#------------------------------------------------------------------------------ #$Date: 2022-04-12 05:18:35 +0300 (Tue, 12 Apr 2022) $ #$Revision: 274469 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/02/25/2022594.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2022594 _cell_angle_alpha 90.000 _cell_angle_beta 97.104 _cell_angle_gamma 90.000 _cell_length_a 5.1300 _cell_length_b 8.6729 _cell_length_c 6.8473 _exptl_crystal_F_000 346.00 _reflns_d_resolution_high 0.7109 _cod_data_source_file ov3158Isup2.hkl _cod_data_source_block I _shelx_title ' shelxt_a.res in P2(1)/n' _shelx_refln_list_code 4 _shelx_f_calc_maximum 150.26 _shelx_f_squared_multiplier 1.000 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 13024.25 12956.86 136.56 o 4 0 0 9225.18 9271.56 68.28 o 6 0 0 861.50 840.35 57.28 o 1 1 0 4135.20 4111.05 50.82 o 2 1 0 3461.02 3650.38 31.42 o 3 1 0 6622.91 6633.76 41.82 o 4 1 0 1175.98 1200.14 20.64 o 5 1 0 921.16 959.94 21.82 o 6 1 0 1144.75 1163.53 46.94 o 7 1 0 1471.17 1467.01 82.04 o 0 2 0 2954.21 2890.60 163.30 o 1 2 0 1027.79 1057.76 17.64 o 2 2 0 3279.51 2970.29 27.25 o 3 2 0 471.44 461.26 11.33 o 4 2 0 2265.36 2297.61 29.21 o 5 2 0 209.68 218.56 12.66 o 6 2 0 1645.15 1679.44 53.80 o 1 3 0 22578.44 23602.53 99.68 o 2 3 0 235.82 242.73 9.03 o 3 3 0 5732.90 5457.58 45.52 o 4 3 0 14.06 18.79 3.88 o 5 3 0 3628.02 3479.91 52.42 o 6 3 0 16.04 13.78 5.29 o 0 4 0 375.73 633.19 21.87 o 1 4 0 395.14 391.45 11.22 o 2 4 0 5582.06 5469.53 60.55 o 3 4 0 602.04 606.40 17.87 o 4 4 0 865.16 831.72 22.45 o 5 4 0 840.44 838.67 28.60 o 6 4 0 1231.51 1277.45 44.83 o 1 5 0 2531.62 2492.13 29.78 o 2 5 0 1142.06 1139.85 20.71 o 3 5 0 901.23 880.22 20.33 o 4 5 0 479.13 463.08 22.62 o 5 5 0 2316.15 2301.42 50.03 o 6 5 0 569.98 534.54 30.23 o 0 6 0 13374.72 13515.97 128.27 o 1 6 0 0.19 4.51 2.49 o 2 6 0 8515.29 8551.92 73.99 o 3 6 0 70.27 83.01 8.39 o 4 6 0 3232.00 3290.43 63.99 o 5 6 0 198.68 223.20 17.93 o 6 6 0 577.53 563.81 41.20 o 1 7 0 2486.63 2348.85 35.48 o 2 7 0 167.40 164.03 9.93 o 3 7 0 2585.73 2511.90 56.07 o 4 7 0 559.60 535.58 27.43 o 5 7 0 486.41 520.82 29.84 o 0 8 0 3472.26 3320.03 62.58 o 1 8 0 51.23 51.42 6.35 o 2 8 0 570.54 611.21 26.51 o 3 8 0 5.05 0.81 3.06 o 4 8 0 1575.68 1654.05 46.67 o 5 8 0 75.08 43.71 14.28 o 1 9 0 3579.94 3659.30 55.73 o 2 9 0 6.10 2.87 3.70 o 3 9 0 2783.39 2792.77 60.89 o 4 9 0 8.90 5.56 5.23 o 0 10 0 1092.66 1149.72 51.24 o 1 10 0 75.78 78.58 9.76 o 2 10 0 951.41 986.40 35.93 o 3 10 0 188.97 176.27 17.93 o 1 11 0 271.62 273.85 21.14 o 2 11 0 0.34 -3.00 5.81 o 3 11 0 306.65 265.85 46.12 o 0 12 0 669.03 763.84 83.27 o 1 12 0 3.06 -15.60 14.88 o -5 0 1 169.81 149.70 11.72 o -3 0 1 847.41 889.94 17.43 o -1 0 1 266.19 284.82 4.76 o 1 0 1 26.94 21.93 2.00 o 3 0 1 751.53 746.70 24.52 o 5 0 1 75.92 80.28 11.83 o -7 1 1 238.17 229.79 44.58 o -6 1 1 27.01 13.64 7.32 o -5 1 1 0.03 1.95 2.09 o -4 1 