#------------------------------------------------------------------------------ #$Date: 2022-02-16 04:56:49 +0200 (Wed, 16 Feb 2022) $ #$Revision: 272987 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/02/25/2022556.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2022556 _cell_angle_alpha 90.000 _cell_angle_beta 99.864 _cell_angle_gamma 90.000 _cell_length_a 10.2225 _cell_length_b 6.4019 _cell_length_c 19.2034 _exptl_crystal_F_000 596.00 _reflns_d_resolution_high 0.8019 _cod_data_source_file um5054mo_sp20049_0m_2p1201GPasup19.hkl _cod_data_source_block mo_sp20049_0m_2p1201GPa _shelx_title ' mo_sp20049_0m_a.res in P2(1)/n' _shelx_refln_list_code 4 _shelx_f_calc_maximum 124.63 _shelx_f_squared_multiplier 1.000 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 4 0 0 3991.83 4049.88 51.23 o 6 0 0 975.51 1089.12 14.38 o 8 0 0 11.58 9.11 2.86 o 10 0 0 91.77 92.44 7.98 o 1 1 0 445.14 396.81 2.51 o 2 1 0 797.51 714.57 5.10 o 3 1 0 93.56 91.95 1.09 o 4 1 0 1344.48 1350.23 10.72 o 5 1 0 3.86 4.94 0.79 o 6 1 0 240.25 230.00 2.72 o 7 1 0 120.57 121.99 3.18 o 8 1 0 0.29 -0.28 2.22 o 9 1 0 38.50 35.86 2.59 o 10 1 0 0.49 4.98 3.70 o 11 1 0 3.71 2.08 6.15 o 2 2 0 110.02 119.47 1.34 o 3 2 0 2.07 1.63 0.74 o 4 2 0 381.38 389.08 3.48 o 5 2 0 65.94 75.19 2.26 o 6 2 0 39.70 39.31 1.31 o 7 2 0 248.05 252.50 3.71 o 8 2 0 199.55 219.21 5.91 o 9 2 0 1.27 0.89 3.22 o 10 2 0 5.71 5.80 3.66 o 11 2 0 3.88 -1.04 6.47 o 1 3 0 1087.43 1066.95 11.84 o 2 3 0 1.49 1.62 0.97 o 4 3 0 96.20 97.81 1.84 o 5 3 0 81.05 89.88 2.01 o 6 3 0 116.36 121.33 2.63 o 7 3 0 70.89 74.18 2.53 o 8 3 0 0.04 -1.36 2.54 o 9 3 0 12.03 9.18 3.50 o 10 3 0 2.98 9.97 4.17 o 11 3 0 35.15 36.21 5.21 o 0 4 0 532.42 560.75 9.95 o 1 4 0 9823.28 10338.93 97.36 o 2 4 0 438.78 443.24 6.86 o 3 4 0 50.21 51.37 2.69 o 4 4 0 3.81 3.17 1.73 o 5 4 0 16.97 15.70 2.25 o 6 4 0 105.29 107.84 2.89 o 7 4 0 418.70 414.45 10.33 o 8 4 0 48.47 44.74 5.12 o 9 4 0 6.73 7.18 3.95 o 10 4 0 3.24 7.74 4.52 o 1 5 0 295.84 293.57 7.43 o 2 5 0 57.07 43.86 8.14 o 3 5 0 38.57 38.80 4.91 o 4 5 0 21.41 17.76 3.72 o 5 5 0 13.33 7.61 3.98 o 6 5 0 0.10 3.52 2.83 o 7 5 0 11.19 9.87 3.50 o 8 5 0 53.62 61.17 5.80 o 9 5 0 3.50 16.06 7.11 o 0 6 0 3308.47 3415.85 79.48 o 1 6 0 90.94 87.50 8.46 o 2 6 0 457.37 462.31 15.85 o 3 6 0 6.53 9.08 9.14 o 4 6 0 31.57 29.29 11.82 o 5 6 0 103.93 98.94 10.28 o 6 6 0 20.10 34.03 30.72 o 7 6 0 6.82 12.71 22.57 o 8 6 0 1.39 -12.13 14.27 o 1 7 0 17.89 10.62 12.28 o 2 7 0 37.08 47.67 11.40 o 3 7 0 3.98 19.98 10.88 o 4 7 0 26.71 35.76 11.26 o 5 7 0 6.01 -4.52 18.52 o -11 0 1 37.80 26.45 10.59 o -9 0 1 88.88 76.87 5.23 o -7 0 1 13.18 12.81 2.08 o -5 0 1 2526.89 2771.02 27.39 o -3 0 1 136.23 133.22 1.88 o -1 0 1 914.26 875.51 35.58 o 3 0 1 877.95 824.93 9.87 o 5 0 1 858.96 871.02 12.63 o 7 0 1 122.39 122.18 5.11 o 9 0 1 580.39 601.45 10.99 o 11 0 1 57.82 57.94 12.96 o -12 1 1 3.18 0.28 9.22 