#------------------------------------------------------------------------------
#$Date: 2021-08-26 05:04:31 +0300 (Thu, 26 Aug 2021) $
#$Revision: 268227 $
#$URL: file:///home/coder/svn-repositories/cod/cif/2/02/24/2022435.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/. The original data for this entry
# were provided by IUCr Journals, http://journals.iucr.org/.
#
# The file may be used within the scientific community so long as
# proper attribution is given to the journal article from which the
# data were obtained.
#
data_2022435
loop_
_publ_author_name
'Al-Dabbagh, Areej'
'Guo, Zhifang'
'Junk, Peter'
'Wang, Jun'
_publ_section_title
;
 Synthesis and characterization of a range of antimony(I/III)
 N,N'-bis(2,6-diisopropylphenyl)formamidinate complexes
;
_journal_coeditor_code           EP3019
_journal_issue                   9
_journal_name_full               'Acta Crystallographica Section C'
_journal_page_first
;
;
_journal_paper_doi               10.1107/S2053229621008512
_journal_volume                  77
_journal_year                    2021
_chemical_formula_iupac          '[Sb Br2 (C25 H35 N2)]'
_chemical_formula_moiety         'C25 H35 Br2 N2 Sb'
_chemical_formula_sum            'C25 H35 Br2 N2 Sb'
_chemical_formula_weight         645.12
_chemical_name_systematic
'[N,N'-Bis(2,6-diisopropylphenyl)formamidinato]dibromidoantimony(III)'
_space_group_crystal_system      triclinic
_space_group_IT_number           2
_space_group_name_Hall           '-P 1'
_space_group_name_H-M_alt        'P -1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_audit_creation_method
;
Olex2 1.3
(compiled 2020.07.31 svn.rc2a77460 for OlexSys, GUI svn.r6145)
;
_cell_angle_alpha                96.69(3)
_cell_angle_beta                 103.93(3)
_cell_angle_gamma                111.72(3)
_cell_formula_units_Z            2
_cell_length_a                   10.105(2)
_cell_length_b                   10.332(2)
_cell_length_c                   14.240(3)
_cell_measurement_reflns_used    6298
_cell_measurement_temperature    100
_cell_measurement_theta_max      25
_cell_measurement_theta_min      2
_cell_volume                     1305.2(6)
_computing_cell_refinement
;
XDS (Kabsch, 1993)
;
_computing_data_collection
;
XDS (Kabsch, 1993)
;
_computing_data_reduction
;
XDS (Kabsch, 1993)
;
_computing_molecular_graphics
;
OLEX2 (Dolomanov et al., 2009) and
X-SEED (Barbour, 2001)
;
_computing_publication_material
;
OLEX2 (Dolomanov et al., 2009)
;
_computing_structure_refinement
;
SHELXL2018 (Sheldrick, 2015b)
;
_computing_structure_solution
;
SIR2004 (Burla et al.,  2005)
;
_diffrn_ambient_temperature      100
_diffrn_measured_fraction_theta_full 0.902
_diffrn_measured_fraction_theta_max 0.699
_diffrn_measurement_device_type  'ADSC Quantum 210r'
_diffrn_measurement_method       'Phi Scan'
_diffrn_radiation_monochromator  'Silicon Double Crystal'
_diffrn_radiation_type           Synchrotron
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0324
_diffrn_reflns_av_unetI/netI     0.0280
_diffrn_reflns_limit_h_max       14
_diffrn_reflns_limit_h_min       -14
_diffrn_reflns_limit_k_max       14
_diffrn_reflns_limit_k_min       -14
_diffrn_reflns_limit_l_max       18
_diffrn_reflns_limit_l_min       -18
_diffrn_reflns_number            23524
_diffrn_reflns_theta_full        25.242
_diffrn_reflns_theta_max         31.920
_diffrn_reflns_theta_min         2.353
