#------------------------------------------------------------------------------ #$Date: 2018-07-31 05:13:51 +0300 (Tue, 31 Jul 2018) $ #$Revision: 209309 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/02/11/2021193.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2021193 _cell_angle_alpha 80.516 _cell_angle_beta 77.366 _cell_angle_gamma 63.826 _cell_length_a 6.3129 _cell_length_b 6.9099 _cell_length_c 13.0901 _exptl_crystal_F_000 244.00 _reflns_d_resolution_high 0.7967 _cod_data_source_file qp3012IIsup3.hkl _cod_data_source_block II _shelx_title ' bt in P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 113.07 _shelx_f_squared_multiplier 1.000 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 202.29 208.76 1.54 o 2 0 0 11.99 10.39 0.38 o 3 0 0 56.69 68.16 2.13 o 4 0 0 253.64 243.66 2.36 o 5 0 0 969.77 974.97 13.01 o 6 0 0 111.36 109.79 3.50 o 7 0 0 43.97 44.89 2.25 o -5 1 0 40.02 43.61 1.33 o -4 1 0 1.89 2.74 0.60 o -3 1 0 393.62 379.90 3.90 o -2 1 0 264.61 275.54 2.27 o -1 1 0 535.72 544.85 3.82 o 0 1 0 149.70 145.57 1.12 o 1 1 0 99.90 96.80 1.40 o 2 1 0 162.43 173.61 2.69 o 3 1 0 1916.66 2014.19 11.51 o 4 1 0 60.70 61.12 0.84 o 5 1 0 49.68 48.91 1.33 o 6 1 0 50.08 57.42 2.74 o 7 1 0 135.22 136.76 4.33 o -4 2 0 1215.56 1211.40 8.88 o -3 2 0 37.56 34.35 0.92 o -2 2 0 20.57 25.18 0.52 o -1 2 0 1059.40 1101.15 6.42 o 0 2 0 245.83 252.12 1.98 o 1 2 0 3934.19 4012.01 22.67 o 2 2 0 515.01 524.74 6.38 o 3 2 0 297.37 280.79 2.84 o 4 2 0 43.59 37.39 0.87 o 5 2 0 35.49 35.65 1.06 o 6 2 0 62.66 64.43 2.75 o 7 2 0 276.55 278.63 6.31 o -5 3 0 77.18 75.31 3.34 o -4 3 0 168.47 170.49 1.97 o -3 3 0 9.46 10.22 0.60 o -2 3 0 179.52 172.50 1.77 o -1 3 0 514.65 522.05 3.35 o 0 3 0 823.26 811.44 5.73 o 1 3 0 55.69 59.74 0.70 o 2 3 0 722.56 741.26 4.56 o 3 3 0 526.48 533.22 4.05 o 4 3 0 506.71 495.22 3.95 o 5 3 0 76.56 80.51 3.07 o 6 3 0 46.53 45.62 2.53 o 7 3 0 74.22 76.61 3.41 o -4 4 0 77.28 80.00 1.59 o -3 4 0 427.52 422.80 3.76 o -2 4 0 122.35 114.36 1.58 o -1 4 0 306.78 290.89 2.69 o 0 4 0 127.72 132.33 1.57 o 1 4 0 331.20 314.96 2.26 o 2 4 0 241.08 234.84 1.87 o 3 4 