0 317.38 367.50 69.69 o 6 2 0 752.84 619.83 57.23 o 7 2 0 0.01 -5.80 38.50 o 8 2 0 203.25 249.29 57.99 o 9 2 0 12.86 21.71 39.79 o 10 2 0 120.05 69.57 43.72 o 11 2 0 87.58 75.26 38.52 o 12 2 0 22.32 69.58 40.05 o 1 3 0 1282.36 976.40 59.52 o 2 3 0 24729.65 25555.38 196.90 o 3 3 0 180.60 165.95 59.90 o 4 3 0 1796.29 2442.86 197.30 o 5 3 0 126.57 119.77 43.33 o 6 3 0 0.76 49.94 55.66 o 7 3 0 131.84 103.15 56.98 o 8 3 0 3525.27 3041.58 130.35 o 9 3 0 10.51 42.22 39.80 o 10 3 0 315.97 408.71 72.93 o 11 3 0 102.86 89.40 38.18 o 12 3 0 291.25 303.19 43.47 o 1 4 0 749.83 618.88 53.43 o 2 4 0 0.05 16.01 46.36 o 3 4 0 422.04 386.15 63.05 o 4 4 0 999.91 1132.29 138.31 o 5 4 0 607.62 600.36 47.93 o 6 4 0 42.03 96.17 55.16 o 7 4 0 268.07 257.30 55.28 o 8 4 0 322.92 382.21 53.78 o 9 4 0 403.90 408.99 46.61 o 10 4 0 8.26 -9.69 36.53 o 11 4 0 3.92 47.75 40.27 o 12 4 0 45.99 55.05 37.05 o 1 5 0 2555.38 2466.45 187.99 o 2 5 0 1763.23 1443.54 195.13 o 3 5 0 121.69 78.14 39.85 o 4 5 0 176.36 196.33 43.91 o 5 5 0 63.90 125.02 40.05 o 6 5 0 8.41 25.21 36.99 o 7 5 0 144.84 124.47 49.75 o 8 5 0 631.53 644.42 56.29 o 9 5 0 96.92 103.21 49.69 o 10 5 0 1025.82 997.74 61.95 o 11 5 0 8.55 42.49 38.77 o 0 6 0 1656.41 1489.54 60.63 o 1 6 0 9101.06 8289.62 624.64 o 2 6 0 1111.96 1172.56 45.02 o 3 6 0 47.85 66.47 38.67 o 4 6 0 93.02 156.55 39.46 o 5 6 0 0.04 0.86 33.51 o 6 6 0 222.68 228.67 35.63 o 7 6 0 121.83 147.51 34.56 o 8 6 0 1098.65 1106.01 60.00 o 9 6 0 367.63 374.41 52.64 o 10 6 0 32.47 29.65 32.98 o 11 6 0 0.01 24.25 38.31 o 1 7 0 2943.77 2971.67 70.76 o 2 7 0 42.01 63.37 31.80 o 3 7 0 1.91 14.94 35.34 o 4 7 0 3227.76 3474.58 329.41 o 5 7 0 166.29 174.05 35.17 o 6 7 0 727.78 744.90 83.49 o 7 7 0 0.00 40.80 30.02 o 8 7 0 49.97 90.44 44.84 o 9 7 0 3.22 -4.03 45.03 o 10 7 0 525.57 469.32 51.39 o 11 7 0 8.29 12.20 44.69 o 0 8 0 148.09 278.37 38.81 o 1 8 0 2864.90 2794.74 64.59 o 2 8 0 884.30 781.43 50.32 o 3 8 0 199.38 234.08 34.01 o 4 8 0 115.78 104.24 29.16 o 5 8 0 498.70 514.20 37.53 o 6 8 0 0.00 -15.60 33.07 o 7 8 0 133.03 98.59 33.83 o 8 8 0 0.49 28.84 35.27 o 9 8 0 3.92 -6.35 45.10 o 10 8 0 0.72 6.79 42.33 o 11 8 0 9.23 9.69 47.80 o 1 9 0 2794.38 2937.64 61.39 o 2 9 0 310.54 302.02 26.74 o 3 9 0 277.98 279.22 39.31 o 4 9 0 369.19 336.88 29.83 o 5 9 0 304.72 353.03 49.37 o 6 9 0 518.60 520.89 33.89 o 7 9 0 218.26 176.00 34.47 o 8 9 0 603.81 677.23 38.61 o 9 9 0 27.16 46.67 41.70 o 10 9 0 437.57 472.53 49.12 o 11 9 0 0.28 6.92 51.39 o 0 10 0 4715.22 4454.79 66.92 o 1 10 0 456.29 383.79 39.81 o 2 10 0 70.44 27.86 37.93 o 3 10 0 55.91 63.00 26.06 o 4 10 0 1010.73 964.09 42.25 o 5 10 0 0.00 0.32 30.89 o 6 10 0 186.57 218.52 31.86 o 7 10 0 