o -11 1 1 11.51 19.92 6.52 o -10 1 1 16.57 23.22 3.84 o -9 1 1 68.60 63.61 3.65 o -8 1 1 144.11 143.08 6.90 o -7 1 1 11.26 11.71 1.70 o -6 1 1 28.09 24.87 1.05 o -5 1 1 373.49 369.79 2.83 o -4 1 1 176.64 176.00 1.58 o -3 1 1 265.53 263.77 2.09 o -2 1 1 401.49 382.31 2.77 o -1 1 1 1441.65 1449.31 10.13 o 0 1 1 833.04 765.87 7.41 o 1 1 1 1955.13 1726.68 13.90 o 2 1 1 290.25 283.50 2.41 o 3 1 1 660.33 594.80 4.79 o 4 1 1 189.72 187.55 2.95 o 5 1 1 426.25 422.92 4.49 o 6 1 1 18.64 20.49 1.63 o 7 1 1 106.84 108.42 2.96 o 8 1 1 43.29 40.63 2.88 o 9 1 1 7.49 5.63 2.43 o 10 1 1 0.68 -1.10 2.77 o 11 1 1 57.42 57.05 4.82 o -12 2 1 14.79 22.59 22.89 o -11 2 1 6.36 1.93 5.99 o -10 2 1 2.76 -0.32 4.04 o -9 2 1 5.64 7.58 3.23 o -8 2 1 20.23 25.20 3.08 o -7 2 1 272.19 278.95 4.02 o -6 2 1 6.14 7.78 1.19 o -5 2 1 187.27 193.68 2.12 o -4 2 1 62.73 64.67 1.09 o -3 2 1 31.83 31.88 0.98 o -2 2 1 275.63 260.53 2.03 o -1 2 1 2924.95 2962.85 26.82 o 0 2 1 15532.47 14693.60 203.45 o 1 2 1 11484.28 11050.26 114.13 o 2 2 1 99.18 98.66 1.71 o 3 2 1 0.60 6.62 1.33 o 4 2 1 473.14 465.25 4.50 o 5 2 1 0.00 1.12 1.10 o 6 2 1 38.67 39.90 1.62 o 7 2 1 229.52 242.43 5.01 o 8 2 1 158.91 152.03 3.63 o 9 2 1 31.31 29.61 2.66 o 10 2 1 0.47 1.78 3.34 o 11 2 1 12.02 8.74 4.70 o -11 3 1 0.64 8.59 5.88 o -10 3 1 7.27 3.89 4.16 o -9 3 1 22.71 29.17 4.55 o -8 3 1 20.59 21.82 3.26 o -7 3 1 9.05 11.36 2.82 o -6 3 1 208.16 218.19 3.81 o -5 3 1 61.21 58.93 2.04 o -4 3 1 203.14 196.53 2.31 o -3 3 1 50.65 49.70 1.29 o -2 3 1 68.22 76.64 1.74 o -1 3 1 126.52 123.15 3.44 o 0 3 1 823.79 799.03 8.45 o 1 3 1 0.20 -1.28 2.13 o 2 3 1 553.15 603.04 6.20 o 3 3 1 172.52 177.45 2.45 o 4 3 1 144.04 121.34 2.02 o 5 3 1 1.83 1.31 1.19 o 6 3 1 0.07 -1.42 1.42 o 7 3 1 69.88 72.43 3.59 o 8 3 1 89.06 91.21 3.05 o 9 3 1 1.49 2.97 3.00 o 10 3 1 0.65 0.40 3.40 o 11 3 1 5.70 -1.72 5.57 o -10 4 1 0.24 0.11 4.83 o -9 4 1 5.94 6.87 4.50 o -8 4 1 91.24 88.38 4.31 o -7 4 1 2.79 1.65 3.37 o -6 4 1 80.72 77.18 4.36 o -5 4 1 6.71 6.72 1.71 o -4 4 1 8.33 7.80 1.46 o -3 4 1 73.57 78.01 2.05 o -2 4 1 43.37 49.04 3.14 o -1 4 1 259.38 286.80 7.77 o 0 4 1 5408.33 5467.47 50.09 o 1 4 1 119.27 125.43 4.58 o 2 4 1 82.89 79.33 3.81 o 3 4 1 95.63 93.09 3.15 o 4 4 1 253.22 264.04 7.31 o 5 4 1 2.01 2.65 2.17 o 6 4 1 182.86 210.82 5.27 o 7 4 1 125.94 125.40 3.63 o 8 4 1 405.11 438.19 7.87 o 9 4 1 0.12 0.10 4.75 o 10 4 1 5.13 3.80 5.27 o -9 5 1 41.36 46.31 6.49 o -8 5 1 1.90 6.11 5.52 o -7 5 1 70.54 81.50 4.76 o -6 5 1 274.04 257.25 6.63 o -5 5 1 32.24 35.82 4.31 o -4 5 1 71.54 75.90 4.37 o -3 5 1 21.78 23.53 5.48 o -2 5 1 2.17 5.13 6.03 o -1 5 1 254.06 250.78 6.81 o 0 5 1 320.38 287.02 15.50 o 1 5 1 0.81 -5.20 5.81 o 2 5 1 20.28 14.81 8.64 o 3 5 1 18.70 16.90 6.00 o 4 5 1 38.11 45.51 3.46 o 5 5 1 23.87 19.40 3.51 o 6 5 1 56.92 57.81 4.12 o 7 5 1 26.92 28.56 4.70 o 8 5 1 7.99 8.82 6.08 o 9 5 1 3.12 3.41 6.82 o -8 6 1 0.13 -9.49 20.48 o -6 6 1 0.00 -6.56 10.83 o -5 6 1 28.46 27.62 9.56 o -4 6 1 3.80 2.16 11.66 o -3 6 1 63.50 61.22 8.63 o -2 6 1 16.19 11.28 7.99 o -1 6 1 431.87 417.15 12.14 o 0 6 1 1558.85 1596.71 24.07 o 1 6 1 435.00 463.40 12.62 o 2 6 1 381.62 387.91 13.21 o 3 6 1 5.62 10.05 7.02 o 4 6 1 38.50 16.93 8.47 o 5 6 1 0.18 5.37 7.63 o 6 6 1 37.08 -16.11 32.98 o 7 6 1 27.95 14.17 14.35 o 8 6 1 2.53 -15.42 17.85 o -5 7 1 6.81 18.52 18.82 o -4 7 1 23.44 8.74 10.91 o -3 7 1 1.01 -10.30 10.72 o -2 7 1 56.62 43.94 10.13 o -1 7 1 142.63 150.61 13.00 o 0 7 1 27.59 18.95 12.95 o 1 7 1 14.62 -5.97 17.85 o 2 7 1 10.83 -4.70 11.36 o 3 7 1 3.34 3.44 20.24 o 4 7 1 3.42 -10.98 10.98 o 5 7 1 10.67 30.42 19.28 o -12 0 2 0.25 13.53 10.32 o -10 0 2 15.93 4.60 4.20 o -8 0 2 7.48 9.34 3.02 o -6 0 2 0.39 0.22 1.37 o -4 0 2 2851.92 2729.79 34.77 o -2 0 2 490.56 463.39 7.57 o 2 0 2 63.00 55.45 1.37 o 4 0 2 212.72 209.21 3.08 o 6 0 2 0.00 1.19 1.65 o 8 0 2 141.51 136.65 16.88 o 10 0 2 5.20 1.07 3.89 o -12 1 2 5.87 -4.98 14.91 o -11 1 2 31.35 21.13 8.16 o -10 1 2 8.83 7.11 3.31 o -9 1 2 0.00 3.68 2.53 o -8 1 2 78.39 83.03 3.74 o -7 1 2 10.35 10.08 1.52 o -6 1 2 729.81 798.97 6.70 o -5 1 2 804.99 847.30 6.77 o -4 1 2 261.58 260.80 2.61 o -3 1 2 163.86 157.51 1.61 o -2 1 2 57.57 55.73 0.88 o -1 1 2 30.53 32.17 1.18 o 0 1 2 5872.64 5098.09 79.00 o 2 1 2 107.38 94.41 1.85 o 3 1 2 79.17 78.98 1.32 o 4 1 2 67.24 67.32 1.95 o 5 1 2 16.10 17.48 1.04 o 6 1 2 331.67 336.04 6.84 o 7 1 2 65.77 69.64 2.57 o 8 1 2 78.82 83.40 3.37 o 9 1 2 2.29 3.06 2.82 o 10 1 2 16.90 16.99 2.88 o 11 1 2 0.30 2.96 3.39 o -12 2 2 1.08 1.95 10.46 o -11 2 2 6.50 17.60 6.60 o -10 2 2 1.52 2.48 4.07 o -9 2 2 2.28 0.75 2.80 o -8 2 2 50.49 53.17 3.95 o -7 2 2 51.86 54.99 2.03 o -6 2 2 117.41 123.15 2.10 o -5 2 2 970.04 1000.74 7.79 o -4 2 2 822.77 853.25 7.26 o -3 2 2 770.97 762.12 5.92 o -2 2 2 1625.85 1626.88 13.39 o -1 2 2 2061.24 1927.96 18.51 o 0 2 2 8.05 6.77 1.39 o 1 2 2 1129.32 1051.49 11.04 o 2 2 2 0.00 0.99 0.79 o 3 2 2 214.68 237.80 3.44 o 4 2 2 74.12 78.46 1.93 o 5 2 2 446.53 416.15 6.11 o 6 2 2 31.45 34.94 1.71 o 7 2 2 36.47 34.90 2.64 o 8 2 2 0.64 3.11 2.80 o 9 2 2 54.87 48.33 2.82 o 10 2 2 54.29 51.16 3.19 o 11 2 2 43.98 41.71 4.41 o -11 3 2 108.32 107.31 8.55 o -10 3 2 1.56 -3.64 4.41 o -9 3 2 118.78 103.88 8.60 o -8 3 2 151.55 134.40 7.98 o -7 3 2 177.08 196.08 11.81 o -6 3 2 547.02 575.68 5.81 o -5 3 2 1080.63 1152.88 9.39 o -4 3 2 0.52 0.77 1.04 o -3 3 2 480.74 514.70 4.92 o -2 3 2 525.71 505.27 4.38 o -1 3 2 295.07 309.03 5.41 o 0 3 2 2.25 -0.08 2.58 o 1 3 2 12.86 13.11 1.65 o 2 3 2 181.71 181.96 2.63 o 3 3 2 414.46 412.20 4.21 o 4 3 2 13.18 11.74 1.31 o 5 3 2 22.08 25.52 1.51 o 6 3 2 6.38 8.41 1.87 o 7 3 2 429.13 445.98 7.17 o 8 3 2 42.10 40.13 3.43 o 9 3 2 3.49 0.90 3.11 o 10 3 2 5.22 8.49 3.99 o 11 3 2 3.94 6.12 10.49 o -11 4 2 7.96 7.72 6.34 o -10 4 2 2.57 8.37 5.78 o -9 4 2 