0 1416.56 1399.90 9.75 o 4 4 0 110.15 110.33 1.47 o 5 4 0 7.80 7.33 1.25 o 6 4 0 15.25 15.25 2.97 o 7 4 0 8.46 6.35 2.09 o -3 5 0 120.33 125.00 2.01 o -2 5 0 10.49 9.00 1.34 o -1 5 0 28.26 26.34 1.35 o 0 5 0 161.24 150.91 1.92 o 1 5 0 159.71 146.63 1.83 o 2 5 0 24.87 21.56 1.14 o 3 5 0 67.00 56.47 1.63 o 4 5 0 91.20 98.69 1.52 o 5 5 0 5.23 5.70 1.00 o 6 5 0 208.86 222.20 3.66 o 7 5 0 10.99 13.11 3.26 o -2 6 0 70.92 72.99 1.74 o -1 6 0 126.37 117.70 2.74 o 0 6 0 93.45 90.15 1.78 o 1 6 0 6.69 5.59 0.81 o 2 6 0 143.26 139.00 1.99 o 3 6 0 2.00 3.02 0.95 o 4 6 0 295.02 296.98 3.75 o 5 6 0 196.48 214.01 3.28 o 6 6 0 96.15 97.59 2.49 o 7 6 0 12.88 15.45 2.52 o -1 7 0 83.29 87.88 2.03 o 0 7 0 20.22 20.78 1.29 o 1 7 0 17.46 16.99 1.31 o 2 7 0 17.96 19.46 1.49 o 3 7 0 65.04 65.23 2.02 o 4 7 0 162.37 166.37 2.94 o 5 7 0 116.09 113.65 3.78 o 6 7 0 25.11 29.25 4.09 o 1 8 0 14.55 15.10 1.46 o 2 8 0 74.99 75.53 2.73 o 3 8 0 17.07 18.35 2.39 o 4 8 0 20.76 23.39 2.73 o 5 8 0 19.20 20.89 2.58 o -5 -8 1 80.30 73.45 3.74 o -4 -8 1 5.44 5.40 2.36 o -3 -8 1 4.89 5.98 2.33 o -2 -8 1 60.16 65.75 2.69 o -1 -8 1 99.94 104.12 2.32 o -6 -7 1 126.25 141.12 5.38 o -5 -7 1 11.16 9.11 2.68 o -4 -7 1 7.90 8.64 1.95 o -3 -7 1 1.53 1.62 1.15 o -2 -7 1 39.62 40.75 3.48 o -1 -7 1 20.52 19.97 1.32 o 0 -7 1 5.80 6.41 1.11 o 1 -7 1 44.01 47.93 1.70 o -7 -6 1 65.41 68.75 3.71 o -6 -6 1 279.13 290.76 4.20 o -5 -6 1 107.67 111.39 4.48 o -4 -6 1 2.13 1.25 2.01 o -3 -6 1 1.54 1.78 1.68 o -2 -6 1 96.46 98.79 1.72 o -1 -6 1 134.20 132.52 1.96 o 0 -6 1 112.44 111.66 1.96 o 1 -6 1 53.75 54.60 1.93 o 2 -6 1 5.89 6.51 1.08 o -7 -5 1 3.37 2.25 3.24 o -6 -5 1 27.27 29.52 2.22 o -5 -5 1 43.17 45.06 1.64 o -4 -5 1 3.20 3.25 0.67 o -3 -5 1 82.66 84.25 1.86 o -2 -5 1 248.73 244.55 2.59 o -1 -5 1 15.88 16.46 0.82 o 0 -5 1 0.02 0.10 0.58 o 1 -5 1 385.90 379.02 3.60 o 2 -5 1 103.94 101.39 1.89 o 3 -5 1 114.75 106.61 1.89 o -7 -4 1 15.67 14.32 2.40 o -6 -4 1 72.95 77.02 3.67 o -5 -4 1 331.16 325.90 4.06 o -4 -4 1 231.87 237.64 2.35 o -3 -4 1 279.06 262.78 2.41 o -2 -4 1 0.25 0.32 0.35 o -1 -4 1 294.09 293.72 2.19 o 0 -4 1 453.05 