680.04 627.14 42.08 o 8 10 0 133.31 123.24 35.03 o 9 10 0 24.15 63.83 33.06 o 10 10 0 136.55 92.14 43.40 o 11 10 0 8.92 55.91 43.52 o 1 11 0 5612.81 6444.80 245.79 o 2 11 0 2076.42 2200.26 61.13 o 3 11 0 514.05 486.89 30.05 o 4 11 0 92.31 113.97 26.87 o 5 11 0 1105.15 1098.24 40.94 o 6 11 0 215.54 227.29 28.56 o 7 11 0 652.35 669.04 35.31 o 8 11 0 75.58 62.80 33.96 o 9 11 0 1.10 14.66 33.54 o 10 11 0 159.25 149.23 35.25 o 0 12 0 15.06 42.73 27.29 o 1 12 0 15.78 43.05 23.15 o 2 12 0 417.24 478.69 40.00 o 3 12 0 3.14 17.67 47.11 o 4 12 0 51.52 75.64 29.11 o 5 12 0 15.38 11.81 26.93 o 6 12 0 2277.70 2120.29 59.84 o 7 12 0 132.23 150.94 28.07 o 8 12 0 6.89 26.72 24.72 o 9 12 0 9.57 21.15 27.63 o 10 12 0 211.82 211.31 33.52 o 1 13 0 238.09 277.73 44.03 o 2 13 0 36.61 22.39 36.35 o 3 13 0 16.33 43.40 49.31 o 4 13 0 91.22 94.72 49.44 o 5 13 0 167.54 163.86 30.65 o 6 13 0 7.16 5.74 37.39 o 7 13 0 72.79 75.36 26.47 o 8 13 0 215.10 198.62 28.01 o 9 13 0 0.00 26.35 29.64 o 10 13 0 10.82 19.97 30.24 o 0 14 0 2674.37 2421.49 204.75 o 1 14 0 458.26 475.71 28.84 o 2 14 0 200.10 211.32 25.41 o 3 14 0 158.44 148.62 46.98 o 4 14 0 24.40 64.40 47.55 o 5 14 0 51.39 74.85 46.35 o 6 14 0 277.37 233.19 30.87 o 7 14 0 0.27 18.39 22.82 o 8 14 0 20.64 29.57 26.62 o 9 14 0 168.40 167.79 29.54 o 1 15 0 39.24 79.02 21.78 o 2 15 0 1047.67 1031.61 31.69 o 3 15 0 749.01 552.09 41.57 o 4 15 0 204.81 144.78 38.81 o 5 15 0 15.36 43.90 50.19 o 6 15 0 314.03 274.29 57.99 o 7 15 0 24.68 24.72 30.88 o 8 15 0 379.99 343.19 27.85 o 9 15 0 172.90 164.53 29.13 o 0 16 0 71.96 56.22 27.73 o 1 16 0 28.25 37.02 22.52 o 2 16 0 15.27 34.31 21.99 o 3 16 0 63.55 56.36 22.15 o 4 16 0 425.64 428.13 49.94 o 5 16 0 764.82 866.06 57.67 o 6 16 0 14.97 28.55 52.01 o 7 16 0 0.13 43.15 55.98 o 8 16 0 75.82 81.83 50.25 o 1 17 0 88.61 136.98 28.30 o 2 17 0 121.47 110.71 20.29 o 3 17 0 3.38 4.01 26.61 o 4 17 0 46.12 15.43 23.67 o 5 17 0 65.89 77.24 39.88 o 6 17 0 123.33 144.22 53.27 o 7 17 0 362.21 325.67 62.45 o 8 17 0 179.19 207.62 64.97 o 0 18 0 345.86 291.14 34.53 o 1 18 0 76.74 115.16 21.13 o 2 18 0 1336.60 1364.88 38.53 o 3 18 0 30.88 18.75 21.62 o 4 18 0 28.28 41.87 27.50 o 5 18 0 0.99 64.09 48.18 o 6 18 0 0.60 7.04 42.52 o 7 18 0 5.98 4.34 56.17 o 1 19 0 80.41 88.92 20.73 o 2 19 0 0.00 4.85 20.08 o 3 19 0 2.08 -2.30 19.14 o 4 19 0 56.63 95.73 24.69 o 5 19 0 28.96 38.92 40.44 o 6 19 0 0.78 16.82 25.50 o 0 20 0 166.34 149.50 35.60 o 1 20 0 4.04 -5.49 20.38 o 2 20 0 0.39 40.06 25.61 o 3 20 0 4.90 -10.86 22.03 o 4 20 0 236.65 329.36 33.26 o 5 20 0 38.94 52.24 26.08 o 6 20 0 0.38 37.78 29.79 o 1 21 0 42.88 33.19 28.60 o 2 21 0 2.05 27.28 27.20 o 3 21 0 0.07 6.79 20.20 o 4 21 