_diffrn_source                   'MX1 Beamline Australian Synchrotron'
_diffrn_standards_number         0
_exptl_absorpt_coefficient_mu    4.133
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details
;
(XDS; Kabsch, 1993)
;
_exptl_crystal_colour            yellow
_exptl_crystal_density_diffrn    1.642
_exptl_crystal_description       cube
_exptl_crystal_F_000             640
_exptl_crystal_size_max          0.1
_exptl_crystal_size_mid          0.04
_exptl_crystal_size_min          0.02
_refine_diff_density_max         0.504
_refine_diff_density_min         -1.249
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.072
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     279
_refine_ls_number_reflns         6298
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      1.072
_refine_ls_R_factor_all          0.0290
_refine_ls_R_factor_gt           0.0282
_refine_ls_shift/su_max          0.003
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[σ²(Fo²)+(0.0394P)²+1.7194P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0746
_refine_ls_wR_factor_ref         0.0751
_reflns_number_gt                6079
_reflns_number_total             6298
_reflns_threshold_expression     'I > 2σ(I)'
_cod_data_source_file            ep3019sup1.cif
_cod_data_source_block           5
_cod_original_cell_volume        1305.2(5)
_cod_database_code               2022435
_shelx_space_group_comment
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;
_shelx_estimated_absorpt_t_min   0.683
_shelx_estimated_absorpt_t_max   0.922
loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x, -y, -z'
loop_
_atom_site_type_symbol
_atom_site_label
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_calc_flag
_atom_site_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
Sb Sb1 0.39366(2) 0.57235(2) 0.85010(2) 0.01444(5) Uani d 1 . .
Br Br1 0.55529(3) 0.73608(2) 1.02516(2) 0.01988(6) Uani d 1 . .
Br Br2 0.25079(3) 0.72234(3) 0.80529(2) 0.02796(7) Uani d 1 . .
N N1 0.57025(19) 0.66793(18) 0.79381(13) 0.0124(3) Uani d 1 . .
N N2 0.3676(2) 0.51144(19) 0.67425(14) 0.0151(3) Uani d 1 . .
C C10 0.7817(2) 0.5702(2) 0.90412(17) 0.0160(4) Uani d 1 . .
H H10 0.672943 0.534523 0.898438 0.019 Uiso calc 1 . .
C C3 0.9817(2) 0.8099(2) 0.90879(17) 0.0157(4) Uani d 1 . .
H H3 1.054777 0.778030 0.939372 0.019 Uiso calc 1 . .
C C1 0.7249(2) 0.7659(2) 0.83235(16) 0.0117(3) Uani d 1 . .
C C14 0.2830(2) 0.4227(2) 0.57749(16) 0.0144(4) Uani d 1 . .
C C6 0.7681(2) 0.9060(2) 0.81703(16) 0.0137(4) Uani d 1 . .
C C2 0.8299(2) 0.7182(2) 0.88170(16) 0.0134(4) Uani d 1 . .
C C13 0.5085(2) 0.5954(2) 0.69805(16) 0.0131(4) Uani d 1 . .
H H13 0.563553 0.604972 0.651889 0.016 Uiso calc 1 . .
C C7 0.6539(3) 0.9632(2) 0.77384(18) 0.0170(4) Uani d 1 . .
H H7 0.556221 0.879527 0.739066 0.020 Uiso calc 1 . .
C C23 0.2786(3) 0.6417(2) 0.51231(18) 0.0194(4) Uani d 1 . .
H H23 0.301999 0.681506 0.584718 0.023 Uiso calc 1 . .
C C16 0.1567(3) 0.3892(3) 0.40455(17) 0.0209(4) Uani d 1 . .
H H16 0.127694 0.427244 0.349446 0.025 Uiso calc 1 . .
C C5 0.9209(2) 0.9947(2) 0.84786(17) 0.0167(4) Uani d 1 . .
H H5 0.952902 1.089822 0.838650 0.020 Uiso calc 1 . .
C C4 1.0272(2) 0.9468(2) 0.89171(17) 0.0167(4) Uani d 1 . .
H H4 1.130791 1.007699 0.909948 0.020 Uiso calc 1 . .
C C21 0.2718(3) 0.2119(2) 0.65622(19) 0.0200(4) Uani d 1 . .
H H21 0.371161 0.281366 0.703045 0.024 Uiso calc 1 . .
C C15 0.2388(2) 0.4820(2) 0.49811(17) 0.0162(4) Uani d 1 . .