453.82 3.69 o 1 -4 1 258.83 256.65 2.50 o 2 -4 1 224.20 213.21 2.28 o 3 -4 1 136.31 132.64 1.88 o 4 -4 1 70.81 67.97 1.71 o -7 -3 1 6.17 4.66 2.03 o -6 -3 1 31.95 32.61 1.57 o -5 -3 1 200.52 202.93 4.47 o -4 -3 1 0.27 0.74 0.67 o -3 -3 1 727.10 695.22 8.44 o -2 -3 1 42.80 42.24 0.68 o -1 -3 1 185.13 192.80 1.49 o 0 -3 1 76.28 83.90 0.87 o 1 -3 1 188.56 212.07 1.64 o 2 -3 1 532.70 519.94 3.55 o 3 -3 1 8.88 9.17 0.56 o 4 -3 1 80.89 84.16 1.28 o 5 -3 1 185.29 190.74 2.51 o -7 -2 1 73.04 71.41 3.85 o -6 -2 1 30.53 27.84 2.14 o -5 -2 1 281.19 284.86 3.60 o -4 -2 1 818.19 840.47 6.15 o -3 -2 1 807.68 813.11 7.01 o -2 -2 1 757.51 748.24 8.72 o -1 -2 1 661.91 650.75 3.90 o 0 -2 1 0.14 0.43 0.18 o 1 -2 1 914.83 923.59 10.50 o 2 -2 1 395.23 389.45 4.73 o 3 -2 1 817.76 817.36 5.10 o 4 -2 1 1.61 1.56 0.70 o 5 -2 1 123.26 116.52 3.75 o -7 -1 1 63.42 65.73 3.49 o -6 -1 1 147.73 143.77 3.87 o -5 -1 1 35.56 35.27 1.67 o -4 -1 1 52.58 46.14 0.77 o -3 -1 1 64.25 87.95 0.89 o -2 -1 1 1837.86 1886.86 22.09 o -1 -1 1 1945.35 1815.35 20.83 o 0 -1 1 1079.16 1068.67 6.06 o 1 -1 1 42.39 38.03 0.44 o 2 -1 1 54.98 59.08 0.84 o 3 -1 1 1131.09 1121.38 9.69 o 4 -1 1 438.75 427.93 3.18 o 5 -1 1 10.82 10.95 1.11 o 6 -1 1 92.05 91.55 4.02 o -6 0 1 30.97 34.25 2.53 o -5 0 1 222.30 219.72 4.85 o -4 0 1 125.41 125.00 1.60 o -3 0 1 842.25 840.23 6.06 o -2 0 1 2001.46 2063.71 13.68 o -1 0 1 103.74 94.44 0.58 o 0 0 1 0.28 1.15 0.07 o 1 0 1 19.37 18.62 0.31 o 2 0 1 2723.47 2857.18 18.82 o 3 0 1 69.16 60.24 1.79 o 4 0 1 60.74 60.04 1.09 o 5 0 1 166.88 172.41 2.63 o 6 0 1 67.59 77.29 2.14 o 7 0 1 0.61 0.10 2.22 o -5 1 1 106.22 111.73 1.61 o -4 1 1 15.07 15.75 0.81 o -3 1 1 139.10 134.96 1.62 o -2 1 1 624.33 655.01 4.74 o -1 1 1 1094.25 1130.58 7.59 o 0 1 1 615.01 599.74 3.45 o 1 1 1 551.85 537.60 6.31 o 2 1 1 531.05 537.84 6.51 o 3 1 1 54.37 61.87 0.73 o 4 1 1 27.79 28.02 0.63 o 5 1 1 549.72 548.38 4.53 o 6 1 1 63.35 58.00 2.72 o 7 1 1 11.14 10.67 1.57 o -5 2 1 18.13 16.46 2.00 o -4 2 1 25.82 24.52 1.02 o -3 2 1 64.41 63.40 1.01 o -2 2 1 211.23 203.59 1.54 o -1 2 1 3309.49 3312.37 18.61 o 0 2 1 30.47 33.36 0.58 