#------------------------------------------------------------------------------ #$Date: 2018-02-24 09:21:13 +0200 (Sat, 24 Feb 2018) $ #$Revision: 206644 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/02/10/2021037.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2021037 _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 9.8015 _cell_length_b 20.9572 _cell_length_c 21.7012 _exptl_crystal_F_000 1600.00 _reflns_d_resolution_high 0.7354 _cod_data_source_file sk3681Isup2.hkl _cod_data_source_block I _shelx_title ' exp_1418 in P 21 21 21' _shelx_refln_list_code 4 _shelx_f_calc_maximum 321.88 _shelx_f_squared_multiplier 1.000 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x+1/2, -y, z+1/2' 'x+1/2, -y+1/2, -z' '-x, y+1/2, -z+1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 2029.19 2853.63 115.59 o 4 0 0 89.59 65.36 10.94 o 6 0 0 1528.94 1325.15 61.82 o 8 0 0 7.77 10.78 29.59 o 10 0 0 1075.54 1101.26 200.26 o 12 0 0 147.54 277.23 124.58 o 2 1 0 23141.99 15857.12 3383.48 o 3 1 0 4126.78 3847.49 154.06 o 4 1 0 38.19 73.06 12.23 o 5 1 0 560.90 508.66 33.73 o 6 1 0 509.08 465.61 38.14 o 7 1 0 9.53 50.52 14.30 o 8 1 0 59.26 80.76 26.81 o 9 1 0 152.31 321.21 113.03 o 10 1 0 198.10 163.17 64.95 o 11 1 0 189.14 302.66 84.07 o 12 1 0 1.46 -34.45 49.22 o 2 2 0 103604.52 129188.80 2626.81 o 3 2 0 22177.53 25594.95 534.49 o 4 2 0 840.85 675.34 83.81 o 5 2 0 8345.16 7276.83 649.60 o 6 2 0 37.92 163.67 50.81 o 7 2 0 297.03 283.13 24.13 o 8 2 0 177.23 174.92 27.06 o 9 2 0 415.42 349.39 112.52 o 10 2 0 8.67 -58.94 58.94 o 11 2 0 16.59 -58.88 58.88 o 12 2 0 19.09 26.64 152.28 o 2 3 0 74.02 89.69 15.87 o 3 3 0 1914.49 2586.81 231.65 o 4 3 0 2690.67 2631.62 124.52 o 5 3 0 3622.47 3601.49 230.93 o 6 3 0 2324.58 2099.51 66.84 o 7 3 0 676.18 746.19 44.46 o 8 3 0 93.36 100.28 24.10 o 9 3 0 316.98 262.18 73.47 o 10 3 0 1239.68 1691.25 254.92 o 11 3 0 40.89 88.26 83.16 o 12 3 0 50.61 99.99 66.22 o 0 4 0 3444.03 9860.33 302.44 o 1 4 0 3844.08 2317.42 81.18 o 2 4 0 14855.83 18886.71 551.25 o 3 4 0 2231.19 3156.49 96.97 o 4 4 0 3429.99 3127.69 157.18 o 5 4 0 24277.11 25195.57 377.13 o 6 4 0 1789.86 1733.49 73.57 o 7 4 0 18.35 38.02 12.93 o 8 4 0 13.19 96.99 47.36 o 9 4 0 101.34 145.46 52.00 o 10 4 0 110.92 23.11 65.86 o 11 4 0 76.91 125.85 86.98 o 12 4 0 40.62 101.91 96.55 o 1 5 0 1097.73 1393.85 71.97 o 2 5 0 20.10 721.39 35.69 o 3 5 0 650.07 961.13 45.48 o 4 5 0 473.43 579.35 121.22 o 5 5 0 1295.39 1307.61 60.24 o 6 5 0 31.81 56.90 13.26 o 7 5 0 935.48 1108.27 58.52 o 8 5 0 167.01 197.97 52.66 o 9 5 0 884.31 1012.32 119.79 o 10 5 0 5.22 39.44 48.30 o 11 5 0 220.09 242.71 116.58 o 12 5 0 4.72 -42.37 83.54 o 0 6 0 33162.88 42546.16 869.61 o 1 6 0 491.69 1027.92 45.60 o 2 6 0 379.67 331.01 29.27 o 3 6 0 17.24 109.03 