C C8 0.6971(3) 1.0513(3) 0.6979(2) 0.0266(5) Uani d 1 . .
H H8A 0.787909 1.138679 0.731471 0.040 Uiso calc 1 . .
H H8B 0.615296 1.076848 0.666978 0.040 Uiso calc 1 . .
H H8C 0.715827 0.994652 0.646558 0.040 Uiso calc 1 . .
C C19 0.2376(2) 0.2733(2) 0.56631(17) 0.0159(4) Uani d 1 . .
C C12 0.8666(3) 0.5757(3) 1.01055(18) 0.0212(4) Uani d 1 . .
H H12A 0.973585 0.608249 1.017970 0.032 Uiso calc 1 . .
H H12B 0.828539 0.480051 1.024063 0.032 Uiso calc 1 . .
H H12C 0.851960 0.642352 1.057592 0.032 Uiso calc 1 . .
C C9 0.6320(3) 1.0516(3) 0.8581(2) 0.0251(5) Uani d 1 . .
H H9A 0.598977 0.991850 0.903764 0.038 Uiso calc 1 . .
H H9B 0.556195 1.086140 0.830331 0.038 Uiso calc 1 . .
H H9C 0.726961 1.133472 0.894285 0.038 Uiso calc 1 . .
C C17 0.1168(3) 0.2429(3) 0.39064(18) 0.0227(5) Uani d 1 . .
H H17 0.063121 0.181960 0.326337 0.027 Uiso calc 1 . .
C C11 0.7991(3) 0.4648(3) 0.82823(19) 0.0260(5) Uani d 1 . .
H H11A 0.738209 0.458346 0.761436 0.039 Uiso calc 1 . .
H H11B 0.765667 0.370240 0.843817 0.039 Uiso calc 1 . .
H H11C 0.904459 0.498365 0.830835 0.039 Uiso calc 1 . .
C C24 0.1483(3) 0.6731(3) 0.4560(2) 0.0292(6) Uani d 1 . .
H H24A 0.126355 0.640131 0.384380 0.044 Uiso calc 1 . .
H H24B 0.175771 0.776332 0.472152 0.044 Uiso calc 1 . .
H H24C 0.059572 0.622939 0.475592 0.044 Uiso calc 1 . .
C C20 0.1531(3) 0.1979(3) 0.7093(2) 0.0238(5) Uani d 1 . .
H H20A 0.146027 0.289893 0.723040 0.036 Uiso calc 1 . .
H H20B 0.181695 0.170014 0.772007 0.036 Uiso calc 1 . .
H H20C 0.055807 0.124802 0.666777 0.036 Uiso calc 1 . .
C C18 0.1560(3) 0.1857(2) 0.47164(19) 0.0209(4) Uani d 1 . .
H H18 0.126627 0.085292 0.462109 0.025 Uiso calc 1 . .
C C22 0.2798(3) 0.0667(3) 0.6325(2) 0.0305(6) Uani d 1 . .
H H22A 0.180534 -0.005746 0.592449 0.046 Uiso calc 1 . .
H H22B 0.312636 0.039146 0.694553 0.046 Uiso calc 1 . .
H H22C 0.351164 0.074027 0.595250 0.046 Uiso calc 1 . .
C C25 0.4177(3) 0.7200(3) 0.4825(2) 0.0258(5) Uani d 1 . .
H H25A 0.503102 0.707310 0.523404 0.039 Uiso calc 1 . .
H H25B 0.439554 0.822127 0.492653 0.039 Uiso calc 1 . .
