#------------------------------------------------------------------------------ #$Date: 2017-08-09 08:35:46 +0300 (Wed, 09 Aug 2017) $ #$Revision: 199667 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/02/08/2020848.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2020848 _cell_angle_alpha 90.000 _cell_angle_beta 91.214 _cell_angle_gamma 90.000 _cell_length_a 13.0866 _cell_length_b 21.9339 _cell_length_c 24.8979 _exptl_crystal_F_000 2952.00 _reflns_d_resolution_high 0.7782 _cod_data_source_file eg3222Isup2.hkl _cod_data_source_block I _shelx_title ' 12345 in P2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 300.45 _shelx_f_squared_multiplier 1.000 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 36967.64 33889.95 763.87 o 3 0 0 28251.95 26314.12 388.90 o 4 0 0 47335.75 44015.27 649.18 o 5 0 0 1181.51 1099.07 21.23 o 6 0 0 229.47 271.13 16.20 o 7 0 0 5147.67 4832.41 73.94 o 8 0 0 572.43 624.97 19.37 o 9 0 0 5259.35 5508.64 85.46 o 10 0 0 3126.23 3578.62 68.80 o 11 0 0 145.92 126.80 13.87 o 12 0 0 2383.00 2566.67 53.01 o 13 0 0 210.42 349.59 24.48 o 14 0 0 1322.97 1412.12 47.31 o 15 0 0 2445.67 2549.34 93.16 o 16 0 0 688.76 703.38 151.44 o 2 1 0 653.23 583.70 8.12 o 3 1 0 3487.35 3440.77 38.60 o 4 1 0 52955.14 49723.23 537.67 o 5 1 0 1143.13 1009.97 14.57 o 6 1 0 48544.41 47700.54 481.67 o 7 1 0 16.54 15.89 5.19 o 8 1 0 2946.35 2748.72 34.63 o 9 1 0 9039.10 9360.34 97.60 o 10 1 0 26.68 40.71 8.12 o 11 1 0 139.47 186.31 11.76 o 12 1 0 121.08 60.23 11.43 o 13 1 0 149.72 148.16 13.66 o 14 1 0 38.95 37.68 14.37 o 15 1 0 59.84 41.55 23.57 o 16 1 0 1870.07 1865.43 105.52 o 1 2 0 13546.77 12080.50 158.06 o 2 2 0 7177.59 6881.00 72.30 o 3 2 0 323.97 373.95 7.05 o 4 2 0 12666.30 12199.63 130.08 o 5 2 0 432.52 436.77 9.54 o 6 2 0 11342.85 11888.51 124.05 o 7 2 0 246.26 215.33 8.72 o 8 2 0 1451.23 1285.65 22.72 o 9 2 0 1205.62 1218.34 21.53 o 10 2 0 4529.42 4657.59 59.22 o 11 2 0 2817.91 2670.39 38.92 o 12 2 0 76.87 62.97 10.83 o 13 2 0 4731.92 5179.40 70.11 o 14 2 0 39.32 72.01 13.98 o 15 2 0 5.86 29.63 20.06 o 16 2 0 1065.01 958.44 50.34 o 1 3 0 10768.24 10252.54 108.02 o 2 3 0 298.60 209.95 5.23 o 3 3 0 658.45 925.63 13.20 o 4 3 0 2843.45 2991.12 37.43 o 5 3 0 19.86 32.74 4.09 o 6 3 0 1485.44 1417.95 19.74 o 7 3 0 121.89 93.33 6.47 o 8 3 0 4.97 5.43 5.97 o 9 3 0 2000.94 1882.87 30.13 o 10 3 0 2724.20 2700.11 35.97 o 11 3 0 2578.27 2570.95 36.65 o 12 3 0 1734.89 1549.89 29.22 o 13 3 0 38.92 38.43 11.00 o 14 3 0 75.04 100.01 16.93 o 15 3 0 421.95 397.41 42.91 o 16 3 0 324.21 344.62 49.18 o 0 4 0 7.02 57.66 6.75 o 1 4 0 58.97 22.24 2.93 o 2 4 0 25292.37 24672.01 267.92 o 3 4 0 16921.57 15965.51 157.48 o 4 4 0 71.70 77.78 4.55 o 5 4 0 5547.61 5534.42 59.54 o 6 4 0 4703.17 4579.89 51.13 o 7 4 0 10940.92 11386.98 119.96 o 8 4 0 4688.32 4792.27 60.85 o 9 4 0 127.83 133.45 8.22 o 10 4 0 1342.16 1370.82 23.25 o 11 4 0 173.15 166.78 11.00 o 12 4 0 34.77 16.99 9.10 o 13 4 0 2866.29 2824.96 43.31 o 14 4 0 0.58 17.96 14.89 