#------------------------------------------------------------------------------ #$Date: 2018-02-24 09:21:13 +0200 (Sat, 24 Feb 2018) $ #$Revision: 206644 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/02/10/2021038.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2021038 _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 28.5958 _cell_length_b 28.5958 _cell_length_c 13.5438 _exptl_crystal_F_000 3200.00 _reflns_d_resolution_high 0.7361 _cod_data_source_file sk3681IIsup3.hkl _cod_data_source_block II _shelx_title ' exp_1588 in I-4' _shelx_refln_list_code 4 _shelx_f_calc_maximum 587.54 _shelx_f_squared_multiplier 1.000 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, z' 'y, -x, -z' '-y, x, -z' 'x+1/2, y+1/2, z+1/2' '-x+1/2, -y+1/2, z+1/2' 'y+1/2, -x+1/2, -z+1/2' '-y+1/2, x+1/2, -z+1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 4 4 0 4518.30 1932.25 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26580.43 22808.02 677.53 o 5 9 0 23872.67 21991.03 924.83 o 7 9 0 13.32 -394.46 394.46 o 9 9 0 2699.71 2443.88 530.71 o -8 10 0 53.85 -274.37 362.38 o -6 10 0 43.68 31.55 198.82 o -4 10 0 563.19 248.66 151.37 o -2 10 0 2131.71 1785.67 251.06 o 0 10 0 2398.19 2355.91 187.24 o 2 10 0 14304.17 12394.88 496.83 o 4 10 0 3632.26 3504.73 413.41 o 6 10 0 8007.52 9843.29 652.03 o 8 10 0 6759.79 6023.41 866.32 o 10 10 0 1470.45 1617.32 602.29 o -9 11 0 5065.22 4985.04 937.36 o -7 11 0 137.30 299.29 225.33 o -5 11 0 53.04 270.39 301.14 o -3 11 0 7095.20 6234.69 765.58 o -1 11 0 7753.54 6558.48 351.50 o 1 11 0 5750.82 5055.67 403.98 o 3 11 0 6965.93 5987.14 365.82 o 5 11 0 11902.70 10287.42 1336.33 o 7 11 0 97.69 -126.63 158.90 o 9 11 0 453.08 284.97 211.01 o 11 11 0 8450.53 8598.24 1214.12 o -10 12 0 390.20 789.18 356.55 o -8 12 0 5046.74 5205.87 930.21 o -6 12 0 230.36 620.58 301.14 o -4 12 0 4182.54 4012.95 702.76 o -2 12 0 6157.08 6763.11 569.95 o 0 12 0 1709.72 2166.00 251.85 o 2 12 0 8805.24 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2573.17 367.29 o 10 18 0 2166.17 1789.67 389.36 o 12 18 0 233.48 418.93 243.95 o 14 18 0 1486.52 1578.60 378.84 o 16 18 0 28.03 -115.51 216.27 o 18 18 0 391.32 1021.71 389.50 o -17 19 0 569.03 592.87 225.63 o -15 19 0 882.19 723.70 263.24 o -13 19 0 79.59 346.74 479.55 o -11 19 0 5010.82 5344.51 1223.13 o -9 19 0 136.23 32.34 318.64 o -7 19 0 3450.07 3830.04 945.32 o -5 19 0 6.29 -171.78 171.78 o -3 19 0 220.55 263.50 307.11 o -1 19 0 355.06 349.92 159.85 o 1 19 0 261.98 158.79 315.19 o 3 19 0 113.67 112.52 385.71 o 5 19 0 938.56 870.55 179.44 o 7 19 0 4641.52 4615.99 450.83 o 9 19 0 9744.99 7978.01 606.16 o 11 19 0 276.84 184.00 311.48 o 13 19 0 12027.09 11615.62 1069.18 o 15 19 0 118.38 -40.44 214.92 o 17 19 0 257.64 420.99 458.34 o 19 19 0 185.62 233.85 828.54 o -18 20 0 1.32 -122.96 348.99 o -16 20 0 860.30 1176.48 395.25 o -14 20 0 1754.40 2687.23 1049.50 o -12 20 0 44.44 213.40 603.88 o -10 20 0 2553.27 2891.09 868.70 o -8 20 0 7339.16 7783.35 1363.10 o -6 20 0 3028.91 3662.56 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