o 1 2 1 2661.12 2630.78 14.79 o 2 2 1 1606.60 1607.54 18.28 o 3 2 1 543.55 547.44 4.91 o 4 2 1 425.76 434.27 3.52 o 5 2 1 252.68 250.61 2.50 o 6 2 1 771.73 755.61 11.08 o 7 2 1 51.72 59.49 3.57 o -5 3 1 29.54 28.93 2.43 o -4 3 1 54.86 58.70 1.22 o -3 3 1 2.64 1.66 0.51 o -2 3 1 225.77 228.55 2.14 o -1 3 1 189.98 186.38 1.45 o 0 3 1 207.83 214.58 1.95 o 1 3 1 73.55 66.12 0.71 o 2 3 1 546.92 554.65 3.52 o 3 3 1 30.42 29.96 0.74 o 4 3 1 79.08 87.37 1.26 o 5 3 1 43.24 42.44 1.11 o 6 3 1 87.27 87.11 3.09 o 7 3 1 22.97 29.08 2.59 o -4 4 1 8.84 13.05 0.95 o -3 4 1 65.84 63.20 1.40 o -2 4 1 74.71 79.54 1.36 o -1 4 1 43.32 47.73 1.05 o 0 4 1 872.54 843.59 6.16 o 1 4 1 474.22 445.11 3.57 o 2 4 1 707.69 721.17 4.57 o 3 4 1 29.25 30.04 0.73 o 4 4 1 28.69 26.01 0.85 o 5 4 1 321.07 322.72 3.07 o 6 4 1 101.87 99.60 3.28 o 7 4 1 98.34 106.71 3.83 o -3 5 1 25.00 27.86 1.24 o -2 5 1 69.19 69.06 1.69 o -1 5 1 23.61 24.62 1.33 o 0 5 1 58.74 60.29 1.25 o 1 5 1 499.27 480.26 4.02 o 2 5 1 274.84 265.92 2.69 o 3 5 1 106.03 110.22 2.13 o 4 5 1 44.81 51.25 1.17 o 5 5 1 102.73 107.63 1.67 o 6 5 1 98.73 105.62 3.83 o 7 5 1 39.08 40.81 3.50 o -2 6 1 301.88 296.11 3.31 o -1 6 1 26.69 27.96 1.73 o 0 6 1 28.68 29.49 1.32 o 1 6 1 225.49 209.90 2.45 o 2 6 1 463.31 457.26 4.09 o 3 6 1 137.30 146.16 2.46 o 4 6 1 28.06 32.21 1.57 o 5 6 1 22.24 23.92 1.39 o 6 6 1 74.22 73.71 3.10 o 7 6 1 82.74 89.63 3.82 o -1 7 1 0.66 1.16 1.06 o 0 7 1 50.19 48.92 1.64 o 1 7 1 40.83 37.04 1.49 o 2 7 1 37.94 37.56 1.71 o 3 7 1 24.43 22.70 1.49 o 4 7 1 15.47 17.20 1.45 o 5 7 1 82.40 87.83 3.61 o 6 7 1 30.69 29.89 4.15 o 1 8 1 19.96 19.73 1.44 o 2 8 1 35.77 37.40 2.30 o 3 8 1 113.32 122.94 3.28 o 4 8 1 139.35 141.39 3.06 o 5 8 1 27.34 28.85 2.88 o -4 -8 2 49.00 44.98 3.14 o -3 -8 2 183.36 196.94 5.67 o -2 -8 2 21.49 19.83 2.36 o -6 -7 2 205.64 231.93 6.59 o -5 -7 2 2.26 3.41 2.70 o -4 -7 2 0.94 0.36 1.72 o -3 -7 2 35.61 41.20 1.80 o -2 -7 2 11.12 8.96 3.53 o -1 -7 2 252.29 248.89 3.04 o 0 -7 2 27.35 27.74 1.44 o 1 -7 2 3.57 4.90 1.23 o -6 -6 2 1.24 1.58 1.36 o -5 -6 2 11.27 6.77 3.61 o -4 -6 2 9.01 9.16 2.17 o -3 -6 2 81.95 