6.79 -0.82 4.41 o -8 4 2 22.45 21.16 4.36 o -7 4 2 77.85 80.64 3.60 o -6 4 2 0.73 0.28 1.95 o -5 4 2 550.54 546.01 8.30 o -4 4 2 87.41 85.49 1.98 o -3 4 2 325.20 322.24 3.94 o -2 4 2 136.28 142.37 4.78 o -1 4 2 221.93 245.21 6.34 o 0 4 2 573.45 605.48 15.09 o 1 4 2 319.20 349.40 7.68 o 2 4 2 576.22 562.49 8.13 o 3 4 2 1.52 1.49 1.88 o 4 4 2 24.70 23.69 2.74 o 5 4 2 0.03 -0.36 2.12 o 6 4 2 207.96 239.18 5.71 o 7 4 2 404.86 415.68 8.75 o 8 4 2 104.59 110.72 5.49 o 9 4 2 3.75 2.15 3.82 o 10 4 2 12.39 21.23 14.00 o -9 5 2 0.54 2.48 6.43 o -8 5 2 5.53 4.33 4.71 o -7 5 2 0.68 0.12 3.30 o -6 5 2 37.00 37.93 3.62 o -5 5 2 542.18 537.00 7.28 o -4 5 2 99.21 107.13 4.88 o -3 5 2 15.59 9.72 5.02 o -2 5 2 54.51 42.30 8.64 o -1 5 2 0.81 4.54 5.94 o 0 5 2 0.05 7.44 5.87 o 1 5 2 77.42 61.13 7.17 o 2 5 2 7.38 14.00 7.01 o 3 5 2 63.10 53.99 2.91 o 4 5 2 0.07 -1.49 3.74 o 5 5 2 25.35 23.02 2.55 o 6 5 2 5.08 12.04 3.14 o 7 5 2 120.12 110.78 4.54 o 8 5 2 0.01 -7.53 7.53 o 9 5 2 15.87 23.94 15.96 o -8 6 2 4.27 -19.13 19.13 o -6 6 2 6.52 -11.68 12.42 o -5 6 2 85.18 70.95 12.00 o -4 6 2 213.47 204.09 10.24 o -3 6 2 22.88 5.56 7.75 o -2 6 2 5.69 7.92 6.18 o -1 6 2 171.45 148.74 8.92 o 0 6 2 62.42 61.27 7.23 o 1 6 2 377.37 372.04 15.09 o 2 6 2 103.37 108.08 11.02 o 3 6 2 63.99 37.64 9.48 o 4 6 2 1.16 -1.77 7.69 o 5 6 2 28.23 25.72 9.06 o 6 6 2 51.06 41.65 10.17 o 7 6 2 256.25 226.64 11.74 o -5 7 2 90.24 102.39 20.03 o -4 7 2 28.72 33.88 21.99 o -3 7 2 9.38 25.61 11.66 o -2 7 2 2.12 21.35 14.09 o -1 7 2 43.87 42.32 21.86 o 0 7 2 67.84 54.65 8.65 o 1 7 2 39.80 34.68 14.74 o 2 7 2 0.84 -7.75 14.85 o 3 7 2 12.18 -0.25 9.44 o 4 7 2 1.66 5.88 8.89 o -11 0 3 1.48 4.97 5.24 o -9 0 3 6.66 9.09 3.95 o -7 0 3 1.61 -0.82 2.83 o -5 0 3 669.96 707.77 11.27 o -3 0 3 1029.77 998.62 14.34 o 5 0 3 0.51 0.32 1.13 o 7 0 3 3559.61 3364.63 171.96 o 9 0 3 1756.86 1671.62 31.64 o 11 0 3 0.27 6.78 6.24 o -12 1 3 0.01 -0.04 6.04 o -11 1 3 64.09 48.77 5.66 o -10 1 3 1.73 6.31 3.20 o -9 1 3 37.80 42.90 3.08 o -8 1 3 2.66 2.29 1.80 o -7 1 3 228.82 212.91 3.85 o -6 1 3 331.65 347.08 3.77 o -5 1 3 8184.73 8738.23 85.63 o -4 1 3 497.16 523.10 4.45 o -3 1 3 2350.03 2325.04 19.95 o -2 1 3 0.07 -0.13 0.92 o 3 1 3 1422.61 1183.84 26.35 o 4 1 3 35.06 30.27 1.03 o 5 1 3 491.38 496.01 4.62 o 6 1 3 146.65 143.48 2.62 o 7 1 3 1218.32 1203.31 15.77 o 8 1 3 15.38 15.40 2.64 o 9 1 3 14.02 14.02 2.65 o 10 1 3 0.75 -2.38 3.25 o 11 1 3 0.30 -0.43 6.45 o -12 2 3 1.24 -6.98 9.70 o -11 2 3 1.19 0.18 11.87 o -10 2 3 2.34 -2.50 3.33 o -9 2 3 0.28 -1.52 2.74 o -8 2 3 0.63 -0.47 2.38 o -7 2 3 0.87 -1.63 1.63 o -6 2 3 0.31 1.35 1.35 o -5 2 3 139.02 150.58 2.96 o -4 2 3 813.86 788.99 7.01 o -3 2 3 332.93 362.60 8.39 o -2 2 3 18.09 19.78 1.28 o -1 2 3 402.65 385.67 5.72 o 0 2 3 5.61 4.23 1.71 o 1 2 3 597.56 577.46 16.97 o 2 2 3 580.84 585.99 8.92 o 3 2 3 11.99 13.34 1.36 o 4 2 3 38.17 42.46 1.86 o 5 2 3 53.67 