#------------------------------------------------------------------------------ #$Date: 2020-10-23 07:36:19 +0300 (Fri, 23 Oct 2020) $ #$Revision: 258573 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/02/22/2022265.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2022265 _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 11.1584 _cell_length_b 13.6425 _cell_length_c 36.0610 _exptl_crystal_F_000 2304.00 _reflns_d_resolution_high 0.6497 _cod_data_source_file ov31431sup2.hkl _cod_data_source_block 1 _shelx_title ' MaleicACN_0m_a.res in P2(1)2(1)2(1)' _shelx_refln_list_code 4 _shelx_f_calc_maximum 339.81 _shelx_f_squared_multiplier 1.000 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 5273.86 5322.30 242.98 o 4 0 0 39816.91 36924.67 2921.14 o 6 0 0 15221.05 15713.12 717.14 o 8 0 0 6961.72 6227.71 495.94 o 10 0 0 532.41 380.15 48.72 o 12 0 0 66.21 134.66 38.92 o 14 0 0 738.13 874.76 96.23 o 16 0 0 1.49 -44.51 44.51 o 1 1 0 1650.38 1323.38 115.79 o 2 1 0 1583.47 1553.13 71.90 o 3 1 0 11518.05 10749.23 425.38 o 4 1 0 728.31 886.15 38.20 o 5 1 0 5184.55 5126.30 203.85 o 6 1 0 142.18 234.78 17.59 o 7 1 0 11.18 159.42 13.08 o 8 1 0 3949.29 4217.85 194.49 o 9 1 0 1242.88 1256.79 61.60 o 10 1 0 2623.42 2539.82 207.76 o 11 1 0 3.74 97.52 24.73 o 12 1 0 24.36 263.50 31.02 o 13 1 0 2.98 52.35 27.66 o 14 1 0 42.06 16.46 43.37 o 15 1 0 100.82 99.43 32.43 o 16 1 0 1.62 66.88 34.63 o 17 1 0 215.25 34.34 49.63 o 0 2 0 11824.24 10004.41 560.15 o 1 2 0 7317.40 6854.36 221.35 o 2 2 0 1934.26 1773.40 71.49 o 3 2 0 140.27 174.91 27.41 o 4 2 0 22015.04 20645.18 816.46 o 5 2 0 10.53 30.60 10.13 o 6 2 0 218.78 249.49 15.32 o 7 2 0 5222.79 5410.10 215.59 o 8 2 0 1733.64 1588.88 66.78 o 9 2 0 5795.02 5392.92 215.29 o 10 2 0 288.49 389.22 47.99 o 11 2 0 1658.70 1699.38 73.06 o 12 2 0 746.28 724.90 54.07 o 13 2 0 132.95 117.73 27.55 o 14 2 0 497.03 602.25 99.40 o 15 2 0 19.26 66.17 30.06 o 16 2 0 1.23 66.32 61.68 o 1 3 0 20444.11 18133.83 642.01 o 2 3 0 1660.43 1600.22 53.68 o 3 3 0 942.54 874.13 38.52 o 4 3 0 79.05 95.10 16.35 o 5 3 0 2016.84 2304.59 93.94 o 6 3 0 2613.82 2170.08 88.95 o 7 3 0 509.00 570.32 37.17 o 8 3 0 2523.91 2206.99 90.88 o 9 3 0 56.71 78.54 14.23 o 10 3 0 54.63 38.72 15.16 o 11 3 0 465.17 485.08 27.14 o 12 3 0 1157.06 1263.51 65.87 o 13 3 0 278.68 296.30 32.71 o 14 3 0 323.56 373.19 35.22 o 15 3 0 260.64 185.12 57.19 o 0 4 0 