77.16 2.21 o -2 -6 2 49.10 49.12 1.68 o -1 -6 2 1.47 1.36 0.79 o 0 -6 2 18.73 19.80 1.37 o 1 -6 2 13.44 12.01 1.72 o 2 -6 2 92.10 86.04 1.90 o -7 -5 2 143.47 154.11 5.26 o -6 -5 2 10.23 10.37 2.15 o -5 -5 2 523.98 534.59 5.88 o -4 -5 2 6.64 8.43 0.98 o -3 -5 2 131.89 145.11 1.94 o -2 -5 2 43.42 46.86 1.33 o -1 -5 2 30.34 29.42 1.01 o 0 -5 2 398.51 401.78 3.62 o 1 -5 2 19.16 17.90 1.34 o 2 -5 2 1.36 1.01 1.26 o 3 -5 2 12.68 12.60 1.08 o -7 -4 2 125.40 150.22 4.61 o -6 -4 2 113.31 114.89 4.06 o -5 -4 2 22.50 22.93 1.51 o -4 -4 2 18.76 17.11 1.03 o -3 -4 2 350.39 358.51 3.06 o -2 -4 2 51.84 53.88 0.88 o -1 -4 2 331.67 345.77 2.53 o 0 -4 2 403.00 405.24 3.41 o 1 -4 2 7.57 6.41 0.59 o 2 -4 2 42.95 41.20 2.14 o 3 -4 2 10.43 10.62 1.05 o 4 -4 2 1.61 1.99 0.93 o -7 -3 2 21.89 20.34 2.53 o -6 -3 2 100.15 95.88 2.32 o -5 -3 2 45.20 45.19 3.05 o -4 -3 2 368.63 366.59 4.08 o -3 -3 2 211.49 209.49 3.12 o -2 -3 2 2.08 3.73 0.34 o -1 -3 2 32.01 36.22 0.63 o 0 -3 2 442.04 411.96 2.76 o 1 -3 2 1.05 0.60 0.29 o 2 -3 2 269.24 270.45 2.11 o 3 -3 2 367.69 372.36 3.24 o 4 -3 2 18.98 21.05 1.15 o 5 -3 2 30.24 29.67 1.67 o -7 -2 2 47.73 44.00 3.40 o -6 -2 2 10.76 11.53 2.00 o -5 -2 2 319.37 301.12 3.77 o -4 -2 2 150.92 136.73 2.14 o -3 -2 2 165.44 171.98 1.97 o -2 -2 2 696.35 738.35 6.32 o -1 -2 2 464.77 456.90 2.87 o 0 -2 2 171.92 166.73 1.14 o 1 -2 2 443.75 439.94 3.99 o 2 -2 2 80.42 79.03 1.31 o 3 -2 2 119.53 121.91 1.21 o 4 -2 2 223.54 225.25 1.95 o 5 -2 2 12.77 13.45 1.16 o 6 -2 2 0.31 0.77 3.84 o -7 -1 2 10.65 10.97 2.53 o -6 -1 2 33.95 33.73 2.23 o -5 -1 2 319.53 310.67 3.95 o -4 -1 2 947.73 942.38 6.86 o -3 -1 2 176.19 197.26 1.51 o -2 -1 2 82.68 77.97 1.93 o -1 -1 2 384.35 352.27 3.09 o 0 -1 2 391.87 407.27 2.48 o 1 -1 2 2172.74 2223.25 12.53 o 2 -1 2 195.22 239.00 3.03 o 3 -1 2 134.68 130.98 1.19 o 4 -1 2 468.71 470.09 3.94 o 5 -1 2 35.19 33.76 1.51 o 6 -1 2 0.51 1.61 3.24 o -6 0 2 107.58 107.13 3.56 o -5 0 2 56.21 57.89 3.07 o -4 0 2 528.59 523.04 3.48 o -3 0 2 229.58 234.83 2.97 o -2 0 2 21.70 22.27 0.32 o -1 0 2 1319.18 1238.29 6.91 o 0 0 2 3768.68 3753.92 19.12 o 1 0 2 97.87 94.62 