55.26 1.82 o 6 2 3 893.81 889.64 8.63 o 7 2 3 1907.20 1942.48 22.73 o 8 2 3 3613.71 3725.32 41.90 o 9 2 3 687.06 692.93 9.88 o 10 2 3 226.11 200.40 7.89 o 11 2 3 7.67 15.89 8.06 o -11 3 3 2.32 7.36 9.60 o -10 3 3 8.52 8.79 3.98 o -9 3 3 72.14 70.83 4.73 o -8 3 3 458.39 476.73 8.51 o -7 3 3 376.11 380.07 5.61 o -6 3 3 2384.86 2500.14 21.01 o -5 3 3 97.85 107.30 3.24 o -4 3 3 1387.72 1438.37 11.98 o -3 3 3 442.42 445.43 4.18 o -2 3 3 469.27 511.05 5.91 o -1 3 3 179.65 183.70 4.37 o 0 3 3 649.20 643.87 8.27 o 1 3 3 5.45 2.94 2.33 o 2 3 3 454.57 463.43 5.10 o 3 3 3 183.06 189.12 2.93 o 4 3 3 160.91 164.96 2.65 o 5 3 3 14.60 15.44 1.69 o 6 3 3 67.14 64.47 3.49 o 7 3 3 381.36 388.73 12.69 o 8 3 3 4.58 4.33 3.05 o 9 3 3 0.07 -4.88 4.88 o 10 3 3 0.17 -1.45 9.31 o 11 3 3 2.35 10.43 10.36 o -11 4 3 0.62 3.79 7.13 o -10 4 3 2.71 0.17 5.32 o -9 4 3 0.00 -3.25 4.28 o -8 4 3 1.51 1.25 3.32 o -7 4 3 9.10 6.09 3.26 o -6 4 3 0.43 -1.81 1.81 o -5 4 3 0.13 0.63 1.55 o -4 4 3 492.04 501.03 5.50 o -3 4 3 24.76 23.76 1.35 o -2 4 3 58.47 67.90 4.46 o -1 4 3 82.59 82.65 4.30 o 0 4 3 369.03 376.81 8.03 o 1 4 3 4.28 10.92 3.60 o 2 4 3 0.75 3.04 1.80 o 3 4 3 51.41 51.12 1.89 o 4 4 3 31.69 33.40 1.70 o 5 4 3 0.00 7.17 4.43 o 6 4 3 175.59 196.68 6.44 o 7 4 3 101.94 105.77 3.72 o 8 4 3 1970.94 2147.63 139.73 o 9 4 3 231.33 241.53 14.83 o 10 4 3 30.69 24.40 9.90 o -9 5 3 2.48 6.98 8.04 o -8 5 3 25.34 25.03 4.95 o -7 5 3 99.61 94.34 5.13 o -6 5 3 324.85 301.22 6.47 o -5 5 3 275.34 270.48 5.43 o -4 5 3 295.46 310.96 5.04 o -3 5 3 24.89 17.48 6.29 o -2 5 3 0.01 -7.72 7.91 o -1 5 3 69.13 66.48 9.44 o 0 5 3 54.34 28.53 7.27 o 1 5 3 20.60 17.07 10.14 o 2 5 3 53.63 53.68 7.68 o 3 5 3 31.01 29.38 4.51 o 4 5 3 12.96 20.51 5.49 o 5 5 3 0.27 -2.69 2.69 o 6 5 3 98.11 99.49 4.23 o 7 5 3 22.54 18.52 10.84 o -8 6 3 0.59 -9.49 19.73 o -7 6 3 0.92 -30.72 30.72 o -6 6 3 4.15 0.73 13.98 o -5 6 3 30.71 39.54 9.95 o -4 6 3 79.54 56.11 9.55 o -3 6 3 42.04 38.57 7.17 o -2 6 3 1.54 10.16 10.72 o -1 6 3 11.73 7.80 9.13 o 0 6 3 10.42 20.02 8.57 o 1 6 3 0.69 7.90 11.45 o 2 6 3 0.43 -0.91 8.79 o 3 6 3 10.94 30.62 11.84 o 4 6 3 2.94 4.08 9.25 o -5 7 3 420.79 378.69 25.45 o -4 7 3 1.04 -11.16 11.16 o -3 7 3 85.79 54.67 11.60 o -2 7 3 28.56 30.56 8.97 o -1 7 3 44.33 7.12 9.61 o 0 7 3 205.94 187.94 9.53 o 1 7 3 63.36 34.01 8.91 o 2 7 3 0.48 -6.77 10.75 o 3 7 3 9.11 46.83 18.97 o -12 0 4 44.34 39.02 6.33 o -10 0 4 197.35 205.77 8.71 o -8 0 4 40.81 37.82 4.46 o -6 0 4 98.05 93.00 3.11 o -4 0 4 1226.76 1290.49 18.62 o 8 0 4 6300.34 6443.90 200.87 o -12 1 4 27.56 28.58 5.12 o -11 1 4 6.82 6.56 4.75 o -10 1 4 495.74 497.93 9.43 o -9 1 4 10.10 13.22 2.24 o -8 1 4 26.75 20.65 2.27 o -7 1 4 24.78 29.28 2.28 o -6 1 4 4.55 1.40 1.63 o -5 1 4 442.86 467.40 4.52 o -4 1 4 298.53 296.08 3.53 o -3 1 4 95.34 95.64 3.22 o 5 1 4 158.87 171.82 3.74 o 6 1 4 492.00 470.49 7.70 o 7 1 4 146.06 156.00 11.60 o 8 1 4 