#------------------------------------------------------------------------------ #$Date: 2020-04-21 06:09:10 +0300 (Tue, 21 Apr 2020) $ #$Revision: 250977 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/02/20/2022088.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2022088 _cell_angle_alpha 90.000 _cell_angle_beta 102.895 _cell_angle_gamma 90.000 _cell_length_a 13.5400 _cell_length_b 14.0473 _cell_length_c 22.0478 _exptl_crystal_F_000 1780.00 _reflns_d_resolution_high 0.8100 _cod_data_source_file qf3038Isup2.hkl _cod_data_source_block I _shelx_title ' shi_3259_yala_a.res in P2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 407.72 _shelx_f_squared_multiplier 1.000 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 53427.19 53810.58 234.92 o 3 0 0 199.95 182.88 29.82 o 4 0 0 5005.60 5684.58 126.49 o 5 0 0 1062.52 1222.70 92.44 o 6 0 0 12400.89 12404.12 226.32 o 7 0 0 10489.58 9950.98 197.26 o 8 0 0 653.89 577.05 90.32 o 9 0 0 117.18 73.97 65.14 o 10 0 0 2873.60 2947.84 198.84 o 11 0 0 187.97 161.63 97.92 o 12 0 0 390.69 447.18 115.48 o 13 0 0 1569.16 1447.78 194.25 o 14 0 0 0.10 376.88 128.81 o 15 0 0 354.43 736.14 259.22 o 16 0 0 36.15 162.91 154.32 o 2 1 0 2.08 9.48 16.34 o 3 1 0 589.67 583.82 27.16 o 4 1 0 1830.08 2152.26 50.25 o 5 1 0 2490.50 2694.68 62.75 o 6 1 0 657.32 811.90 44.40 o 7 1 0 25.94 95.06 32.02 o 8 1 0 1597.53 1786.28 108.78 o 9 1 0 10157.30 10016.37 260.97 o 10 1 0 4379.60 4878.97 176.05 o 11 1 0 3100.36 2805.60 143.75 o 12 1 0 5198.21 4987.13 226.57 o 13 1 0 543.27 801.04 122.29 o 14 1 0 2019.47 2287.82 186.95 o 15 1 0 6.98 124.56 98.96 o 16 1 0 18.50 -13.62 114.84 o 0 2 0 17131.26 16850.99 273.09 o 1 2 0 166233.22 167421.19 947.43 o 2 2 0 4631.25 4526.12 72.56 o 3 2 0 2824.15 2764.31 62.81 o 4 2 0 7349.25 7728.41 111.63 o 5 2 0 10273.64 10518.03 128.09 o 6 2 0 3702.64 4007.52 90.47 o 7 2 0 6268.80 6120.53 142.35 o 8 2 0 809.06 894.51 68.98 o 9 2 0 16.41 50.08 48.76 o 10 2 0 652.29 819.39 208.70 o 11 2 0 17.19 128.15 91.09 o 12 2 0 1917.60 1668.39 152.08 o 13 2 0 251.21 150.59 93.03 o 14 2 0 222.65 457.78 136.14 o 15 2 0 48.22 51.89 128.19 o 16 2 0 863.73 1001.48 152.53 o 1 3 0 3507.51 3397.04 76.81 o 2 3 0 5948.61 6510.95 88.56 o 3 3 0 628.66 707.99 37.51 o 4 3 0 5141.14 5676.59 80.03 o 5 3 0 547.60 787.46 38.86 o 6 3 0 434.52 474.34 41.23 o 7 3 0 3548.48 3559.47 158.90 o 8 3 0 265.84 272.12 76.97 o 9 3 0 1413.68 1347.92 141.03 o 10 3 0 3215.65 2993.71 387.58 o 11 3 0 7187.28 7056.17 335.82 o 12 3 0 3835.77 3720.58 259.81 o 13 3 0 1529.01 1167.73 177.99 o 14 3 0 417.88 393.75 115.69 o 15 3 0 912.57 1050.64 154.91 o 16 3 0 134.38 273.63 133.83 o 0 4 0 9599.86 9264.36 119.36 o 1 4 0 13694.74 14534.18 134.36 o 2 4 0 114554.15 118161.24 472.58 o 3 4 0 352.68 294.06 33.61 o 4 4 0 5921.17 5651.58 90.13 o 5 4 0 15167.75 14962.38 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100.44 o 8 6 0 235.15 168.80 50.77 o 9 6 0 1727.92 1390.34 104.16 o 10 6 0 595.91 734.75 140.75 o 11 6 0 469.22 804.11 147.01 o 12 6 0 10.10 