0.81 o 2 0 2 1489.61 1552.92 8.85 o 3 0 2 386.31 371.89 3.32 o 4 0 2 375.48 362.89 2.29 o 5 0 2 312.92 315.91 3.81 o 6 0 2 1.12 0.29 1.08 o 7 0 2 5.51 8.46 2.29 o -5 1 2 1.91 0.35 0.97 o -4 1 2 44.96 46.45 1.15 o -3 1 2 1005.13 972.97 8.77 o -2 1 2 104.76 135.71 1.39 o -1 1 2 755.78 739.23 3.84 o 0 1 2 1644.10 1642.33 9.27 o 1 1 2 264.11 247.02 3.22 o 2 1 2 968.91 968.65 11.32 o 3 1 2 928.10 949.81 5.65 o 4 1 2 2.49 2.60 0.35 o 5 1 2 707.42 667.10 9.00 o 6 1 2 105.14 96.63 3.53 o 7 1 2 2.27 2.50 1.93 o -5 2 2 12.86 12.03 3.26 o -4 2 2 588.64 572.72 5.90 o -3 2 2 398.62 396.36 3.41 o -2 2 2 1048.34 1045.54 13.25 o -1 2 2 292.83 294.34 1.99 o 0 2 2 76.64 74.21 0.68 o 1 2 2 12784.04 12846.14 72.21 o 2 2 2 54.58 53.07 1.42 o 3 2 2 311.89 304.33 3.00 o 4 2 2 98.42 84.89 1.20 o 5 2 2 14.28 15.70 0.99 o 6 2 2 36.32 37.92 2.72 o 7 2 2 16.24 16.26 2.83 o -5 3 2 59.10 60.90 4.67 o -4 3 2 22.36 23.95 1.01 o -3 3 2 0.67 0.07 0.49 o -2 3 2 570.15 569.99 4.37 o -1 3 2 578.71 568.94 3.62 o 0 3 2 46.64 42.66 0.84 o 1 3 2 225.93 239.17 1.71 o 2 3 2 480.59 516.87 3.31 o 3 3 2 0.02 -0.08 0.31 o 4 3 2 2657.46 2598.41 17.47 o 5 3 2 50.75 47.80 1.14 o 6 3 2 275.09 276.28 3.65 o 7 3 2 92.35 88.95 3.44 o -4 4 2 4.71 4.04 0.88 o -3 4 2 665.97 682.33 5.44 o -2 4 2 3.30 3.75 0.62 o -1 4 2 68.06 62.75 1.16 o 0 4 2 85.22 78.95 1.20 o 1 4 2 736.88 715.97 5.32 o 2 4 2 288.68 295.33 2.19 o 3 4 2 16.89 14.74 0.57 o 4 4 2 193.07 180.14 1.95 o 5 4 2 222.11 210.37 2.34 o 6 4 2 33.62 39.11 2.43 o 7 4 2 63.42 60.51 2.89 o -3 5 2 7.00 7.63 0.99 o -2 5 2 9.84 8.42 1.32 o -1 5 2 145.19 149.83 2.12 o 0 5 2 969.98 936.97 7.01 o 1 5 2 98.41 89.79 1.42 o 2 5 2 81.10 76.24 1.79 o 3 5 2 5.71 4.76 1.28 o 4 5 2 24.32 23.03 0.90 o 5 5 2 291.94 293.00 2.98 o 6 5 2 64.70 64.51 2.66 o 7 5 2 23.54 25.58 3.43 o -2 6 2 136.85 134.01 2.20 o -1 6 2 151.38 142.57 4.62 o 0 6 2 241.29 235.17 2.75 o 1 6 2 42.77 38.60 1.24 o 2 6 2 42.26 41.44 1.25 o 3 6 2 2.22 2.13 0.88 o 4 6 2 130.66 124.88 2.34 o 5 6 2 6.82 6.98 0.89 o 6 6 2 41.89 47.20 2.76 o 7 6 2 59.47 60.13 3.26 o -1 7 2 2.35 1.86 1.10 o 0 7 2 50.43 48.69 1.60 o 1 7 2 102.11 