571.48 561.19 22.29 o -12 2 4 41.43 39.13 9.58 o -11 2 4 19.91 11.07 5.15 o -10 2 4 52.97 59.32 5.67 o -9 2 4 34.90 34.13 2.85 o -8 2 4 2.31 4.11 2.55 o -7 2 4 109.84 116.04 2.63 o -6 2 4 3.30 3.22 1.70 o -5 2 4 34.82 32.06 1.55 o -4 2 4 345.06 355.97 4.11 o -3 2 4 77.40 87.80 2.41 o -2 2 4 68.48 65.16 2.87 o -1 2 4 778.82 708.65 11.16 o 0 2 4 1073.95 1027.20 24.42 o 4 2 4 51.36 53.31 2.41 o 5 2 4 6.12 5.96 1.67 o 6 2 4 3.79 6.80 2.95 o 7 2 4 562.57 544.33 23.04 o 8 2 4 1819.66 1870.93 42.75 o 9 2 4 790.85 784.42 20.42 o -11 3 4 38.32 32.10 9.66 o -10 3 4 12.07 17.44 4.21 o -9 3 4 367.36 410.39 7.97 o -8 3 4 141.91 142.86 3.80 o -7 3 4 232.30 255.56 6.76 o -6 3 4 116.15 115.55 2.63 o -5 3 4 255.47 278.83 3.98 o -4 3 4 62.49 62.67 1.51 o -3 3 4 678.25 699.44 7.10 o -2 3 4 40.89 48.31 1.55 o -1 3 4 262.09 257.59 6.96 o 0 3 4 6.85 4.22 2.49 o 1 3 4 91.66 88.22 4.73 o 2 3 4 502.59 515.88 7.48 o 3 3 4 498.59 504.49 6.20 o 4 3 4 14.87 15.12 2.06 o 5 3 4 13.91 15.02 2.40 o 6 3 4 9.01 6.48 4.19 o 7 3 4 1820.37 1992.28 66.11 o 8 3 4 11.11 10.06 5.42 o 9 3 4 72.35 69.11 5.38 o -11 4 4 15.64 13.75 6.18 o -10 4 4 0.25 -2.11 5.18 o -9 4 4 40.17 40.96 4.19 o -8 4 4 28.79 37.05 4.52 o -7 4 4 122.34 127.71 3.43 o -6 4 4 32.19 33.40 2.16 o -5 4 4 13.20 11.30 1.90 o -4 4 4 26.79 24.59 1.95 o -3 4 4 2.14 1.49 1.05 o -2 4 4 74.18 61.64 5.03 o -1 4 4 69.97 78.65 4.55 o 0 4 4 0.53 0.36 3.93 o 1 4 4 145.52 130.65 4.55 o 2 4 4 5.46 2.51 5.04 o 3 4 4 37.99 37.37 3.52 o 4 4 4 1.14 2.95 4.20 o 5 4 4 12.26 10.26 2.79 o 6 4 4 14.59 14.61 3.44 o 7 4 4 1029.87 965.95 33.73 o 8 4 4 2.15 -4.57 4.57 o 9 4 4 1240.79 1339.82 48.79 o -9 5 4 52.52 43.16 8.02 o -8 5 4 1.49 4.68 3.84 o -7 5 4 33.25 27.62 3.53 o -6 5 4 53.02 53.94 3.70 o -5 5 4 228.43 220.24 3.88 o -4 5 4 16.54 22.32 3.78 o -3 5 4 263.86 262.83 13.15 o -2 5 4 1.48 13.39 9.14 o -1 5 4 0.00 -8.79 9.41 o 0 5 4 3.82 -1.34 7.87 o 1 5 4 55.99 48.92 8.65 o 2 5 4 17.35 16.58 10.01 o 3 5 4 50.14 15.81 9.63 o 4 5 4 5.97 -6.08 6.08 o 5 5 4 33.69 34.40 4.76 o 6 5 4 72.43 82.06 5.01 o 7 5 4 737.66 735.52 56.61 o -8 6 4 2.17 1.66 18.22 o -7 6 4 1.70 10.09 21.69 o -6 6 4 0.35 -10.64 11.68 o -5 6 4 1.97 7.23 12.89 o -4 6 4 4.33 -1.41 6.89 o -3 6 4 0.47 19.61 8.61 o -2 6 4 10.08 2.70 7.88 o -1 6 4 3.39 4.43 9.24 o 0 6 4 13.19 14.40 8.47 o 1 6 4 40.36 25.83 12.55 o 2 6 4 0.92 -11.24 14.64 o 3 6 4 25.09 -3.50 14.16 o 4 6 4 6.58 -3.46 28.46 o 5 6 4 0.68 40.51 27.71 o -4 7 4 45.25 30.53 25.90 o -3 7 4 26.85 11.71 37.87 o -2 7 4 48.01 30.42 34.79 o -1 7 4 33.66 23.27 20.96 o 0 7 4 35.81 23.21 19.43 o 1 7 4 99.46 111.22 22.21 o 2 7 4 0.37 5.07 16.13 o 3 7 4 2.07 -33.58 33.58 o -11 0 5 167.71 161.46 10.12 o -9 0 5 15.90 15.86 4.96 o -7 0 5 0.34 -2.36 4.31 o -5 0 5 348.44 328.00 5.10 o -12 1 5 0.25 9.32 4.47 o -11 1 5 97.41 93.28 9.69 o -10 1 5 185.04 171.38 4.41 o -9 1 5 445.80 440.30 7.03 o -8 1 5 186.25 163.48 4.18 o -7 1 