0 20.12 27.20 21.69 o 5 21 0 206.84 213.27 24.39 o 0 22 0 1.41 -31.70 33.08 o 1 22 0 11.71 13.12 32.28 o 2 22 0 13.25 24.08 20.68 o 3 22 0 0.24 9.08 21.28 o 1 23 0 0.01 27.81 24.03 o 2 0 1 8703.15 8352.34 211.83 o 3 0 1 837.56 788.52 94.66 o 4 0 1 180.43 142.15 56.09 o 5 0 1 3206.32 3129.05 72.07 o 6 0 1 11.95 10.84 41.25 o 7 0 1 95.77 93.06 45.85 o 8 0 1 1.17 -6.04 43.76 o 9 0 1 332.10 373.49 43.89 o 10 0 1 1534.16 1698.11 99.53 o 11 0 1 5.89 7.03 40.10 o 12 0 1 26.07 48.49 42.41 o -12 1 1 88.38 39.87 41.17 o -11 1 1 142.53 133.58 38.49 o -10 1 1 984.14 1021.52 51.35 o -9 1 1 126.64 124.16 37.31 o -8 1 1 354.16 303.18 44.59 o -7 1 1 19.26 29.92 40.47 o -6 1 1 398.94 406.42 49.05 o -5 1 1 2007.26 2215.66 63.98 o -4 1 1 1351.79 1299.66 101.20 o -3 1 1 1652.29 1728.04 125.48 o -2 1 1 1395.55 1527.13 108.66 o -1 1 1 3796.79 3627.63 146.92 o 1 1 1 3797.20 3571.49 153.66 o 2 1 1 1395.56 976.51 113.02 o 3 1 1 1652.95 1720.75 104.66 o 4 1 1 1351.35 1221.92 84.97 o 5 1 1 2005.79 2193.34 94.97 o 6 1 1 400.05 389.95 43.87 o 7 1 1 19.22 48.48 45.14 o 8 1 1 353.80 327.83 42.21 o 9 1 1 126.72 180.16 42.86 o 10 1 1 983.36 1074.53 67.71 o 11 1 1 142.42 107.16 44.23 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1883.07 1584.63 120.38 o -3 3 1 466.92 391.07 62.30 o -2 3 1 10910.24 9594.03 768.70 o -1 3 1 10032.60 9378.33 109.50 o 0 3 1 5088.72 4470.12 103.08 o 1 3 1 10030.62 9161.70 195.19 o 2 3 1 10913.10 9420.40 1906.00 o 3 3 1 466.65 405.53 62.66 o 4 3 1 1879.44 1996.51 245.20 o 5 3 1 537.58 573.23 67.30 o 6 3 1 2258.40 2799.27 84.41 o 7 3 1 121.49 199.38 58.24 o 8 3 1 948.75 1143.18 66.79 o 9 3 1 79.38 107.26 36.64 o 10 3 1 660.20 627.72 41.18 o 11 3 1 6.79 6.87 40.76 o 12 3 1 45.09 75.56 42.63 o -12 4 1 61.71 57.97 42.19 o -11 4 1 19.49 46.41 35.43 o -10 4 1 547.93 580.83 61.98 o -9 4 1 483.36 492.34 40.34 o -8 4 1 473.64 473.10 57.49 o -7 4 1 105.54 117.80 53.15 o -6 4 1 508.48 647.11 47.30 o -5 4 1 1706.53 1697.21 156.92 o -4 4 1 625.84 643.34 48.61 o -3 4 1 1522.95 1438.94 124.12 o -2 4 1 1498.86 1243.78 78.46 o -1 4 1 6715.50 6699.15 393.57 o 0 4 1 3418.67 3100.69 404.35 o 1 4 1 6714.37 6208.09 85.93 o 2 4 1 1494.31 1224.15 127.65 o 3 4 1 1522.20 1400.32 63.92 o 4 4 1 625.67 736.96 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109.15 109.69 46.23 o -7 6 1 25.74 20.84 35.32 o -6 6 1 414.51 422.84 40.87 o -5 6 1 39.46 70.26 36.33 o -4 6 1 616.09 730.30 73.74 o -3 6 1 1235.35 1367.33 49.03 o -2 6 1 843.30 839.94 51.38 o -1 6 1 4633.48 4843.48 89.75 o 0 6 1 310.63 362.24 50.13 o 1 6 1 4632.21 4508.34 669.42 o 2 6 1 841.38 899.57 43.38 o 3 6 1 1235.39 1240.83 103.71 o 4 6 1 615.21 776.03 164.82 o 5 6 1 39.44 66.56 