17.81 o 4 6 0 1423.91 1538.52 64.35 o 5 6 0 821.43 777.25 54.06 o 6 6 0 3860.83 4144.72 110.52 o 7 6 0 34.06 27.06 11.64 o 8 6 0 415.97 616.12 93.33 o 9 6 0 6.62 67.98 43.23 o 10 6 0 80.84 350.00 123.79 o 11 6 0 12.48 -35.39 71.34 o 1 7 0 4.73 -9.41 17.29 o 2 7 0 168.47 301.56 30.29 o 3 7 0 1669.49 1342.56 62.45 o 4 7 0 2411.19 2359.19 104.32 o 5 7 0 221.49 174.80 34.32 o 6 7 0 2218.85 2148.32 85.99 o 7 7 0 293.13 342.14 35.58 o 8 7 0 3.56 30.16 33.14 o 9 7 0 41.89 105.26 46.73 o 10 7 0 582.89 606.40 152.63 o 11 7 0 182.60 322.82 145.34 o 0 8 0 2525.58 2963.18 142.70 o 1 8 0 1491.69 1782.11 95.93 o 2 8 0 275.31 446.37 40.39 o 3 8 0 349.39 382.18 45.99 o 4 8 0 1311.89 1455.02 87.40 o 5 8 0 1227.35 1143.70 62.43 o 6 8 0 944.21 837.50 74.05 o 7 8 0 96.44 85.06 26.85 o 8 8 0 16.96 36.22 39.07 o 9 8 0 183.08 321.09 156.02 o 10 8 0 8.28 150.68 93.71 o 11 8 0 54.48 157.46 105.99 o 1 9 0 5722.43 5811.71 256.21 o 2 9 0 1737.92 1917.40 86.02 o 3 9 0 361.31 446.53 50.71 o 4 9 0 1224.01 1405.44 89.92 o 5 9 0 659.38 702.09 63.91 o 6 9 0 1760.94 1850.78 113.35 o 7 9 0 302.77 285.81 46.29 o 8 9 0 2.35 2.66 47.92 o 9 9 0 144.31 247.97 75.29 o 10 9 0 393.44 614.37 108.98 o 11 9 0 20.77 -5.03 52.62 o 0 10 0 2336.69 2125.16 134.57 o 1 10 0 345.97 315.13 40.12 o 2 10 0 4722.61 5358.25 192.81 o 3 10 0 817.94 843.01 74.14 o 4 10 0 1900.19 1820.83 107.17 o 5 10 0 417.48 382.83 51.31 o 6 10 0 18.18 29.18 31.81 o 7 10 0 2.55 -12.54 28.20 o 8 10 0 160.44 85.20 40.89 o 9 10 0 314.74 277.04 69.50 o 10 10 0 158.80 279.50 99.18 o 11 10 0 0.04 -95.48 95.48 o 1 11 0 5782.78 6075.15 174.79 o 2 11 0 3014.42 3133.56 136.73 o 3 11 0 64.10 33.54 20.69 o 4 11 0 241.47 221.63 43.03 o 5 11 0 1044.91 1101.96 86.66 o 6 11 0 181.50 115.18 77.87 o 7 11 0 636.63 583.91 83.06 o 8 11 0 37.95 52.56 54.43 o 9 11 0 264.54 330.84 82.71 o 10 11 0 98.72 160.04 128.03 o 11 11 0 396.82 194.51 109.85 o 0 12 0 5086.04 5287.48 293.05 o 1 12 0 2389.92 2418.95 113.57 o 2 12 0 165.14 113.80 27.07 o 3 12 0 3.91 -2.24 24.27 o 4 12 0 3886.28 3921.48 176.49 o 5 12 0 994.56 980.18 86.67 o 6 12 0 151.78 103.52 64.39 o 7 12 0 195.54 191.63 54.01 o 8 12 0 1977.62 1669.34 242.61 o 9 12 0 9.28 0.00 45.21 o 10 12 0 172.82 150.62 93.34 o 1 13 0 1318.86 1548.64 92.46 o 2 13 0 15.35 37.78 23.31 o 3 13 0 63.93 58.98 32.86 o 4 13 0 2072.55 2182.86 142.01 o 5 13 0 982.25 956.93 88.35 o 6 13 0 923.83 938.66 90.52 o 7 13 0 744.68 756.40 106.36 o 8 13 0 73.50 253.97 106.36 o 9 13 0 4.49 -74.06 74.06 o 10 13 0 152.26 209.29 91.00 o 0 14 0 20.25 26.61 37.18 o 1 14 0 3182.68 2906.48 133.39 o 2 14 0 184.14 128.03 27.75 o 3 14 0 1176.19 1234.38 125.73 o 4 14 0 669.69 627.96 77.23 o 5 14 0 5223.16 5507.42 225.96 o 6 14 0 267.06 277.69 49.30 o 7 14 0 18.96 134.85 56.08 o 8 14 0 266.17 183.23 91.93 