#------------------------------------------------------------------------------ #$Date: 2021-08-24 04:55:41 +0300 (Tue, 24 Aug 2021) $ #$Revision: 268181 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/02/24/2022424.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2022424 _cell_angle_alpha 71.048 _cell_angle_beta 87.964 _cell_angle_gamma 82.954 _cell_length_a 10.3585 _cell_length_b 13.0835 _cell_length_c 13.9799 _exptl_crystal_F_000 684.00 _reflns_d_resolution_high 0.7491 _cod_data_source_file yo30804sup4.hkl _cod_data_source_block 4 _shelx_title ' char357 in P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 184.64 _shelx_f_squared_multiplier 1.000 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 9484.79 12509.74 207.83 o 3 0 0 6525.20 7339.54 145.10 o 4 0 0 19223.79 23339.19 441.45 o 5 0 0 1899.06 2030.23 52.53 o 6 0 0 1.09 -1.79 9.59 o 7 0 0 474.76 419.73 22.50 o 8 0 0 1917.47 2170.79 124.58 o 9 0 0 1187.51 1357.84 68.78 o 10 0 0 384.70 332.84 60.80 o 11 0 0 51.39 9.49 24.38 o 12 0 0 584.60 566.09 80.03 o 13 0 0 447.50 539.45 78.67 o -13 1 0 261.29 241.62 51.48 o -12 1 0 631.86 577.66 78.46 o -11 1 0 658.48 708.62 75.73 o -10 1 0 17.91 23.95 19.23 o -9 1 0 438.64 494.28 46.18 o -8 1 0 1457.58 1417.55 64.97 o -7 1 0 2849.90 3148.83 78.37 o -6 1 0 244.32 276.13 16.59 o -5 1 0 2907.61 3404.47 77.97 o -4 1 0 2890.31 2868.63 65.39 o -3 1 0 403.13 438.16 16.38 o -2 1 0 2.25 5.84 3.28 o -1 1 0 18.68 25.90 5.61 o 1 1 0 11473.57 15164.44 974.05 o 2 1 0 162.65 189.79 10.48 o 3 1 0 514.12 738.20 22.97 o 4 1 0 3836.85 5373.13 112.16 o 5 1 0 475.99 568.65 24.23 o 6 1 0 120.38 205.25 16.19 o 7 1 0 487.63 435.41 37.64 o 8 1 0 44.13 17.49 26.89 o 9 1 0 114.62 27.53 32.34 o 10 1 0 124.86 78.92 34.85 o 11 1 0 13.35 -2.51 19.66 o 12 1 0 8.59 15.57 17.44 o 13 1 0 11.86 18.47 16.64 o -13 2 0 6.90 28.76 23.36 o -12 2 0 79.87 106.41 32.85 o -11 2 0 234.84 243.45 50.89 o -10 2 0 447.01 592.92 103.03 o -9 2 0 259.29 753.63 72.41 o -8 2 0 39.27 75.80 19.06 o -7 2 0 88.10 73.79 19.34 o -6 2 0 2091.95 2121.90 100.96 o -5 2 0 5576.49 6845.40 321.46 o -4 2 0 0.77 -1.02 9.65 o -3 2 0 936.14 1486.91 52.12 o -2 2 0 747.03 801.31 22.57 o -1 2 0 7443.32 7711.16 165.91 o 0 2 0 1477.70 1616.77 31.34 o 1 2 0 26.58 22.64 7.72 o 2 2 0 4134.88 6107.92 150.73 o 3 2 0 8642.22 10629.89 561.38 o 4 2 0 2607.12 2773.88 63.64 o 5 2 0 312.27 333.63 17.96 o 6 2 0 235.17 340.40 19.85 o 7 2 0 31.65 15.73 17.17 o 8 2 0 1162.73 1324.14 59.39 o 9 2 0 544.12 519.20 70.29 o 10 2 0 0.66 7.32 24.72 o 11 2 0 20.48 56.97 31.65 o 12 2 0 8.08 -14.30 14.30 o 13 2 0 97.85 62.80 23.87 o -13 3 0 64.57 99.56 22.08 o -12 3 0 21.95 14.30 12.34 o -11 3 0 0.41 1.49 14.59 o -10 3 0 147.55 111.37 28.28 o -9 3 0 408.05 641.61 75.95 o -7 3 0 895.97 999.88 53.51 o -6 3 0 43.43 -2.25 17.91 o -5 3 0 3670.90 3449.31 106.83 o -4 3 0 3632.53 3008.51 93.03 o -3 3 0 519.68 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1501.48 41.24 o 1 7 0 48.77 50.98 10.44 o 2 7 0 984.00 986.30 31.06 o 3 7 0 521.19 462.21 23.18 o 4 7 0 1919.88 2148.60 57.34 o 5 7 0 520.26 536.85 39.72 o 6 7 0 4.81 5.73 16.91 o 7 7 0 210.51 247.66 34.32 o 8 7 0 385.87 409.90 100.56 o 9 7 0 160.63 169.44 33.29 o 10 7 0 51.30 43.91 19.40 o 11 7 0 3.78 -17.49 17.49 o 12 7 0 4.32 -2.72 15.27 o 13 7 0 57.23 156.57 30.85 o -11 8 0 0.20 -15.21 15.21 o -10 8 0 34.78 26.88 17.64 o -9 8 0 416.18 504.83 54.64 o -8 8 0 562.03 553.87 57.19 o -7 8 0 64.83 31.45 23.47 o -6 8 0 0.95 -37.36 38.70 o -5 8 0 210.56 229.16 46.76 o -4 8 0 1246.82 1254.62 87.14 o -3 8 0 963.70 971.71 44.14 o -2 8 0 823.90 769.82 44.29 o -1 8 0 122.72 93.30 15.83 o 0 8 0 2409.22 2399.59 57.48 o 1 8 0 1514.85 1461.04 41.54 o 2 8 0 190.06 156.92 14.56 o 3 8 0 568.04 559.43 23.30 o 4 8 0 198.79 165.13 15.14 o 5 8 0 115.47 87.12 28.66 o 6 8 0 303.96 320.41 37.15 o 7 8 0 445.77 423.32 43.06 o 8 8 0 6.14 22.40 17.25 o 9 8 0 381.11 385.74 43.41 o 10 8 0 97.77 93.02 26.37 o 11 8 0 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