264.10 247.82 17.95 o 1 4 0 7297.70 6537.77 211.53 o 2 4 0 5434.32 4470.88 145.73 o 3 4 0 9632.87 8684.85 281.08 o 4 4 0 884.69 1035.42 45.23 o 5 4 0 971.55 1562.74 65.44 o 6 4 0 4922.50 4460.93 178.30 o 7 4 0 8845.70 8195.28 291.21 o 8 4 0 375.89 328.78 18.92 o 10 4 0 376.04 490.54 27.65 o 11 4 0 3165.41 3203.17 151.17 o 12 4 0 630.96 566.04 30.59 o 13 4 0 250.31 287.37 24.21 o 14 4 0 57.01 67.73 56.51 o 15 4 0 5.94 55.87 58.53 o 1 5 0 299.36 319.68 16.72 o 2 5 0 477.96 451.29 20.84 o 3 5 0 6501.22 6163.74 200.52 o 4 5 0 455.47 597.40 42.74 o 5 5 0 2681.45 2612.43 122.08 o 6 5 0 163.87 186.70 15.06 o 7 5 0 2179.99 2070.24 99.76 o 8 5 0 197.17 379.67 36.18 o 9 5 0 241.79 258.04 20.80 o 10 5 0 416.07 352.06 21.75 o 11 5 0 309.75 337.58 35.19 o 12 5 0 19.02 61.06 36.91 o 13 5 0 988.84 827.31 68.87 o 14 5 0 6.99 -3.21 55.96 o 15 5 0 120.72 17.02 67.61 o 0 6 0 1412.44 1357.20 68.03 o 1 6 0 3508.68 2974.27 98.75 o 2 6 0 12093.70 11037.81 357.80 o 3 6 0 1953.38 1712.38 59.12 o 4 6 0 848.18 755.84 30.96 o 5 6 0 5571.80 5128.18 183.69 o 6 6 0 613.76 590.84 43.85 o 7 6 0 896.24 774.09 63.69 o 8 6 0 610.69 649.29 30.92 o 9 6 0 4382.94 4519.38 162.85 o 10 6 0 1083.47 1109.13 47.67 o 11 6 0 38.09 44.39 14.04 o 12 6 0 673.09 530.40 73.36 o 13 6 0 1320.35 1506.56 104.80 o 14 6 0 75.96 49.40 39.53 o 1 7 0 5.14 19.03 17.03 o 2 7 0 1608.78 1600.88 56.51 o 3 7 0 657.33 685.95 30.36 o 4 7 0 8730.82 8712.72 283.01 o 5 7 0 2710.39 2838.02 104.82 o 6 7 0 4289.55 3942.09 142.64 o 7 7 0 94.77 27.03 16.28 o 8 7 0 1202.42 1146.06 49.67 o 9 7 0 4.43 85.91 17.04 o 10 7 0 108.61 123.11 16.58 o 11 7 0 401.21 442.34 41.91 o 12 7 0 919.80 804.60 63.02 o 13 7 0 2.56 68.48 37.88 o 14 7 0 138.89 -18.01 64.89 o 0 8 0 2330.67 2244.45 108.42 o 1 8 0 5513.34 5204.72 170.64 o 2 8 0 34.98 25.03 14.53 o 3 8 0 3881.32 3620.31 119.99 o 4 8 0 405.60 413.41 20.05 o 5 8 0 5379.72 5017.36 180.66 o 6 8 0 151.48 226.83 18.60 o 7 8 0 53.80 81.74 24.69 o 8 8 0 647.19 589.26 34.69 o 9 8 0 4894.15 4988.39 202.86 o 10 8 0 710.81 699.84 53.99 o 11 8 0 240.52 302.83 22.35 o 12 8 0 19.62 29.40 53.19 o 13 8 0 967.13 873.83 110.52 o 1 9 0 258.08 174.38 15.94 o 2 9 0 4.50 33.73 14.25 o 3 9 0 1135.39 1106.13 43.40 o 4 9 0 677.74 595.58 28.23 o 5 9 0 10.10 13.60 14.57 o 6 9 0 483.15 469.71 26.98 o 7 9 0 101.65 197.17 20.15 o 8 9 0 218.48 244.01 28.19 o 9 9 0 17.04 51.87 20.08 o 10 9 0 211.20 263.29 26.93 