99.87 1.95 o 2 7 2 65.68 64.06 1.61 o 3 7 2 154.96 160.91 2.87 o 4 7 2 18.34 20.73 1.50 o 5 7 2 8.24 7.67 1.59 o 1 8 2 51.70 54.44 1.88 o 2 8 2 25.85 27.84 2.19 o 3 8 2 38.46 39.77 2.59 o 4 8 2 113.87 127.14 2.95 o 5 8 2 19.02 17.95 1.78 o -4 -8 3 19.36 19.88 2.70 o -3 -8 3 73.81 79.37 4.50 o -2 -8 3 38.38 40.34 2.65 o -5 -7 3 11.86 11.91 2.94 o -4 -7 3 35.66 37.93 4.41 o -3 -7 3 27.33 28.65 2.47 o -2 -7 3 127.77 133.95 4.89 o -1 -7 3 18.68 17.30 1.41 o 0 -7 3 64.64 64.73 1.87 o 1 -7 3 0.49 0.63 1.23 o -6 -6 3 36.01 38.25 2.05 o -5 -6 3 26.00 27.26 4.02 o -4 -6 3 167.79 163.58 4.23 o -3 -6 3 42.99 46.16 3.18 o -2 -6 3 36.14 37.75 1.56 o -1 -6 3 42.77 39.52 1.33 o 0 -6 3 42.57 46.00 1.57 o 1 -6 3 19.72 20.62 1.78 o 2 -6 3 23.74 26.51 1.38 o -7 -5 3 97.54 101.10 3.28 o -6 -5 3 41.53 42.04 2.40 o -5 -5 3 46.02 47.40 1.78 o -4 -5 3 32.22 27.43 1.35 o -3 -5 3 50.75 57.47 1.84 o -2 -5 3 46.53 47.00 1.36 o -1 -5 3 117.11 110.79 1.67 o 0 -5 3 217.02 209.89 2.38 o 1 -5 3 47.89 46.32 1.53 o 2 -5 3 26.05 26.88 1.45 o 3 -5 3 49.31 47.33 1.79 o -7 -4 3 0.98 0.76 1.97 o -6 -4 3 44.11 46.75 2.51 o -5 -4 3 74.61 75.59 2.11 o -4 -4 3 0.82 0.53 0.77 o -3 -4 3 0.54 0.18 0.48 o -2 -4 3 204.42 191.76 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2.12 o -1 3 13 74.20 78.73 4.54 o 0 3 13 178.27 181.10 2.56 o 1 3 13 97.08 94.49 3.18 o 2 3 13 21.20 24.06 1.48 o 3 3 13 29.90 29.77 1.59 o 4 3 13 27.32 27.77 1.79 o 5 3 13 50.99 57.22 2.23 o 6 3 13 59.46 60.42 1.97 o -1 4 13 64.36 69.31 2.08 o 0 4 13 82.93 89.09 2.55 o 2 4 13 2.09 2.11 3.19 o 3 4 13 29.65 27.57 1.67 o 4 4 13 2.05 1.23 1.25 o 5 4 13 4.89 6.39 1.91 o 6 4 13 20.14 21.43 3.75 o 0 5 13 8.19 12.34 1.80 o 2 5 13 4.61 3.46 2.97 o 3 5 13 14.70 11.68 2.99 o 4 5 13 2.51 3.40 1.97 o 5 5 13 53.20 52.38 2.27 o 2 6 13 48.82 53.31 3.28 o 3 6 13 31.01 26.79 3.85 o 4 6 13 51.62 52.27 3.54 o -1 -3 14 1.36 3.15 2.44 o 0 -3 14 24.65 29.91 3.20 o 1 -3 14 57.81 69.74 4.76 o -2 -2 14 68.48 90.64 3.23 o -1 -2 14 10.75 9.25 1.68 o 0 -2 14 0.04 -0.68 1.99 o 1 -2 14 145.83 140.77 4.64 o 2 -2 14 79.14 79.56 4.17 o -2 -1 14 117.30 116.82 3.35 o -1 -1 14 