63.92 109.69 o 13 6 0 237.24 342.94 132.31 o 14 6 0 934.87 1372.52 202.15 o 15 6 0 0.77 243.78 128.65 o 1 7 0 408.66 383.12 26.34 o 2 7 0 468.26 463.06 40.45 o 3 7 0 4598.84 4730.89 135.42 o 4 7 0 9729.54 9246.89 219.95 o 5 7 0 8595.44 8134.99 211.18 o 6 7 0 1225.68 1406.71 95.09 o 7 7 0 3998.76 3178.54 109.35 o 8 7 0 2573.31 2466.05 205.69 o 9 7 0 2134.19 2105.11 187.79 o 10 7 0 222.36 187.76 93.94 o 11 7 0 522.89 598.66 179.53 o 12 7 0 1712.52 1617.99 204.93 o 13 7 0 2162.30 1952.34 234.97 o 14 7 0 3404.51 3732.55 311.53 o 0 8 0 14969.50 12821.67 210.22 o 1 8 0 148.16 98.60 28.11 o 2 8 0 7461.63 7268.75 148.62 o 3 8 0 1275.51 1310.57 84.12 o 4 8 0 9359.90 9060.66 151.92 o 5 8 0 3.87 29.48 32.84 o 6 8 0 4821.26 4880.41 204.61 o 7 8 0 29.77 133.74 58.69 o 8 8 0 767.10 691.22 107.21 o 9 8 0 23.25 44.33 129.37 o 10 8 0 99.08 224.59 183.99 o 11 8 0 234.93 362.44 191.43 o 12 8 0 241.93 215.84 119.41 o 13 8 0 603.10 982.23 180.41 o 14 8 0 51.24 48.38 101.72 o 1 9 0 499.36 490.76 69.83 o 2 9 0 2834.10 3047.43 131.14 o 3 9 0 2.80 -39.44 41.79 o 4 9 0 8825.89 8557.82 228.68 o 5 9 0 439.72 387.00 39.19 o 6 9 0 7886.83 7077.02 266.47 o 7 9 0 6275.93 6496.27 462.58 o 8 9 0 3046.68 3482.07 364.75 o 9 9 0 56.00 309.41 174.16 o 10 9 0 170.58 333.98 203.16 o 11 9 0 1122.46 1328.31 269.01 o 12 9 0 147.80 273.45 193.25 o 13 9 0 3204.65 2811.26 403.40 o 0 10 0 257.65 207.23 40.11 o 1 10 0 4272.96 3661.77 249.75 o 2 10 0 878.20 898.96 133.49 o 3 10 0 8992.84 8692.93 231.77 o 4 10 0 1038.94 956.29 88.13 o 5 10 0 5709.82 5581.52 174.81 o 6 10 0 983.00 1338.11 228.90 o 7 10 0 1419.86 1336.10 234.24 o 8 10 0 364.99 297.34 167.77 o 9 10 0 215.01 13.87 140.76 o 10 10 0 76.27 423.39 188.75 o 11 10 0 74.12 125.12 162.77 o 12 10 0 897.02 586.70 221.42 o 13 10 0 64.94 -103.11 174.43 o 1 11 0 214.58 77.24 69.80 o 2 11 0 2640.45 2495.04 127.35 o 3 11 0 1454.48 1476.44 116.02 o 4 11 0 477.18 349.57 59.61 o 5 11 0 7188.40 6674.73 345.23 o 6 11 0 2101.31 1833.26 280.64 o 7 11 0 5987.21 5564.73 470.44 o 8 11 0 235.59 208.53 160.05 o 9 11 0 177.67 336.88 174.36 o 10 11 0 224.10 240.00 175.97 o 11 11 0 810.02 660.19 210.83 o 12 11 0 1441.55 1200.26 296.26 o 0 12 0 280.22 257.55 42.79 o 1 12 0 313.95 351.94 52.05 o 2 12 0 587.41 732.15 82.07 o 3 12 0 21.08 77.17 67.46 o 4 12 0 3543.79 3087.75 147.51 o 5 12 0 22.92 130.45 155.49 o 6 12 0 2139.06 1588.88 266.28 o 7 12 0 98.50 368.12 207.25 o 8 12 0 561.94 513.88 211.81 o 9 12 0 464.20 355.64 209.49 o 10 12 0 40.88 -90.66 155.51 o 11 12 0 267.02 355.44 241.10 o 1 13 0 206.18 302.71 67.88 o 2 13 0 1.04 30.95 60.42 o 3 13 0 34.20 59.32 63.86 o 4 13 0 1782.37 2008.68 204.81 o 5 13 0 2835.52 2725.95 504.56 o 6 13 0 4218.72 4370.10 430.80 o 7 13 0 92.64 336.13 158.68 o 8 13 0 1784.93 1802.85 314.35 o 9 13 0 548.48 492.89 251.88 o 10 13 0 534.70 734.78 230.93 o 0 14 0 2178.12 2226.38 199.79 o 1 14 0 2561.92 2358.59 183.95 o 2 14 0 387.50 672.06 128.44 o 3 14 0 1371.24 1201.96 146.68 o 4 14 0 58.70 131.60 93.81 o 5 14 0 3282.79 3145.57 262.00 o 6 