o 11 9 0 7.37 0.67 18.96 o 12 9 0 74.43 54.52 24.32 o 13 9 0 4.66 59.44 65.98 o 0 10 0 17019.01 17235.93 790.16 o 1 10 0 2666.05 2485.84 85.66 o 2 10 0 5632.36 5408.28 178.12 o 3 10 0 1067.23 995.93 45.72 o 4 10 0 552.30 642.33 38.41 o 5 10 0 5729.47 5877.08 193.37 o 6 10 0 705.22 599.10 34.73 o 7 10 0 1339.74 1298.48 65.86 o 8 10 0 110.39 131.20 21.29 o 9 10 0 1347.97 1394.33 78.02 o 10 10 0 29.66 25.78 21.47 o 11 10 0 189.50 224.00 25.89 o 12 10 0 48.49 27.90 19.13 o 1 11 0 883.46 939.04 42.60 o 2 11 0 614.59 560.01 27.68 o 3 11 0 197.80 209.84 19.70 o 4 11 0 956.83 994.83 43.52 o 5 11 0 418.69 507.24 26.39 o 6 11 0 165.46 129.77 23.11 o 7 11 0 483.19 495.15 30.20 o 8 11 0 757.54 746.85 40.62 o 9 11 0 217.59 203.17 26.09 o 10 11 0 1.09 30.17 25.16 o 11 11 0 46.53 26.16 59.22 o 12 11 0 512.47 511.68 33.00 o 0 12 0 2371.91 2200.66 112.42 o 1 12 0 226.75 276.03 22.57 o 2 12 0 353.15 392.40 27.41 o 3 12 0 149.42 124.21 27.02 o 4 12 0 151.23 227.84 22.87 o 5 12 0 521.36 587.16 29.83 o 6 12 0 473.61 587.96 35.05 o 7 12 0 1793.22 1780.06 77.82 o 8 12 0 13.42 49.70 26.31 o 9 12 0 294.41 253.60 29.24 o 10 12 0 10.64 -2.97 27.60 o 11 12 0 490.03 511.74 71.94 o 12 12 0 217.31 261.76 43.77 o 1 13 0 70.76 40.56 22.27 o 2 13 0 191.30 159.70 25.32 o 3 13 0 7.67 38.12 22.14 o 4 13 0 269.00 235.14 23.64 o 5 13 0 0.48 -3.90 24.57 o 6 13 0 2.19 -24.78 24.78 o 7 13 0 241.77 214.59 28.69 o 8 13 0 1038.28 1034.75 58.13 o 9 13 0 0.63 -27.32 27.32 o 10 13 0 29.58 59.26 29.28 o 11 13 0 141.40 80.44 32.77 o 12 13 0 14.41 54.87 40.41 o 0 14 0 909.38 871.36 58.33 o 1 14 0 852.33 837.31 39.10 o 2 14 0 47.19 11.21 23.50 o 3 14 0 192.46 228.70 28.65 o 4 14 0 571.52 738.10 41.23 o 5 14 0 20.88 35.36 27.46 o 6 14 0 311.16 269.69 40.46 o 7 14 0 30.62 -26.56 29.62 o 8 14 0 609.25 603.81 46.54 o 9 14 0 177.06 170.01 31.63 o 10 14 0 122.03 169.64 35.13 o 11 14 0 27.05 3.13 45.72 o 12 14 0 166.92 70.77 41.99 o 1 15 0 161.08 175.35 31.16 o 2 15 0 111.03 107.74 30.62 o 3 15 0 38.15 29.73 30.49 o 4 15 0 9.44 2.88 30.85 o 5 15 0 151.27 175.78 31.71 o 6 15 0 8.66 -2.83 29.72 o 7 15 0 93.55 80.72 34.24 o 8 15 0 78.10 48.95 54.07 o 9 15 0 4.51 -27.35 35.20 o 10 15 0 42.92 118.99 60.58 o 11 15 0 6.46 77.25 50.09 o 0 16 0 1117.17 1184.36 90.27 o 1 16 0 194.48 142.09 38.76 o 2 16 0 27.18 35.75 40.45 o 3 16 0 108.97 74.13 36.03 o 4 16 0 1825.11 2107.98 96.20 o 5 16 0 122.47 91.03 34.16 o 