H H25C 0.399660 0.680628 0.412286 0.039 Uiso calc 1 . .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Br Br -0.2901 2.4595 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Sb Sb -0.5866 1.5461 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_2
_geom_angle_site_symmetry_3
_geom_angle
_geom_angle_publ_flag
Br2 Sb1 Br1 . . . 94.98(3) y
C13 Sb1 Br1 . . . 119.68(4) y
C13 Sb1 Br2 . . . 95.33(6) y
N1 Sb1 Br1 . . . 90.13(6) n
N1 Sb1 Br2 . . . 98.93(5) n
N1 Sb1 N2 . . . 58.20(7) n
N2 Sb1 Br1 . . . 148.10(5) n
N2 Sb1 Br2 . . . 87.08(5) n
C1 N1 Sb1 . . . 137.39(14) n
C13 N1 Sb1 . . . 100.51(14) n
C13 N1 C1 . . . 121.57(19) n
C14 N2 Sb1 . . . 149.66(15) n
C13 N2 Sb1 . . . 86.44(14) n
C13 N2 C14 . . . 123.0(2) n
C2 C10 H10 . . . 107.6 n
C2 C10 C12 . . . 111.47(19) n
C2 C10 C11 . . . 111.3(2) n
C12 C10 H10 . . . 107.6 n
C11 C10 H10 . . . 107.6 n
C11 C10 C12 . . . 111.17(18) n
C2 C3 H3 . . . 119.5 n
C4 C3 H3 . . . 119.5 n
C4 C3 C2 . . . 120.99(19) n
C6 C1 N1 . . . 119.20(18) n
C2 C1 N1 . . . 119.01(18) n
C2 C1 C6 . . . 121.76(19) n
C15 C14 N2 . . . 120.54(19) n
C15 C14 C19 . . . 121.7(2) n
C19 C14 N2 . . . 117.6(2) n
C1 C6 C7 . . . 121.91(19) n
C5 C6 C1 . . . 117.69(19) n
C5 C6 C7 . . . 120.32(19) n
C3 C2 C10 . . . 120.33(18) n
C3 C2 C1 . . . 118.14(19) n
C1 C2 C10 . . . 121.52(18) n
N1 C13 H13 . . . 122.8 n
N2 C13 N1 . . . 114.4(2) n
N2 C13 H13 . . . 122.8 n
C6 C7 H7 . . . 107.9 n
C6 C7 C8 . . . 112.6(2) n
C6 C7 C9 . . . 109.54(19) n
C8 C7 H7 . . . 107.9 n
C9 C7 H7 . . . 107.9 n
C9 C7 C8 . . . 110.8(2) n
C15 C23 H23 . . . 107.5 n
C15 C23 C24 . . . 112.4(2) n
C15 C23 C25 . . . 111.9(2) n
C24 C23 H23 . . . 107.5 n
C25 C23 H23 . . . 107.5 n
C25 C23 C24 . . . 109.8(2) n
C15 C16 H16 . . . 119.3 n
C17 C16 H16 . . . 119.3 n
C17 C16 C15 . . . 121.4(2) n
C6 C5 H5 . . . 119.3 n
C4 C5 C6 . . . 121.39(19) n
C4 C5 H5 . . . 119.3 n
C3 C4 C5 . . . 119.84(19) n
C3 C4 H4 . . . 120.1 n
C5 C4 H4 . . . 120.1 n
C19 C21 H21 . . . 107.9 n
C19 C21 C20 . . . 109.14(19) n
C19 C21 C22 . . . 114.4(2) n
C20 C21 H21 . . . 107.9 n
C22 C21 H21 . . . 107.9 n
C22 C21 C20 . . . 109.4(2) n
C14 C15 C23 . . . 121.5(2) n
C16 C15 C14 . . . 117.8(2) n
C16 C15 C23 . . . 120.6(2) n
C7 C8 H8A . . . 109.5 n
C7 C8 H8B . . . 109.5 n
C7 C8 H8C . . . 109.5 n
H8A C8 H8B . . . 109.5 n
H8A C8 H8C . . . 109.5 n
H8B C8 H8C . . . 109.5 n
C14 C19 C21 . . . 120.2(2) n
C18 C19 C14 . . . 118.0(2) n
C18 C19 C21 . . . 121.7(2) n
C10 C12 H12A . . . 109.5 n
