#------------------------------------------------------------------------------ #$Date: 2019-02-14 05:35:50 +0200 (Thu, 14 Feb 2019) $ #$Revision: 213637 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/02/14/2021488.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2021488 _cell_angle_alpha 95.774 _cell_angle_beta 92.199 _cell_angle_gamma 113.630 _cell_length_a 11.4402 _cell_length_b 13.4019 _cell_length_c 18.6407 _exptl_crystal_F_000 1088.00 _reflns_d_resolution_high 0.8396 _cod_data_source_file jx3027IV_DABCOsup5.hkl _cod_data_source_block IV_DABCO _shelx_title ' DABCO_NEW_a.res in P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 397.10 _shelx_f_squared_multiplier 1.000 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 15007.63 14821.43 186.21 o 2 0 0 1007.68 908.80 18.48 o 3 0 0 379.77 410.83 8.20 o 4 0 0 575.83 569.81 14.06 o 5 0 0 3598.98 3443.98 65.64 o 6 0 0 175.65 197.60 10.83 o 7 0 0 13.76 5.82 5.62 o 8 0 0 287.13 239.11 13.88 o 9 0 0 3011.01 2860.48 66.24 o 10 0 0 1050.72 1156.64 37.51 o 11 0 0 5.41 29.14 19.56 o 12 0 0 2.69 -11.25 11.25 o -12 1 0 33.96 25.12 13.43 o -11 1 0 297.25 425.78 28.54 o -10 1 0 35.96 15.98 12.56 o -9 1 0 4.09 7.34 13.89 o -8 1 0 225.84 192.53 12.46 o -7 1 0 5.89 14.01 5.62 o -6 1 0 352.39 297.58 11.48 o -5 1 0 127.00 114.75 6.91 o -4 1 0 493.37 395.83 10.99 o -3 1 0 650.76 733.84 14.01 o -2 1 0 98.35 80.41 3.05 o -1 1 0 604.48 570.82 8.42 o 0 1 0 703.74 785.69 27.25 o 1 1 0 506.50 430.15 6.90 o 2 1 0 1185.69 1213.99 17.68 o 3 1 0 798.53 839.25 13.29 o 4 1 0 581.64 559.12 16.62 o 5 1 0 1487.52 1500.01 31.96 o 6 1 0 704.98 623.03 17.85 o 7 1 0 132.68 114.25 9.86 o 8 1 0 3.69 10.95 9.63 o 9 1 0 179.24 247.80 18.28 o 10 1 0 314.15 406.55 23.59 o 11 1 0 62.94 63.77 14.61 o 12 1 0 95.49 120.71 24.47 o -13 2 0 7.64 -5.36 8.16 o -12 2 0 211.71 260.66 21.33 o -11 2 0 182.82 187.93 17.26 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