5 165.49 171.05 6.42 o -6 1 5 449.95 483.77 7.09 o -5 1 5 104.49 101.97 1.84 o -4 1 5 275.72 299.17 7.10 o -12 2 5 56.19 43.12 8.19 o -11 2 5 54.72 38.72 5.49 o -10 2 5 244.65 284.91 5.99 o -9 2 5 92.59 89.54 2.86 o -8 2 5 36.57 44.67 4.57 o -7 2 5 179.82 172.81 4.66 o -6 2 5 12.59 12.91 1.82 o -5 2 5 9.47 9.40 1.31 o -4 2 5 142.49 166.13 3.36 o -3 2 5 103.60 114.91 5.05 o -11 3 5 2.91 10.85 6.46 o -10 3 5 380.64 388.95 10.21 o -9 3 5 86.64 101.15 3.89 o -8 3 5 55.54 55.77 3.59 o -7 3 5 80.79 84.20 2.76 o -6 3 5 79.04 79.96 2.29 o -5 3 5 0.00 0.35 1.58 o -4 3 5 82.96 86.68 3.01 o -3 3 5 66.72 75.87 2.67 o -2 3 5 8.49 8.97 3.03 o -1 3 5 21.81 20.92 2.73 o 0 3 5 932.46 946.13 15.46 o 1 3 5 16.02 10.86 4.02 o 5 3 5 83.92 81.29 3.62 o 6 3 5 223.36 233.06 12.12 o -11 4 5 11.91 14.11 10.84 o -10 4 5 279.17 313.10 9.33 o -9 4 5 5.24 10.88 3.38 o -8 4 5 89.30 83.38 3.82 o -7 4 5 67.42 83.03 6.29 o -6 4 5 57.92 59.14 2.88 o -5 4 5 1.56 1.54 2.02 o -4 4 5 81.24 78.07 2.00 o -3 4 5 12.82 11.05 3.09 o -2 4 5 10.07 15.68 16.49 o -1 4 5 18.66 13.58 4.70 o 0 4 5 26.55 21.61 4.75 o 1 4 5 3.61 5.76 4.68 o 2 4 5 34.21 31.93 2.70 o 3 4 5 0.09 -2.39 3.10 o 4 4 5 43.68 43.90 4.59 o 5 4 5 28.69 30.64 4.33 o 6 4 5 0.58 7.13 5.23 o 7 4 5 20.73 24.39 5.21 o -9 5 5 160.06 168.61 16.57 o -8 5 5 21.64 25.50 7.96 o -7 5 5 129.56 147.30 9.41 o -6 5 5 24.18 18.33 2.28 o -5 5 5 98.11 87.13 3.78 o -4 5 5 6.57 14.47 7.21 o -3 5 5 1.74 1.95 4.14 o -2 5 5 3.83 0.54 10.19 o -1 5 5 352.87 327.81 22.89 o 0 5 5 44.37 25.31 9.90 o 1 5 5 483.78 485.36 24.62 o 2 5 5 329.39 296.38 30.95 o 3 5 5 21.77 35.72 15.30 o 4 5 5 0.78 -4.51 6.54 o 5 5 5 250.11 246.46 6.15 o 6 5 5 2.77 -6.02 26.05 o -8 6 5 2.66 -18.22 18.22 o -7 6 5 0.05 -0.07 41.26 o -6 6 5 1.38 1.36 20.03 o -5 6 5 0.43 -1.23 14.53 o -4 6 5 41.73 35.65 12.19 o -3 6 5 1.09 27.51 18.69 o -2 6 5 0.25 -2.89 11.47 o -1 6 5 7.55 0.26 11.31 o 0 6 5 105.93 87.13 19.45 o 1 6 5 54.26 43.51 11.65 o 2 6 5 0.31 45.60 33.69 o 3 6 5 44.78 29.82 15.78 o 4 6 5 8.31 5.95 14.60 o 5 6 5 54.79 37.05 28.76 o -4 7 5 10.82 11.09 17.65 o -3 7 5 15.11 16.93 16.81 o -2 7 5 7.34 -6.43 17.99 o -1 7 5 0.02 -18.55 25.30 o 1 7 5 1.26 1.42 15.49 o 2 7 5 177.52 168.80 37.05 o 3 7 5 25.50 50.60 35.54 o 4 7 5 7.34 29.67 33.88 o -12 0 6 8.38 13.29 6.33 o -10 0 6 1218.80 1189.31 19.00 o -8 0 6 30.64 1.90 7.83 o -6 0 6 263.44 281.56 5.15 o -12 1 6 6.67 8.30 5.50 o -11 1 6 1.27 4.05 7.88 o -10 1 6 113.50 102.94 5.03 o -9 1 6 0.51 4.82 3.31 o -8 1 6 8.23 0.99 4.73 o -7 1 6 261.72 258.58 5.90 o -6 1 6 66.45 56.39 1.67 o -5 1 6 247.48 227.66 11.44 o -12 2 6 11.38 37.80 23.94 o -11 2 6 97.18 89.67 5.39 o -10 2 6 273.11 272.96 5.36 o -9 2 6 149.33 156.23 4.08 o -8 2 6 133.82 138.33 5.58 o -7 2 6 33.03 43.07 4.35 o -6 2 6 34.32 34.17 1.97 o -5 2 6 9.11 9.50 1.67 o -11 3 6 14.47 19.58 5.59 o -10 3 6 15.32 11.01 3.46 o -9 3 6 115.39 119.21 3.90 o -8 3 6 2.81 2.59 