6 16 0 45.86 71.05 43.94 o 7 16 0 0.81 -13.90 37.44 o 8 16 0 4.73 65.02 70.52 o 9 16 0 81.41 74.50 57.74 o 1 17 0 39.05 29.73 39.37 o 2 17 0 86.35 73.16 41.58 o 3 17 0 12.93 15.47 39.88 o 4 17 0 752.81 702.21 78.50 o 5 17 0 70.36 -9.97 44.68 o 6 17 0 81.43 111.21 45.15 o 7 17 0 1.76 56.86 105.38 o 8 17 0 7.90 -58.92 110.00 o 0 18 0 130.52 177.10 95.11 o 1 18 0 16.07 3.53 42.35 o 2 18 0 4.95 16.05 44.47 o 3 18 0 141.81 123.01 46.57 o 4 18 0 4.68 54.35 71.79 o 5 18 0 202.83 259.24 116.15 o 6 18 0 14.34 33.37 117.73 o 7 18 0 6.81 131.27 111.57 o 1 19 0 16.19 84.07 70.77 o 2 19 0 63.46 98.69 74.86 o 3 19 0 2.44 16.84 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216.39 17.14 o -5 1 1 4579.37 4372.10 168.52 o -4 1 1 4829.65 4760.97 175.07 o -3 1 1 21252.59 20816.39 927.93 o -2 1 1 15883.03 15110.28 814.45 o 2 1 1 14970.89 14182.35 665.00 o 3 1 1 20594.04 19874.58 927.80 o 4 1 1 4247.95 4126.19 156.31 o 5 1 1 4375.69 4138.05 137.22 o 6 1 1 31.14 317.35 37.53 o 7 1 1 12572.93 12170.35 586.86 o 8 1 1 827.89 977.95 41.46 o 9 1 1 2190.40 2035.30 94.01 o 10 1 1 843.95 861.21 73.07 o 11 1 1 3938.91 4217.80 334.34 o 12 1 1 1059.40 1061.70 79.65 o 13 1 1 141.70 139.94 28.94 o 14 1 1 172.23 284.19 57.95 o 15 1 1 548.11 517.90 46.24 o 16 1 1 177.09 92.89 34.96 o 17 1 1 18.36 -1.13 55.64 o -16 2 1 49.41 82.45 57.77 o -15 2 1 180.86 166.94 32.37 o -14 2 1 187.23 261.02 54.17 o -13 2 1 174.55 163.66 30.09 o -12 2 1 175.78 193.93 27.83 o -11 2 1 484.09 540.52 39.57 o -10 2 1 227.43 263.30 23.12 o -9 2 1 39.88 134.03 18.67 o -8 2 1 1801.80 1729.91 71.35 o -7 2 1 1751.01 1848.32 76.65 o -6 2 1 2305.54 2629.97 101.30 o -5 2 1 5918.85 5901.55 245.32 o -4 2 1 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9455.89 8896.80 366.19 o -2 3 1 6865.12 6355.86 181.34 o -1 3 1 29481.98 26421.25 1125.36 o 0 3 1 2078.33 2336.32 70.95 o 1 3 1 25664.50 23288.70 974.45 o 2 3 1 6096.96 5680.66 195.66 o 3 3 1 10251.70 9515.57 327.38 o 4 3 1 11858.73 10812.48 420.47 o 5 3 1 18513.07 17508.26 709.31 o 6 3 1 420.16 464.78 27.30 o 7 3 1 873.86 914.29 44.51 o 8 3 1 819.40 883.90 38.63 o 9 3 1 1067.56 1184.29 50.72 o 10 3 1 409.16 515.25 27.29 o 11 3 1 774.15 1028.40 45.51 o 12 3 1 19.08 66.16 15.32 o 13 3 1 715.26 657.93 80.28 o 14 3 1 709.01 665.91 41.08 o 15 3 1 10.54 95.06 54.52 o 16 3 1 24.48 -58.94 58.94 o -15 4 1 2.80 15.35 59.78 o -14 4 1 380.70 413.49 31.83 o -13 