#------------------------------------------------------------------------------ #$Date: 2019-12-13 07:42:58 +0200 (Fri, 13 Dec 2019) $ #$Revision: 245043 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/02/18/2021847.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2021847 _cell_angle_alpha 76.504 _cell_angle_beta 74.536 _cell_angle_gamma 66.398 _cell_length_a 12.8003 _cell_length_b 14.3922 _cell_length_c 19.0048 _exptl_crystal_F_000 1170.00 _reflns_d_resolution_high 0.7828 _cod_data_source_file fp3081mol3sup4.hkl _cod_data_source_block mol3 _shelx_title ' mol3 in P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 259.75 _shelx_f_squared_multiplier 1.000 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 11784.78 13766.22 243.93 o 3 0 0 2.01 0.05 2.27 o 4 0 0 1582.69 1648.77 39.37 o 5 0 0 234.34 169.26 31.38 o 6 0 0 348.63 403.03 31.37 o 7 0 0 5210.13 5219.24 119.37 o 8 0 0 8.12 4.75 4.76 o 9 0 0 559.93 514.32 25.59 o 10 0 0 369.03 351.61 41.96 o 11 0 0 513.01 499.84 28.15 o 12 0 0 285.17 254.63 23.23 o 13 0 0 5.44 10.34 10.87 o 14 0 0 8.97 3.62 12.35 o -14 1 0 10.36 19.43 13.56 o -13 1 0 18.57 15.02 11.98 o -12 1 0 121.56 110.37 24.57 o -11 1 0 536.09 606.76 72.95 o -10 1 0 659.50 672.71 31.00 o -9 1 0 950.80 812.18 45.74 o -8 1 0 2.77 3.05 6.96 o -7 1 0 1534.44 1440.47 34.05 o -6 1 0 2057.86 2120.82 45.22 o -5 1 0 133.65 131.17 7.86 o -4 1 0 2904.21 2691.35 52.65 o -3 1 0 4003.01 3940.32 72.81 o -2 1 0 277.66 245.59 9.29 o -1 1 0 48.57 107.64 5.06 o 2 1 0 2458.32 2605.71 47.63 o 3 1 0 2234.50 2471.93 46.74 o 4 1 0 3266.51 3284.51 67.83 o 5 1 0 581.53 573.50 15.82 o 6 1 0 1287.31 1403.92 31.70 o 7 1 0 3663.45 3426.99 134.02 o 8 1 0 2584.12 2448.81 74.09 o 9 1 0 1251.06 1263.46 42.48 o 10 1 0 1075.71 1145.64 41.53 o 11 1 0 1164.08 1119.68 42.28 o 12 1 0 0.75 0.20 9.88 o 13 1 0 10.98 11.89 12.35 o 14 1 0 0.16 13.24 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13.62 o 10 8 22 26.50 29.46 16.64 o 1 9 22 14.95 24.95 21.17 o 2 9 22 2.07 4.74 14.10 o 3 9 22 32.31 37.07 19.28 o 4 9 22 264.37 251.42 27.53 o 5 9 22 0.57 -4.30 11.44 o 6 9 22 64.97 96.75 19.24 o 7 9 22 62.71 68.85 25.70 o 8 9 22 420.01 468.93 36.47 o 9 9 22 73.21 85.22 20.41 o 10 9 22 80.04 85.49 20.99 o 3 10 22 51.99 47.25 17.11 o 4 10 22 63.67 89.59 19.78 o 5 10 22 5.93 20.39 15.23 o 6 10 22 424.43 507.72 53.68 o 7 10 22 325.58 381.66 33.56 o 8 10 22 376.76 461.44 36.78 o 9 10 22 239.17 335.05 33.36 o 5 11 22 16.00 19.34 15.23 o 6 11 22 141.57 149.78 24.43 o 7 11 22 909.55 1010.81 52.07 o 8 11 22 297.42 319.95 32.31 o 1 -1 23 408.72 470.03 44.98 o 2 -1 23 26.61 38.92 19.08 o 3 -1 23 101.69 176.23 28.79 o 4 -1 23 286.47 326.91 34.80 o 0 0 23 1.92 -5.95 26.46 o 1 0 23 9.05 8.69 17.16 o 2 0 23 1.26 115.67 57.46 o 3 0 23 525.12 451.43 70.31 o 4 0 23 538.99 589.97 136.83 o 5 0 23 182.45 185.22 32.51 o 6 0 23 107.36 112.10 25.25 o 0 1 23 0.25 7.45 19.44 o 1 1 23 57.59 82.42 57.46 o 2 1 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21.92 o 5 5 23 293.98 327.02 32.28 o 6 5 23 2.11 -3.11 13.14 o 7 5 23 67.93 98.01 21.98 o 8 5 23 146.08 195.73 33.64 o 9 5 23 144.50 182.88 37.42 o 1 6 23 142.50 214.70 38.56 o 2 6 23 392.88 422.81 36.16 o 3 6 23 65.08 51.15 18.50 o 4 6 23 13.58 9.09 14.94 o 5 6 23 0.86 15.88 22.68 o 6 6 23 13.99 12.84 17.77 o 7 6 23 122.13 166.02 25.39 o 8 6 23 594.29 714.31 45.18 o 9 6 23 470.62 567.09 63.88 o 2 7 23 205.63 248.16 29.10 o 3 7 23 0.96 -11.75 12.70 o 4 7 23 46.82 74.56 19.76 o 5 7 23 354.93 408.55 34.33 o 6 7 23 248.43 333.74 32.26 o 7 7 23 334.65 388.55 34.55 o 8 7 23 510.30 591.52 41.76 o 9 7 23 317.03 357.20 34.98 o 2 8 23 9.80 7.51 14.85 o 3 8 23 7.39 4.05 13.98 o 4 8 23 0.26 7.29 13.56 o 5 8 23 170.93 221.55 26.96 o 6 8 23 218.61 249.58 28.81 o 7 8 23 132.54 141.55 24.06 o 8 8 23 187.82 217.89 32.89 o 4 9 23 46.20 40.35 21.92 o 5 9 23 2.75 9.83 13.56 o 6 9 23 2.96 -17.60 24.57 o 7 9 23 40.77 44.77 17.37 o 8 9 23 1.84 -13.25 13.25 o 3 2 24 3.73 161.03 52.16 o 4 2 24 1.31 43.53 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