C10 C12 H12B . . . 109.5 n
C10 C12 H12C . . . 109.5 n
H12A C12 H12B . . . 109.5 n
H12A C12 H12C . . . 109.5 n
H12B C12 H12C . . . 109.5 n
C7 C9 H9A . . . 109.5 n
C7 C9 H9B . . . 109.5 n
C7 C9 H9C . . . 109.5 n
H9A C9 H9B . . . 109.5 n
H9A C9 H9C . . . 109.5 n
H9B C9 H9C . . . 109.5 n
C16 C17 H17 . . . 120.2 n
C16 C17 C18 . . . 119.7(2) n
C18 C17 H17 . . . 120.2 n
C10 C11 H11A . . . 109.5 n
C10 C11 H11B . . . 109.5 n
C10 C11 H11C . . . 109.5 n
H11A C11 H11B . . . 109.5 n
H11A C11 H11C . . . 109.5 n
H11B C11 H11C . . . 109.5 n
C23 C24 H24A . . . 109.5 n
C23 C24 H24B . . . 109.5 n
C23 C24 H24C . . . 109.5 n
H24A C24 H24B . . . 109.5 n
H24A C24 H24C . . . 109.5 n
H24B C24 H24C . . . 109.5 n
C21 C20 H20A . . . 109.5 n
C21 C20 H20B . . . 109.5 n
C21 C20 H20C . . . 109.5 n
H20A C20 H20B . . . 109.5 n
H20A C20 H20C . . . 109.5 n
H20B C20 H20C . . . 109.5 n
C19 C18 C17 . . . 121.2(2) n
C19 C18 H18 . . . 119.4 n
C17 C18 H18 . . . 119.4 n
C21 C22 H22A . . . 109.5 n
C21 C22 H22B . . . 109.5 n
C21 C22 H22C . . . 109.5 n
H22A C22 H22B . . . 109.5 n
H22A C22 H22C . . . 109.5 n
H22B C22 H22C . . . 109.5 n
C23 C25 H25A . . . 109.5 n
C23 C25 H25B . . . 109.5 n
C23 C25 H25C . . . 109.5 n
H25A C25 H25B . . . 109.5 n
H25A C25 H25C . . . 109.5 n
H25B C25 H25C . . . 109.5 n
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_site_symmetry_1
_geom_bond_site_symmetry_2
_geom_bond_distance
_geom_bond_publ_flag
Sb1 Br1 . . 2.5989(14) y
Sb1 Br2 . . 2.5172(7) y
Sb1 N1 . . 2.091(2) y
Sb1 N2 . . 2.435(2) y
N1 C1 . . 1.433(3) n
N1 C13 . . 1.348(3) n
N2 C14 . . 1.424(3) n
N2 C13 . . 1.295(3) n
C10 H10 . . 1.0000 n
C10 C2 . . 1.521(3) n
C10 C12 . . 1.534(3) n
C10 C11 . . 1.531(3) n
C3 H3 . . 0.9500 n
C3 C2 . . 1.397(3) n
C3 C4 . . 1.387(3) n
C1 C6 . . 1.409(3) n
C1 C2 . . 1.405(3) n
C14 C15 . . 1.405(3) n
C14 C19 . . 1.414(3) n
C6 C7 . . 1.519(3) n
C6 C5 . . 1.396(3) n
C13 H13 . . 0.9500 n
C7 H7 . . 1.0000 n
C7 C8 . . 1.534(4) n
C7 C9 . . 1.531(3) n
C23 H23 . . 1.0000 n
C23 C15 . . 1.522(3) n
C23 C24 . . 1.533(3) n
C23 C25 . . 1.529(4) n
C16 H16 . . 0.9500 n
C16 C15 . . 1.401(3) n
C16 C17 . . 1.389(3) n
C5 H5 . . 0.9500 n
C5 C4 . . 1.390(3) n
C4 H4 . . 0.9500 n
C21 H21 . . 1.0000 n
C21 C19 . . 1.517(3) n
C21 C20 . . 1.539(4) n
C21 C22 . . 1.534(3) n
C8 H8A . . 0.9800 n
C8 H8B . . 0.9800 n
C8 H8C . . 0.9800 n
C19 C18 . . 1.394(3) n
C12 H12A . . 0.9800 n
C12 H12B . . 0.9800 n
C12 H12C . . 0.9800 n
C9 H9A . . 0.9800 n
C9 H9B . . 0.9800 n