3.25 o -7 3 6 73.48 80.81 4.11 o -6 3 6 0.76 10.40 5.48 o -5 3 6 0.91 1.72 2.23 o -4 3 6 0.00 0.83 1.65 o -3 3 6 311.00 329.56 7.64 o -2 3 6 20.42 21.78 6.48 o -10 4 6 7.25 8.68 5.01 o -9 4 6 278.16 306.01 10.62 o -8 4 6 31.26 31.76 3.63 o -7 4 6 188.93 173.91 5.65 o -6 4 6 8.17 8.38 3.90 o -5 4 6 3.12 1.75 3.32 o -4 4 6 0.03 9.27 7.22 o -3 4 6 44.99 42.39 4.62 o -2 4 6 11.35 9.82 2.59 o -1 4 6 3.66 -0.64 8.36 o 0 4 6 38.76 33.65 6.37 o 1 4 6 63.69 60.23 5.01 o -9 5 6 125.97 134.83 9.49 o -8 5 6 39.46 32.93 9.04 o -7 5 6 1.29 -1.12 3.54 o -6 5 6 97.63 101.76 8.22 o -5 5 6 7.97 6.80 3.24 o -4 5 6 19.37 21.06 2.96 o -3 5 6 61.94 56.27 4.34 o -2 5 6 255.78 272.40 18.25 o -1 5 6 2.36 2.31 10.32 o 0 5 6 292.55 229.62 53.46 o 1 5 6 1.10 1.51 22.29 o 2 5 6 524.93 596.73 52.10 o 3 5 6 661.27 812.21 53.16 o 4 5 6 143.34 152.97 16.82 o -8 6 6 0.04 -15.67 15.67 o -7 6 6 0.01 31.42 25.45 o -6 6 6 0.77 10.70 16.20 o -5 6 6 48.68 37.21 12.14 o -4 6 6 12.58 25.64 12.62 o -3 6 6 11.46 -11.60 11.60 o -2 6 6 0.56 14.75 18.02 o -1 6 6 48.60 32.11 12.39 o 0 6 6 0.16 -17.09 21.67 o 1 6 6 69.46 92.95 38.62 o 2 6 6 6.64 3.76 19.94 o 3 6 6 24.45 23.66 15.22 o -4 7 6 14.38 32.23 53.76 o -3 7 6 0.64 -13.06 30.95 o -2 7 6 3.59 -7.66 14.69 o -1 7 6 3.49 -17.88 17.88 o 0 7 6 1.32 19.91 16.46 o 1 7 6 23.94 33.28 21.43 o 2 7 6 185.85 131.08 28.81 o -11 0 7 16.04 12.52 9.61 o -9 0 7 3.44 0.37 4.77 o -12 1 7 4.60 2.43 13.92 o -11 1 7 4.68 1.38 3.55 o -10 1 7 0.46 -4.00 4.00 o -9 1 7 96.48 94.83 6.14 o -8 1 7 101.96 105.01 4.28 o -7 1 7 90.77 93.50 7.53 o -11 2 7 15.32 15.68 4.34 o -10 2 7 55.92 61.21 3.49 o -9 2 7 115.26 115.80 4.70 o -8 2 7 8.34 8.24 3.74 o -7 2 7 190.06 191.19 6.77 o -6 2 7 21.32 23.15 2.36 o -11 3 7 0.12 -0.87 5.48 o -10 3 7 5.24 1.49 3.89 o -9 3 7 20.23 18.94 3.51 o -8 3 7 119.24 113.49 6.00 o -7 3 7 35.55 43.52 8.13 o -6 3 7 2.98 3.92 3.24 o -5 3 7 4.86 6.12 3.44 o -10 4 7 34.35 39.16 8.02 o -9 4 7 8.60 29.32 26.85 o -8 4 7 144.82 145.53 6.35 o -7 4 7 23.50 24.38 4.82 o -6 4 7 46.21 53.94 6.12 o -5 4 7 7.10 9.12 6.17 o -4 4 7 10.70 10.75 2.45 o -3 4 7 32.55 33.32 9.97 o -9 5 7 7.05 3.32 4.74 o -8 5 7 53.27 50.57 5.46 o -7 5 7 30.36 31.54 6.21 o -6 5 7 0.04 -0.38 3.13 o -5 5 7 0.16 -0.11 2.39 o -4 5 7 36.25 82.81 23.94 o -3 5 7 8.27 23.88 18.30 o -2 5 7 15.28 -12.30 12.30 o -1 5 7 66.13 52.10 22.59 o -8 6 7 10.36 19.28 39.15 o -7 6 7 0.94 40.10 18.08 o -6 6 7 24.72 4.69 16.87 o -5 6 7 0.12 -5.21 22.78 o -4 6 7 3.76 9.81 11.34 o -3 6 7 0.88 -1.45 20.75 o -2 6 7 25.82 33.75 13.67 o -1 6 7 6.51 61.72 29.21 o 0 6 7 38.32 61.19 46.15 o -3 7 7 6.15 62.26 27.71 o -2 7 7 7.65 -10.92 14.70 o -1 7 7 0.56 -1.73 19.97 o -10 2 8 11.32 15.70 6.20 o -10 3 8 0.84 1.80 3.86 o -9 3 8 0.51 0.17 5.49 o -8 3 8 124.72 126.05 8.31 o -8 4 8 45.15 61.47 5.82 o -7 4 8 89.63 96.22 13.19 o -8 5 8 14.36 8.53 18.95 o -7 5 8 55.61 39.60 15.69 o -6 5 8 1.01 -24.55 28.01 o