#------------------------------------------------------------------------------ #$Date: 2019-11-15 08:06:30 +0200 (Fri, 15 Nov 2019) $ #$Revision: 227865 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/02/18/2021823.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2021823 _cell_angle_alpha 75.991 _cell_angle_beta 77.963 _cell_angle_gamma 71.388 _cell_length_a 10.0432 _cell_length_b 11.0358 _cell_length_c 21.1594 _exptl_crystal_F_000 1014.00 _reflns_d_resolution_high 0.7461 _cod_data_source_file dg3001Isup2.hkl _cod_data_source_block I _shelx_title ' SMB_AsPh4TcF6_0m_a.res in P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 289.85 _shelx_f_squared_multiplier 1.000 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 5872.17 4606.48 143.85 o 2 0 0 16673.62 15898.22 620.63 o 3 0 0 11.54 15.77 2.18 o 4 0 0 11498.19 11237.87 312.64 o 5 0 0 1746.81 1657.77 23.65 o 6 0 0 6.22 6.57 3.20 o 7 0 0 8135.78 7913.04 119.57 o 8 0 0 23.94 33.11 7.93 o 9 0 0 10663.23 10477.60 183.08 o 10 0 0 361.21 383.95 18.07 o 11 0 0 5548.15 5528.17 96.84 o 12 0 0 8.15 13.73 11.65 o -12 1 0 2675.95 2691.05 79.32 o -11 1 0 316.09 305.77 25.18 o -10 1 0 3200.78 3267.51 68.09 o -9 1 0 129.43 119.82 11.42 o -8 1 0 3935.31 4078.85 66.21 o -7 1 0 1260.04 1248.14 26.28 o -6 1 0 366.77 373.09 13.02 o -5 1 0 26273.95 24411.56 413.04 o -4 1 0 580.05 685.37 16.85 o -3 1 0 12941.77 12152.50 168.89 o -2 1 0 160.53 286.19 10.71 o -1 1 0 35320.95 29794.05 928.16 o 0 1 0 3854.96 3258.58 56.27 o 1 1 0 20109.47 19226.82 265.18 o 2 1 0 20164.92 19610.10 470.58 o 3 1 0 2768.31 3039.55 41.75 o 4 1 0 46805.03 46168.82 1203.37 o 5 1 0 156.25 203.85 6.69 o 6 1 0 38350.74 32584.75 1567.85 o 7 1 0 4277.99 4007.83 62.87 o 8 1 0 5506.24 5326.25 82.31 o 9 1 0 10.39 14.69 8.41 o 10 1 0 1999.17 1980.77 39.41 o 11 1 0 1731.91 1623.80 36.32 o 12 1 0 620.66 652.74 24.91 o -11 2 0 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547.67 o 3 7 0 5265.31 5528.23 83.64 o 4 7 0 11831.98 11705.12 195.83 o 5 7 0 60.87 57.93 8.37 o 6 7 0 8391.03 8240.04 121.64 o 7 7 0 583.21 658.66 40.74 o 8 7 0 1618.12 1761.04 34.52 o 9 7 0 4676.69 4859.85 77.55 o 10 7 0 13.02 14.48 19.90 o 11 7 0 6158.81 6367.10 125.26 o 12 7 0 465.84 485.84 42.47 o -8 8 0 2236.69 2293.53 60.18 o -7 8 0 179.42 172.54 46.30 o -6 8 0 2380.43 2369.14 57.78 o -5 8 0 492.82 521.71 25.66 o -4 8 0 478.94 485.14 17.43 o -3 8 0 958.21 1000.84 20.38 o -2 8 0 1316.27 1304.09 23.26 o -1 8 0 3098.85 3055.07 43.58 o 0 8 0 2456.74 2428.80 35.79 o 1 8 0 6806.84 6824.42 87.76 o 2 8 0 632.65 719.85 14.82 o 3 8 0 4577.96 4546.40 61.78 o 4 8 0 10.88 20.63 7.33 o 5 8 0 1311.56 1238.56 39.10 o 6 8 0 2938.88 2938.16 50.66 o 7 8 0 102.02 117.67 11.03 o 8 8 0 8881.26 8790.12 131.50 o 9 8 0 1987.11 2070.34 53.23 o 10 8 0 4811.27 4938.63 100.10 o 11 8 0 242.97 224.64 20.78 o 12 8 0 1062.07 1070.89 46.68 o -7 9 0 54.56 79.58 18.75 o -6 9 0 2662.02 2666.69 65.23 o -5 9 0 252.93 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