C9 H9C . . 0.9800 n
C17 H17 . . 0.9500 n
C17 C18 . . 1.396(4) n
C11 H11A . . 0.9800 n
C11 H11B . . 0.9800 n
C11 H11C . . 0.9800 n
C24 H24A . . 0.9800 n
C24 H24B . . 0.9800 n
C24 H24C . . 0.9800 n
C20 H20A . . 0.9800 n
C20 H20B . . 0.9800 n
C20 H20C . . 0.9800 n
C18 H18 . . 0.9500 n
C22 H22A . . 0.9800 n
C22 H22B . . 0.9800 n
C22 H22C . . 0.9800 n
C25 H25A . . 0.9800 n
C25 H25B . . 0.9800 n
C25 H25C . . 0.9800 n
loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_2
_geom_torsion_site_symmetry_3
_geom_torsion_site_symmetry_4
_geom_torsion
_geom_torsion_publ_flag
Sb1 N1 C1 C6 . . . . -108.4(2) n
Sb1 N1 C1 C2 . . . . 73.6(3) n
Sb1 N1 C13 N2 . . . . 7.3(2) n
Sb1 N2 C14 C15 . . . . 121.3(3) n
Sb1 N2 C14 C19 . . . . -54.6(4) n
Sb1 N2 C13 N1 . . . . -6.15(17) n
N1 C1 C6 C7 . . . . 8.8(3) n
N1 C1 C6 C5 . . . . -174.5(2) n
N1 C1 C2 C10 . . . . -6.2(3) n
N1 C1 C2 C3 . . . . 172.88(19) n
N2 C14 C15 C23 . . . . -0.3(3) n
N2 C14 C15 C16 . . . . 179.6(2) n
N2 C14 C19 C21 . . . . 3.2(3) n
N2 C14 C19 C18 . . . . -179.3(2) n
C1 N1 C13 N2 . . . . -179.69(18) n
C1 C6 C7 C8 . . . . -138.4(2) n
C1 C6 C7 C9 . . . . 97.8(3) n
C1 C6 C5 C4 . . . . 0.3(3) n
C14 N2 C13 N1 . . . . -178.20(19) n
C14 C19 C18 C17 . . . . -1.7(3) n
C6 C1 C2 C10 . . . . 175.9(2) n
C6 C1 C2 C3 . . . . -5.1(3) n
C6 C5 C4 C3 . . . . -2.3(4) n
C2 C3 C4 C5 . . . . 0.6(4) n
C2 C1 C6 C7 . . . . -173.3(2) n
C2 C1 C6 C5 . . . . 3.4(3) n
C13 N1 C1 C6 . . . . 81.8(3) n
C13 N1 C1 C2 . . . . -96.2(2) n
C13 N2 C14 C15 . . . . -74.5(3) n
C13 N2 C14 C19 . . . . 109.5(2) n
C7 C6 C5 C4 . . . . 177.1(2) n
C16 C17 C18 C19 . . . . -1.4(4) n
C5 C6 C7 C8 . . . . 45.0(3) n
C5 C6 C7 C9 . . . . -78.8(3) n
C4 C3 C2 C10 . . . . -177.9(2) n
C4 C3 C2 C1 . . . . 3.0(3) n
C21 C19 C18 C17 . . . . 175.8(2) n
C15 C14 C19 C21 . . . . -172.7(2) n
C15 C14 C19 C18 . . . . 4.8(3) n
C15 C16 C17 C18 . . . . 1.5(4) n
C19 C14 C15 C23 . . . . 175.5(2) n
C19 C14 C15 C16 . . . . -4.7(3) n
C12 C10 C2 C3 . . . . 45.4(3) n
C12 C10 C2 C1 . . . . -135.5(2) n
C17 C16 C15 C14 . . . . 1.5(4) n
C17 C16 C15 C23 . . . . -178.7(2) n
C11 C10 C2 C3 . . . . -79.3(3) n
C11 C10 C2 C1 . . . . 99.8(2) n
C24 C23 C15 C14 . . . . -138.5(2) n
C24 C23 C15 C16 . . . . 41.6(3) n
C20 C21 C19 C14 . . . . 82.1(2) n
C20 C21 C19 C18 . . . . -95.3(3) n
C22 C21 C19 C14 . . . . -155.0(2) n
C22 C21 C19 C18 . . . . 27.6(3) n
C25 C23 C15 C14 . . . . 97.3(3) n
C25 C23 C15 C16 . . . . -82.5(3) n

_cod_database_fobs_code 2022435