37.20 o 6 6 1 415.29 359.22 37.33 o 7 6 1 25.88 51.13 36.69 o 8 6 1 109.34 115.73 46.73 o 9 6 1 448.61 474.54 55.54 o 10 6 1 252.26 264.47 50.06 o 11 6 1 40.24 57.52 41.59 o -11 7 1 21.67 24.42 38.33 o -10 7 1 59.60 90.00 44.91 o -9 7 1 326.92 288.37 48.05 o -8 7 1 915.05 890.66 76.23 o -7 7 1 642.19 630.66 74.50 o -6 7 1 713.68 770.30 41.92 o -5 7 1 167.24 171.09 35.09 o -4 7 1 594.06 559.87 38.65 o -3 7 1 1965.65 2218.87 59.95 o -2 7 1 2518.34 2703.47 158.31 o -1 7 1 2230.80 1980.44 62.14 o 0 7 1 5990.46 5180.46 72.24 o 1 7 1 2230.51 2164.23 208.21 o 2 7 1 2520.52 2692.39 50.63 o 3 7 1 1964.29 1902.88 147.99 o 4 7 1 594.12 560.42 35.70 o 5 7 1 167.06 140.67 31.05 o 6 7 1 714.29 779.44 43.24 o 7 7 1 642.10 625.39 73.27 o 8 7 1 915.34 794.93 52.71 o 9 7 1 326.71 305.92 51.39 o 10 7 1 59.61 63.96 47.17 o 11 7 1 21.68 38.35 35.59 o -11 8 1 38.17 48.02 55.54 o -10 8 1 269.97 242.08 44.47 o -9 8 1 27.81 17.04 42.58 o -8 8 1 12.29 24.39 33.67 o -7 8 1 165.86 201.57 33.57 o -6 8 1 116.10 105.07 31.54 o -5 8 1 219.98 213.00 32.53 o -4 8 1 4675.28 5016.23 69.48 o -3 8 1 1435.18 1454.52 54.42 o -2 8 1 1472.82 1384.45 55.54 o -1 8 1 930.78 934.62 52.58 o 0 8 1 8696.24 9004.66 145.04 o 1 8 1 932.35 690.96 46.16 o 2 8 1 1473.92 1605.15 109.59 o 3 8 1 1433.55 1435.44 38.05 o 4 8 1 4675.39 5150.04 288.59 o 5 8 1 219.89 196.10 36.36 o 6 8 1 116.08 118.24 35.31 o 7 8 1 165.73 197.11 43.24 o 8 8 1 12.40 34.13 35.83 o 9 8 1 27.81 50.76 44.72 o 10 8 1 269.66 204.72 45.66 o 11 8 1 38.18 68.74 50.00 o -11 9 1 1.86 -16.67 44.72 o -10 9 1 10.64 55.66 41.32 o -9 9 1 2.02 12.77 45.91 o -8 9 1 3.51 22.31 33.83 o -7 9 1 11.57 63.34 32.15 o -6 9 1 367.49 295.62 34.40 o -5 9 1 445.75 391.20 30.53 o -4 9 1 44.38 63.16 26.88 o -3 9 1 373.79 408.03 29.59 o -2 9 1 980.88 1181.61 58.18 o -1 9 1 2569.61 1805.65 52.96 o 0 9 1 9077.02 9724.17 83.77 o 1 9 1 2571.41 2614.33 185.60 o 2 9 1 978.19 1096.68 94.81 o 3 9 1 375.20 426.83 30.50 o 4 9 1 44.52 52.21 24.99 o 5 9 1 445.21 371.35 31.94 o 6 9 1 367.94 421.54 36.49 o 7 9 1 11.58 32.35 33.05 o 8 9 1 3.57 18.23 33.80 o 9 9 1 1.98 24.84 42.27 o 10 9 1 10.63 15.03 41.38 o 11 9 1 1.86 6.60 44.34 o -11 10 1 126.04 106.67 36.30 o -10 10 1 26.67 39.95 31.54 o -9 10 1 11.30 28.83 33.78 o -8 10 1 20.01 19.74 37.81 o -7 10 1 627.53 602.64 36.22 o -6 10 1 620.81 590.67 31.28 o -5 10 1 132.89 125.29 26.76 o -4 10 1 400.48 409.46 28.47 o -3 10 1 2.13 4.47 47.42 o -2 10 1 1784.90 1996.67 63.02 o -1 10 1 108.84 138.56 37.42 o 0 10 1 1087.97 1202.89 30.99 o 1 10 1 108.42 122.58 25.13 o 2 10 1 1786.48 1892.22 73.40 o 3 10 1 2.18 30.38 28.61 o 4 10 1 400.01 334.19 33.55 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