14 0 6.33 52.93 95.33 o 7 14 0 1879.21 1751.76 316.50 o 8 14 0 75.02 358.73 201.61 o 9 14 0 311.84 322.37 212.76 o 1 15 0 0.94 94.24 63.12 o 2 15 0 274.55 349.38 251.82 o 3 15 0 677.79 752.05 172.14 o 4 15 0 639.56 441.13 133.42 o 5 15 0 1471.41 1269.81 185.41 o 6 15 0 339.20 208.08 132.55 o 7 15 0 477.20 365.47 156.18 o 8 15 0 103.09 335.33 246.04 o 0 16 0 637.88 545.83 250.54 o 1 16 0 673.27 742.18 128.49 o 2 16 0 325.10 247.67 119.85 o 3 16 0 55.19 80.24 130.98 o 4 16 0 283.94 201.16 149.70 o 5 16 0 4.63 -146.92 165.75 o 6 16 0 981.65 869.63 179.28 o 1 17 0 316.69 538.70 120.95 o 2 17 0 10.43 234.38 129.66 o 3 17 0 5.67 -13.41 155.66 o -16 1 1 907.26 1489.74 365.95 o -15 1 1 625.19 758.67 161.14 o -14 1 1 651.90 872.52 133.76 o -13 1 1 1137.03 1231.57 140.96 o -12 1 1 1244.34 1232.57 134.96 o -11 1 1 1077.34 1038.78 115.10 o -10 1 1 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3516.86 94.46 o -2 5 1 17669.98 18710.11 268.70 o -1 5 1 2214.76 2033.05 57.65 o 0 5 1 90.54 116.56 28.19 o 1 5 1 2616.33 2685.98 70.90 o 2 5 1 84.28 108.67 25.49 o 3 5 1 4005.64 3746.92 87.27 o 4 5 1 186.48 166.70 36.95 o 5 5 1 332.62 361.84 33.12 o 6 5 1 1807.19 1820.78 85.84 o 7 5 1 5040.92 4951.75 131.58 o 8 5 1 1919.31 2011.25 106.61 o 9 5 1 1107.47 1193.59 103.67 o 10 5 1 3082.79 2940.40 220.01 o 11 5 1 884.50 663.15 121.64 o 12 5 1 529.34 518.91 138.02 o 13 5 1 7.13 -50.15 115.29 o 14 5 1 735.17 1123.13 185.75 o 15 5 1 10.22 -49.04 135.14 o -15 6 1 0.10 -8.02 141.29 o -14 6 1 7.95 103.52 111.15 o -13 6 1 22.85 178.81 112.34 o -12 6 1 0.48 126.60 101.11 o -11 6 1 21.21 30.72 149.16 o -10 6 1 867.93 889.56 164.85 o -9 6 1 366.65 313.46 121.82 o -8 6 1 3091.76 3019.49 88.26 o -7 6 1 473.40 498.61 36.26 o -6 6 1 0.00 38.86 18.47 o -5 6 1 338.93 379.26 35.07 o -4 6 1 1542.19 1438.75 65.00 o -3 6 1 42.22 100.96 23.50 o -2 6 1 1507.56 1596.10 57.39 o -1 6 1 3937.92 3921.20 84.27 o 0 6 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4395.39 89.90 o 3 7 1 1286.25 1428.12 63.27 o 4 7 1 3534.97 3246.99 75.11 o 5 7 1 3040.06 3116.01 128.92 o 6 7 1 3758.86 4160.91 142.99 o 7 7 1 114.90 78.18 50.94 o 8 7 1 127.63 27.05 75.61 o 9 7 1 1336.50 1336.29 159.72 o 10 7 1 22.08 170.10 86.07 o 11 7 1 397.12 700.54 146.84 o 12 7 1 4.09 61.93 131.22 o 13 7 1 73.17 54.52 98.42 o 14 7 1 202.01 194.18 136.44 o -14 8 1 245.89 309.47 262.78 o -13 8 1 9.60 401.78 181.97 o -12 8 1 2.79 116.30 116.67 o -11 8 1 13.17 36.01 142.96 o -10 8 1 1181.16 1114.86 234.11 o -9 8 1 853.01 615.29 178.94 o -8 8 1 176.81 198.94 74.28 o -7 8 1 4063.46 3786.88 418.02 o -6 8 1 2112.61 1772.43 121.55 o -5 8 1 129.85 133.30 46.29 o -4 8 1 17.49 60.77 48.37 o -3 8 1 337.46 309.42 86.46 o -2 8 1 43.14 90.78 32.90 o -1 8 1 261.36 173.94 37.17 o 0 8 1 173.18 119.58 31.27 o 1 8 1 3717.40 3802.12 89.78 o 2 8 1 646.22 653.99 40.37 o 3 8 1 577.82 601.58 80.06 o 4 8 1 1710.09 1875.72 65.12 o 5 8 1 567.82 447.46 50.38 o 6 8 1 2927.28 2730.64 120.29 o 7 8 1 183.77 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