o 15 4 0 738.98 684.86 47.51 o 16 4 0 17.68 -42.88 42.88 o 1 5 0 7240.56 7312.22 78.63 o 2 5 0 40754.52 36820.79 467.92 o 3 5 0 14508.33 13731.29 136.32 o 4 5 0 176.26 173.63 6.47 o 5 5 0 614.34 553.58 10.08 o 6 5 0 7.61 0.33 4.00 o 7 5 0 5093.17 5250.59 56.64 o 8 5 0 3107.49 3387.94 40.59 o 9 5 0 2.22 3.43 6.68 o 10 5 0 768.13 634.57 14.74 o 11 5 0 151.79 156.86 9.41 o 12 5 0 4918.16 5027.84 65.56 o 13 5 0 458.49 459.32 19.35 o 14 5 0 388.08 307.32 19.09 o 15 5 0 306.60 405.65 34.48 o 16 5 0 331.92 272.05 50.96 o 0 6 0 70.80 154.94 8.52 o 1 6 0 221.76 255.13 7.05 o 2 6 0 2946.04 3383.54 39.07 o 3 6 0 290.78 308.36 7.56 o 4 6 0 9197.80 9429.54 95.43 o 5 6 0 13138.50 13930.57 149.08 o 6 6 0 8174.41 8050.63 86.14 o 7 6 0 2008.72 2046.91 27.04 o 8 6 0 918.87 972.08 17.38 o 9 6 0 55.82 44.77 6.27 o 10 6 0 3532.87 3293.35 44.38 o 11 6 0 186.98 208.50 13.38 o 12 6 0 541.87 572.92 19.11 o 13 6 0 673.53 648.87 22.38 o 14 6 0 262.12 284.63 20.21 o 15 6 0 28.62 -7.70 27.48 o 16 6 0 66.89 124.26 63.88 o 1 7 0 78392.06 72703.07 852.04 o 2 7 0 9589.67 9904.35 103.09 o 3 7 0 365.65 414.90 9.94 o 4 7 0 94.22 77.82 4.99 o 5 7 0 1487.92 1891.40 24.63 o 6 7 0 982.55 824.98 15.34 o 7 7 0 846.49 819.89 14.41 o 8 7 0 759.51 735.53 14.26 o 9 7 0 68.75 117.67 9.23 o 10 7 0 2419.43 2367.08 35.09 o 11 7 0 1.36 -3.86 10.21 o 12 7 0 886.06 767.25 22.79 o 13 7 0 82.46 115.33 13.74 o 14 7 0 34.56 67.17 21.99 o 15 7 0 21.30 77.94 37.98 o 16 7 0 181.92 128.57 52.69 o 0 8 0 3862.02 3789.86 81.05 o 1 8 0 33.09 29.80 4.57 o 2 8 0 9212.48 8506.72 87.00 o 3 8 0 1578.49 1563.63 21.74 o 4 8 0 1216.43 1185.23 16.91 o 5 8 0 3785.82 4422.85 51.63 o 6 8 0 211.74 137.67 6.82 o 7 8 0 292.13 369.71 10.47 o 8 8 0 15.77 31.61 5.51 o 9 8 0 157.82 163.94 10.21 o 10 8 0 121.46 99.97 10.40 o 11 8 0 858.65 923.58 22.34 o 12 8 0 74.07 98.39 15.91 o 13 8 0 647.98 713.96 24.33 o 14 8 0 272.62 278.95 27.87 o 15 8 0 730.48 750.24 53.20 o 16 8 0 131.71 130.05 99.02 o 1 9 0 858.71 865.69 14.31 o 2 9 0 808.51 971.43 15.35 o 3 9 0 5027.21 5272.63 58.27 o 4 9 0 2851.92 2903.16 35.05 o 5 9 0 395.94 369.28 12.28 o 6 9 0 717.14 793.64 16.77 o 7 9 0 5197.64 5544.70 73.29 o 8 9 0 895.45 930.42 19.34 o 9 9 0 2603.74 2495.40 39.61 o 10 9 0 45.72 24.79 9.71 o 11 9 0 125.66 129.59 11.62 o 12 9 0 219.15 262.46 17.87 o 13 9 0 444.51 442.97 29.57 o 14 9 0 52.02 39.53 22.30 o 15 9 0 1296.41 1377.24 77.34 o 0 10 0 4106.64 4599.97 70.90 o 1 10 0 460.00 461.66 11.36 o 2 10 0 18.78 11.58 4.88 o 3 10 0 2039.04 2149.35 26.97 o 4 10 0 105.79 98.76 7.23 o 5 10 0 4236.23 4315.86 46.69 o 6 10 0 6135.57 6481.04 74.56 o 7 10 0 3931.88 3914.14 48.55 o 8 10 0 32.76 14.26 6.64 o 9 10 0 60.54 12.82 9.00 o 10 10 0 6.87 -5.76 9.41 o 11 10 0 765.87 801.75 22.03 o 12 10 0 525.63 604.43 31.85 o 13 10 0 8.95 21.29 22.56 o 14 10 0 169.07 180.86 36.57 o 15 10 0 209.68 195.33 44.87 o 1 11 0 4509.29 4330.38 58.08 o 2 11 0 3708.98 3761.69 42.88 o 3 11 0 4905.54 4881.05 57.70 o 4 11 0 8675.72 8507.31 103.27 o 5 11 0 72.69 