o 9 14 0 6.17 118.78 76.74 o 10 14 0 96.54 147.75 68.49 o 1 15 0 173.93 180.97 39.10 o 2 15 0 2288.34 2191.56 119.45 o 3 15 0 17.88 37.99 35.43 o 4 15 0 192.97 200.95 50.01 o 5 15 0 318.38 282.16 54.21 o 6 15 0 1754.41 1682.53 129.74 o 7 15 0 674.52 753.28 108.85 o 8 15 0 133.01 86.31 78.91 o 9 15 0 258.42 257.24 117.56 o 10 15 0 99.61 162.09 108.93 o 0 16 0 2616.08 2495.58 241.86 o 1 16 0 150.85 106.01 32.09 o 2 16 0 508.70 467.22 59.99 o 3 16 0 3516.48 3818.92 197.37 o 4 16 0 3081.09 2870.35 171.46 o 5 16 0 678.64 791.25 89.66 o 6 16 0 249.94 295.56 57.96 o 7 16 0 20.04 58.94 40.02 o 8 16 0 2.70 -6.25 53.46 o 9 16 0 79.82 175.71 96.02 o 10 16 0 110.86 197.06 107.32 o 1 17 0 1453.09 1423.50 103.20 o 2 17 0 155.33 210.82 45.69 o 3 17 0 192.47 192.04 52.19 o 4 17 0 984.13 945.55 101.51 o 5 17 0 4.21 -41.74 41.74 o 6 17 0 254.03 243.54 52.83 o 7 17 0 2.54 51.56 35.02 o 8 17 0 153.98 232.46 112.47 o 9 17 0 502.37 504.52 173.10 o 10 17 0 2.70 -94.20 94.20 o 0 18 0 2875.70 2855.50 220.10 o 1 18 0 1045.73 1160.49 97.34 o 2 18 0 331.42 325.76 54.92 o 3 18 0 50.40 25.82 46.50 o 4 18 0 655.52 705.09 89.22 o 5 18 0 4.30 3.08 35.96 o 6 18 0 437.61 410.46 74.28 o 7 18 0 5.64 -1.05 26.09 o 8 18 0 145.32 116.89 94.74 o 9 18 0 5.26 18.47 56.70 o 1 19 0 18.17 34.28 55.13 o 2 19 0 12.07 5.26 33.69 o 3 19 0 194.37 180.16 46.38 o 4 19 0 88.96 20.61 45.02 o 5 19 0 52.14 -25.54 32.78 o 6 19 0 374.45 345.11 63.92 o 7 19 0 274.23 469.09 158.55 o 8 19 0 43.64 143.50 87.20 o 9 19 0 62.68 86.83 91.95 o 0 20 0 24.29 33.28 39.25 o 1 20 0 522.95 596.74 72.92 o 2 20 0 5.42 -22.34 33.37 o 3 20 0 28.35 45.86 32.85 o 4 20 0 10.67 -14.70 49.82 o 5 20 0 1091.65 1201.99 126.14 o 6 20 0 63.10 54.58 95.02 o 7 20 0 17.65 32.63 59.78 o 8 20 0 18.01 119.79 94.90 o 1 21 0 3.93 -26.56 35.26 o 2 21 0 356.89 455.77 82.64 o 3 21 0 8.23 -2.40 43.97 o 4 21 0 86.50 76.75 32.86 o 5 21 0 10.19 18.33 35.55 o 6 21 0 132.72 154.76 43.97 o 7 21 0 31.38 8.04 57.51 o 0 22 0 1321.94 1591.47 184.39 o 1 22 0 140.07 95.51 44.34 o 2 22 0 172.90 233.19 61.46 o 3 22 0 35.09 63.63 42.31 o 4 22 0 333.23 430.90 82.52 o 5 22 0 17.37 10.07 32.82 o 6 22 0 27.14 11.65 53.06 o 1 23 0 292.68 311.39 61.93 o 2 23 0 199.40 176.12 57.30 o 3 23 0 22.91 20.15 30.41 o 4 23 0 129.63 123.10 42.35 o 5 23 0 146.52 217.20 61.08 o 6 23 0 1.42 -10.33 68.22 o 0 24 0 762.75 824.11 252.54 o 1 24 0 43.40 25.86 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188.70 o -3 1 1 6699.69 7454.55 253.85 o -2 1 1 30717.33 29013.59 1325.23 o 2 1 1 30802.88 31628.43 1746.98 o 3 1 1 6905.58 8056.31 118.54 o 4 1 1 8489.17 7288.91 483.63 o 5 1 1 1079.98 1157.99 54.85 o 6 1 1 1461.22 1409.47 92.08 o 7 1 1 535.53 552.06 41.13 o 8 1 1 1499.70 1757.14 100.29 o 9 1 1 306.26 288.22 110.85 o 10 1 1 135.08 161.67 