4 1 53.35 40.64 22.88 o -12 4 1 589.54 608.05 32.71 o -11 4 1 125.03 111.73 16.12 o -10 4 1 651.77 703.97 45.06 o -9 4 1 1116.32 1067.79 54.39 o -8 4 1 849.02 899.09 35.12 o -7 4 1 309.26 340.01 20.42 o -6 4 1 1744.27 1758.69 77.99 o -5 4 1 1491.96 1546.18 69.42 o -4 4 1 706.44 716.97 53.53 o -3 4 1 2381.66 2156.60 78.50 o -2 4 1 836.56 763.27 27.61 o -1 4 1 41434.76 36974.73 1464.59 o 0 4 1 18076.04 15424.53 461.66 o 1 4 1 41606.34 37074.78 1691.19 o 2 4 1 672.41 644.43 27.43 o 3 4 1 1762.06 1717.36 69.54 o 4 4 1 1079.06 988.82 45.34 o 5 4 1 1593.28 1763.76 62.86 o 6 4 1 2014.43 2132.94 110.10 o 7 4 1 318.68 365.22 24.52 o 8 4 1 676.61 721.63 34.30 o 9 4 1 1289.88 1285.57 50.32 o 10 4 1 397.74 497.46 28.81 o 11 4 1 174.72 216.75 22.72 o 12 4 1 490.85 462.10 27.99 o 13 4 1 105.50 99.54 55.55 o 14 4 1 410.16 411.86 71.93 o 15 4 1 20.10 74.62 58.91 o -15 5 1 75.72 94.57 67.30 o -14 5 1 184.46 144.20 64.85 o -13 5 1 842.72 997.80 49.83 o -12 5 1 367.70 426.49 28.19 o -11 5 1 1296.40 1176.96 57.51 o -10 5 1 1273.89 1306.78 58.59 o -9 5 1 6672.25 6583.64 233.27 o -8 5 1 4057.00 3846.62 140.96 o -7 5 1 259.64 301.79 21.74 o -6 5 1 2377.42 2432.94 104.48 o -5 5 1 10086.99 9934.68 376.53 o -4 5 1 18619.30 17607.37 656.67 o -3 5 1 359.59 365.97 18.11 o -2 5 1 7080.73 6562.32 224.54 o -1 5 1 7146.70 6752.96 199.95 o 0 5 1 15435.46 12818.57 415.16 o 1 5 1 5933.92 5554.26 199.80 o 2 5 1 7816.24 7272.95 224.63 o 3 5 1 489.52 488.35 20.17 o 4 5 1 20248.08 19473.81 656.73 o 5 5 1 9231.86 9007.58 377.33 o 6 5 1 2769.60 2672.82 93.86 o 7 5 1 180.06 211.85 16.48 o 8 5 1 4109.81 3959.60 140.83 o 9 5 1 6601.87 6467.79 233.05 o 10 5 1 1690.29 1637.24 58.12 o 11 5 1 1424.18 1345.92 67.13 o 12 5 1 398.52 490.43 42.95 o 13 5 1 768.98 759.91 68.69 o 14 5 1 152.74 79.46 71.27 o 15 5 1 63.65 53.87 68.17 o -14 6 1 66.90 81.42 64.88 o -13 6 1 334.75 328.41 45.90 o -12 6 1 123.10 142.03 24.14 o -11 6 1 490.53 473.78 27.63 o -10 6 1 1842.93 1799.00 68.98 o -9 6 1 710.89 656.01 31.01 o -8 6 1 301.14 336.59 22.24 o -7 6 1 322.49 323.22 20.11 o -6 6 1 1555.38 1382.68 62.91 o -5 6 1 708.17 725.66 34.82 o -4 6 1 845.80 868.62 33.48 o -3 6 1 2090.97 1917.80 68.38 o -2 6 1 2034.50 2025.18 75.76 o -1 6 1 3262.55 3045.25 107.68 o 0 6 1 15654.96 14989.17 485.22 o 1 6 1 3728.17 3515.75 117.93 o 2 6 1 2511.84 2480.29 75.95 o 3 6 1 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