59.88 7.17 o 6 11 0 2078.15 1826.94 26.63 o 7 11 0 147.70 130.23 8.80 o 8 11 0 5491.31 5451.25 65.67 o 9 11 0 235.71 237.90 12.77 o 10 11 0 93.78 101.23 11.71 o 11 11 0 212.51 171.49 14.74 o 12 11 0 148.85 114.51 19.20 o 13 11 0 63.66 25.47 36.24 o 14 11 0 115.73 69.63 35.26 o 15 11 0 450.45 518.39 53.23 o 0 12 0 22831.61 24146.77 339.78 o 1 12 0 604.92 549.70 16.00 o 2 12 0 12137.47 11517.62 118.21 o 3 12 0 1339.73 1239.32 19.75 o 4 12 0 10381.43 10590.25 113.97 o 5 12 0 7272.71 7507.54 80.08 o 6 12 0 2145.23 2168.76 30.81 o 7 12 0 308.69 357.31 13.18 o 8 12 0 3865.97 3986.67 53.97 o 9 12 0 358.98 394.24 17.30 o 10 12 0 1937.03 1885.50 37.41 o 11 12 0 2758.12 2666.42 48.63 o 12 12 0 1348.61 1481.84 46.22 o 13 12 0 1193.08 1227.25 45.27 o 14 12 0 813.44 654.23 48.20 o 15 12 0 351.01 315.26 54.86 o 1 13 0 10524.85 10192.40 113.75 o 2 13 0 6098.37 6142.69 68.93 o 3 13 0 10155.81 10404.08 120.11 o 4 13 0 3369.60 3728.40 44.36 o 5 13 0 25.85 -3.67 7.58 o 6 13 0 306.37 330.84 12.57 o 7 13 0 3.99 14.37 8.57 o 8 13 0 77.89 89.05 10.22 o 9 13 0 441.98 487.05 15.06 o 10 13 0 2.00 3.36 12.47 o 11 13 0 2724.64 2616.96 47.62 o 12 13 0 264.66 304.45 32.01 o 13 13 0 70.64 64.34 33.32 o 14 13 0 4200.02 4176.46 117.24 o 0 14 0 1482.41 1424.86 31.97 o 1 14 0 68.83 86.88 7.89 o 2 14 0 1633.20 1609.24 24.43 o 3 14 0 5696.02 5705.74 63.52 o 4 14 0 629.37 556.80 15.30 o 5 14 0 2762.64 2690.55 35.64 o 6 14 0 42.03 26.86 8.77 o 7 14 0 2565.92 2564.04 38.70 o 8 14 0 3859.38 3843.63 55.07 o 9 14 0 1009.15 1044.14 24.39 o 10 14 0 2271.03 2092.40 42.72 o 11 14 0 92.73 106.77 21.56 o 12 14 0 851.25 968.74 40.24 o 13 14 0 450.97 453.64 44.29 o 14 14 0 518.31 531.20 49.73 o 1 15 0 1117.71 1117.03 21.04 o 2 15 0 89.90 69.12 8.62 o 3 15 0 3386.97 3209.73 40.37 o 4 15 0 1643.56 1444.10 24.34 o 5 15 0 663.55 670.51 17.10 o 6 15 0 2944.95 2937.65 38.86 o 7 15 0 2648.85 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53.84 o 1 24 0 225.89 240.59 20.90 o 2 24 0 2685.06 2744.15 59.09 o 3 24 0 907.77 854.33 34.29 o 4 24 0 255.81 338.18 26.18 o 5 24 0 1597.58 1706.06 48.08 o 6 24 0 76.65 21.17 29.77 o 7 24 0 753.32 852.11 44.77 o 8 24 0 293.22 258.13 51.65 o 1 25 0 617.75 622.98 29.47 o 2 25 0 142.99 179.92 21.09 o 3 25 0 298.46 364.03 28.67 o 4 25 0 78.59 148.68 26.64 o 5 25 0 558.13 593.87 54.08 o 6 25 0 1836.91 1956.67 68.53 o 7 25 0 1.35 -2.48 59.75 o 0 26 0 1136.32 1248.11 87.63 o 1 26 0 33.93 28.45 34.60 o 2 26 0 562.17 542.99 44.13 o 3 26 0 1130.65 1129.15 54.68 o 4 26 0 3.52 33.33 36.16 o 5 26 0 443.50 464.03 74.64 o 6 26 0 9.59 48.48 47.90 o 1 27 0 1399.06 1331.06 64.69 o 2 27 0 345.39 393.42 45.91 o 3 27 0 7.79 -40.37 40.37 o 4 27 0 361.30 437.49 80.08 o 0 28 0 746.97 648.52 85.90 o 1 28 0 6.72 101.95 51.50 o -16 1 1 781.20 675.92 44.64 o -15 1 1 1367.92 1361.04 70.65 o -14 1 1 750.46 714.32 25.05 o -13 1 1 105.53 70.67 12.63 o -12 1 1 589.85 539.85 22.38 o -11 1 1 1629.59 1598.38 26.75 o -10 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