30.16 29.57 2.30 o 0 -1 14 7.56 11.41 2.26 o 1 -1 14 2.18 1.60 1.67 o 2 -1 14 142.12 149.30 5.04 o 3 -1 14 38.33 40.43 2.41 o -2 0 14 63.52 67.11 2.49 o -1 0 14 5.95 4.69 4.09 o 0 0 14 162.30 154.33 4.35 o 1 0 14 6.26 7.28 1.92 o 2 0 14 69.15 69.42 3.30 o 3 0 14 53.11 62.38 2.20 o 4 0 14 8.58 10.30 1.84 o -2 1 14 14.29 15.50 2.25 o -1 1 14 24.74 23.34 1.38 o 0 1 14 8.24 8.07 2.10 o 1 1 14 7.57 6.37 2.32 o 2 1 14 11.59 9.77 3.09 o 3 1 14 33.99 31.74 1.77 o 4 1 14 52.63 55.47 2.17 o 5 1 14 148.55 147.14 2.79 o -1 2 14 67.56 69.85 2.14 o 0 2 14 78.61 80.98 2.34 o 1 2 14 27.73 29.10 2.42 o 2 2 14 20.64 19.84 2.96 o 3 2 14 184.45 195.92 3.52 o 4 2 14 157.19 158.61 3.10 o 5 2 14 30.45 29.50 2.00 o -1 3 14 6.97 7.45 4.70 o 0 3 14 3.49 3.28 1.47 o 1 3 14 4.85 5.52 2.07 o 2 3 14 10.50 9.97 1.39 o 3 3 14 76.02 72.30 2.16 o 4 3 14 39.42 39.79 2.07 o 5 3 14 8.48 9.35 1.60 o 0 4 14 48.69 49.99 2.23 o 2 4 14 1.28 3.41 2.32 o 3 4 14 0.71 1.09 1.32 o 4 4 14 86.46 83.29 2.46 o 5 4 14 58.06 61.98 2.57 o 2 5 14 39.22 34.36 3.54 o 3 5 14 41.68 45.94 3.69 o 4 5 14 4.23 4.73 2.18 o 0 -2 15 71.31 78.81 3.94 o 1 -2 15 153.57 163.95 5.11 o -1 -1 15 15.80 17.84 3.34 o 0 -1 15 63.96 53.31 3.42 o 1 -1 15 160.18 167.98 4.86 o 2 -1 15 59.61 73.13 4.44 o -1 0 15 7.17 8.45 3.18 o 0 0 15 228.51 223.49 5.50 o 1 0 15 12.89 13.32 2.11 o 2 0 15 0.83 1.28 1.98 o 3 0 15 121.16 129.20 4.50 o -1 1 15 2.01 3.15 1.62 o 0 1 15 71.71 66.91 3.48 o 1 1 15 29.75 35.09 3.24 o 2 1 15 34.78 36.85 3.54 o 3 1 15 354.31 371.32 4.95 o 4 1 15 30.47 33.42 2.09 o 0 2 15 41.74 27.19 2.78 o 1 2 15 306.43 300.79 6.26 o 2 2 15 146.09 141.67 4.86 o 3 2 15 5.76 5.28 2.08 o 4 2 15 27.11 30.87 1.99 o 1 3 15 34.93 37.04 2.95 o 2 3 15 28.74 34.69 2.83 o 3 3 15 13.62 13.92 1.61 o 4 3 15 295.24 316.30 4.73 o 3 4 15 37.25 39.28 2.04 o 4 4 15 0.19 0.11 1.52 o 1 0 16 67.85 74.14 3.81 o 2 0 16 4.62 7.31 2.49 o 0 1 16 164.73 161.19 5.04 o 1 1 16 82.30 80.85 4.03 o 2 1 16 123.61 126.11 5.01 o 3 1 16 0.34 0.42 2.38 o 1 2 16 0.68 1.92 2.31 o 2 2 16 176.83 168.75 5.41 o 3 2 16 10.77 14.89 3.56 o 2 3 16 84.18 93.89 4.01 o 3 3 16 86.62 83.19 3.99 o