62.76 o 11 1 1 38.82 14.86 54.06 o 12 1 1 41.43 17.20 36.69 o -12 2 1 97.57 113.61 150.86 o -11 2 1 51.71 39.91 46.06 o -10 2 1 395.58 428.45 128.99 o -9 2 1 657.68 881.88 170.11 o -8 2 1 888.55 826.38 59.42 o -7 2 1 338.13 319.94 29.18 o -6 2 1 33.66 34.58 13.58 o -5 2 1 3529.86 3578.96 201.10 o -4 2 1 8152.93 8160.14 471.04 o -3 2 1 18277.61 19314.01 262.24 o -2 2 1 15341.63 16061.87 249.66 o 2 2 1 14892.21 17304.56 504.84 o 3 2 1 17526.89 19116.57 238.02 o 4 2 1 8684.41 8952.06 246.18 o 5 2 1 3294.11 3149.24 295.44 o 6 2 1 47.69 52.26 30.23 o 7 2 1 429.98 427.98 36.09 o 8 2 1 792.24 802.12 95.96 o 9 2 1 685.82 740.53 95.82 o 10 2 1 390.35 397.18 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2407.26 72.62 o -3 4 1 3996.13 3477.71 135.62 o -2 4 1 3166.90 3878.27 105.56 o -1 4 1 379.05 1053.94 41.71 o 0 4 1 4942.99 3957.34 238.89 o 1 4 1 302.65 744.19 54.42 o 2 4 1 3216.51 4096.99 86.71 o 3 4 1 3686.63 3335.74 396.74 o 4 4 1 2317.06 2696.66 236.66 o 5 4 1 1156.14 1063.81 36.06 o 6 4 1 4496.82 4742.60 281.00 o 7 4 1 735.10 721.44 57.04 o 8 4 1 2232.01 2547.88 177.24 o 9 4 1 32.33 73.44 33.78 o 10 4 1 27.25 88.31 73.95 o 11 4 1 23.86 66.69 44.95 o 12 4 1 37.30 2.44 44.60 o -12 5 1 21.47 -75.96 75.96 o -11 5 1 9.95 81.34 90.63 o -10 5 1 165.54 162.62 76.73 o -9 5 1 47.34 119.16 60.86 o -8 5 1 437.14 641.10 92.70 o -7 5 1 344.26 343.88 33.66 o -6 5 1 761.85 777.50 50.92 o -5 5 1 411.56 437.50 32.52 o -4 5 1 683.05 459.69 32.51 o -3 5 1 2514.58 2598.99 94.64 o -2 5 1 4150.92 4744.28 225.47 o -1 5 1 6342.65 7356.09 177.42 o 0 5 1 2932.30 1339.70 61.11 o 1 5 1 6011.53 6733.18 168.12 o 2 5 1 4323.48 5048.46 109.27 o 3 5 1 2414.08 2750.20 136.41 o 4 5 1 692.27 518.40 36.38 o 5 5 1 342.79 336.70 61.66 o 6 5 1 865.25 827.47 72.05 o 7 5 1 297.60 272.01 28.54 o 8 5 1 523.09 598.28 102.23 o 9 5 1 24.31 41.52 92.08 o 10 5 1 126.29 247.06 95.21 o 11 5 1 18.54 109.06 94.36 o 12 5 1 20.85 32.16 61.97 o -11 6 1 101.61 166.39 107.45 o -10 6 1 82.16 205.25 97.47 o -9 6 1 346.25 421.39 78.96 o -8 6 1 287.48 375.63 76.38 o -7 6 1 695.56 713.70 67.83 o -6 6 1 283.89 282.65 34.35 o -5 6 1 2232.50 2245.78 93.37 o -4 6 1 1335.30 1519.36 76.60 o -3 6 1 1434.69 1544.43 63.52 o -2 6 1 2300.58 2978.01 179.15 o -1 6 1 906.77 1204.92 55.92 o 0 6 1 3288.61 2970.70 117.86 o 1 6 1 856.87 1163.61 47.67 o 2 6 1 2293.01 3220.17 169.29 o 3 6 1 1450.96 1501.91 67.82 o 4 6 1 1301.73 1342.31 75.48 o 5 6 1 2241.20 2123.18 233.30 o 6 6 1 271.64 250.87 17.57 o 7 6 1 678.31 645.92 64.40 o 8 6 1 276.46 433.07 77.60 o 9 6 1 421.45 565.04 96.30 o 10 6 1 85.48 144.88 80.26 o 11 6 1 92.56 36.28 68.71 o -11 7 1 34.44 120.43 102.81 o -10 7 1 52.65 126.12 88.81 o -9 7 1 181.53 268.84 69.35 o -8 7 1 297.88 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