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Information card for entry 2022431
Preview
| Coordinates | 2022431.cif |
|---|---|
| Structure factors | 2022431.hkl |
| Original IUCr paper | HTML |
| Chemical name | Bis[μ-<i>N</i>,<i>N</i>'-bis(2,6-diisopropylphenyl)formamidinato]diantimony(I)(2 <i>Sb</i>—<i>Sb</i>) tetrahydrofuran heptasolvate |
|---|---|
| Formula | C78 H126 N4 O7 Sb2 |
| Calculated formula | C78 H126 N4 O7 Sb2 |
| Title of publication | Synthesis and characterization of a range of antimony(I/III) <i>N</i>,<i>N</i>'-bis(2,6-diisopropylphenyl)formamidinate complexes |
| Authors of publication | Al-Dabbagh, Areej; Guo, Zhifang; Junk, Peter; Wang, Jun |
| Journal of publication | Acta Crystallographica Section C |
| Year of publication | 2021 |
| Journal volume | 77 |
| Journal issue | 9 |
| a | 21.243 ± 0.004 Å |
| b | 18.997 ± 0.004 Å |
| c | 21.743 ± 0.004 Å |
| α | 90° |
| β | 118.6 ± 0.03° |
| γ | 90° |
| Cell volume | 7704 ± 3 Å3 |
| Cell temperature | 100 K |
| Ambient diffraction temperature | 100 K |
| Number of distinct elements | 5 |
| Space group number | 14 |
| Hermann-Mauguin space group symbol | P 1 21/c 1 |
| Hall space group symbol | -P 2ybc |
| Residual factor for all reflections | 0.1045 |
| Residual factor for significantly intense reflections | 0.0914 |
| Weighted residual factors for significantly intense reflections | 0.2653 |
| Weighted residual factors for all reflections included in the refinement | 0.2713 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.188 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | Synchrotron |
| Has coordinates | Yes |
| Has disorder | Yes |
| Has Fobs | Yes |
| Revision | Date | Message | Files |
|---|---|---|---|
| 268227 (current) | 2021-08-26 | cif/ hkl/ Adding structures of 2022431, 2022432, 2022433, 2022434, 2022435, 2022436 via cif-deposit CGI script. |
2022431.cif 2022431.hkl |
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Users of the data should acknowledge the original authors of the
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