1 23.18 25.58 2.92 o -3 1 1 15.16 19.58 2.07 o -2 1 1 165.92 192.26 4.23 o -1 1 1 1529.87 1560.80 13.75 o 1 1 1 1607.27 1679.24 21.87 o 2 1 1 44.71 53.38 3.17 o 3 1 1 0.49 1.26 1.66 o 4 1 1 73.24 69.67 7.79 o 5 1 1 34.90 25.60 4.62 o 6 1 1 6.08 23.00 7.17 o 7 1 1 149.94 184.04 41.47 o -7 2 1 17.77 32.96 18.49 o -6 2 1 24.10 25.77 6.87 o -5 2 1 246.78 252.19 12.72 o -4 2 1 9.56 12.45 2.21 o -3 2 1 79.21 83.11 4.49 o -2 2 1 1868.59 2006.79 15.40 o -1 2 1 183.69 174.26 3.96 o 0 2 1 457.41 504.24 8.74 o 1 2 1 29.32 41.55 2.61 o 2 2 1 2357.67 2529.21 19.60 o 3 2 1 325.93 359.98 11.42 o 4 2 1 27.42 21.00 3.74 o 5 2 1 151.45 161.17 12.91 o 6 2 1 27.83 29.86 6.56 o -6 3 1 2.85 1.38 5.41 o -5 3 1 48.23 53.25 6.48 o -4 3 1 36.06 38.13 3.84 o -3 3 1 384.78 386.40 7.69 o -2 3 1 61.49 65.01 3.47 o -1 3 1 84.94 119.02 5.66 o 0 3 1 322.86 381.65 9.04 o 1 3 1 341.57 329.22 8.78 o 2 3 1 111.78 100.85 3.72 o 3 3 1 188.01 195.53 6.63 o 4 3 1 15.91 14.11 5.07 o 5 3 1 18.06 12.71 4.12 o 6 3 1 44.72 51.63 9.72 o -6 4 1 166.88 174.78 16.23 o -5 4 1 31.37 32.16 6.16 o -4 4 1 21.37 12.89 3.58 o -3 4 1 6.41 6.40 1.96 o -2 4 1 4.55 2.13 2.04 o -1 4 1 83.96 82.34 5.91 o 0 4 1 167.64 150.43 8.67 o 1 4 1 12.83 19.32 2.64 o 2 4 1 470.12 461.05 9.10 o 3 4 1 109.31 113.84 6.90 o 4 4 1 0.06 1.48 2.98 o 5 4 1 29.04 34.04 6.45 o 6 4 1 0.60 -10.49 6.99 o -6 5 1 365.41 347.72 26.68 o -5 5 1 6.40 6.49 3.83 o -4 5 1 558.64 583.38 21.90 o -3 5 1 1.86 3.57 2.48 o -2 5 1 292.48 287.14 10.45 o -1 5 1 19.38 25.99 3.81 o 0 5 1 115.35 113.13 8.38 o 1 5 1 209.39 229.97 11.00 o 2 5 1 295.17 311.08 10.14 o 3 5 1 55.20 55.81 6.53 o 4 5 1 650.06 655.26 27.76 o 5 5 1 0.16 2.29 3.51 o 6 5 1 233.81 234.51 23.15 o -6 6 1 32.94 35.07 10.85 o -5 6 1 362.98 342.97 22.86 o -4 6 1 4.31 4.56 3.17 o -3 6 1 30.04 27.53 4.73 o -2 6 1 1633.61 1621.26 28.19 o -1 6 1 223.60 251.55 14.14 o 0 6 1 514.32 508.24 19.27 o 1 6 1 0.27 4.52 2.27 o 2 6 1 2486.59 2328.45 43.12 o 3 6 1 247.50 245.71 19.00 o 4 6 1 14.16 18.10 5.94 o 5 6 1 59.32 52.89 9.60 o -5 7 1 118.63 130.12 14.61 o -4 7 1 343.24 344.47 19.79 o -3 7 1 298.74 273.00 16.36 o -2 7 1 734.64 678.80 21.42 o -1 7 1 6.59 8.36 2.82 o 0 7 1 2.44 1.90 2.66 o 1 7 1 941.61 966.88 28.29 o 2 7 1 2.23 2.86 2.78 o 3 7 1 208.68 194.38 18.16 o 4 7 1 330.37 299.46 21.00 o 5 7 1 0.62 6.09 4.53 o -5 8 1 365.38 348.31 27.79 o -4 8 1 33.77 26.11 6.27 o -3 8 1 160.50 164.93 15.72 o -2 8 1 132.01 136.26 10.68 o -1 8 1 219.17 234.89 13.15 o 0 8 1 192.96 174.25 11.09 o 1 8 1 32.28 34.22 5.86 o 2 8 1 5.30 2.81 3.34 o 3 8 1 111.13 120.73 13.41 o 4 8 1 161.62 145.62 15.33 o 5 8 1 360.93 377.75 39.77 o -4 9 1 84.07 65.08 11.32 o -3 9 1 89.87 83.78 10.49 o -2 9 1 13.35 9.05 4.16 o -1 9 1 421.95 428.85 23.44 o 0 9 1 98.05 107.51 9.27 o 1 9 1 252.40 257.90 16.00 o 2 9 1 49.64 43.78 8.41 o 3 9 1 268.12 266.67 20.86 o 4 9 1 42.20 66.01 11.33 o -4 10 1 0.04 -20.59 15.97 o -3 10 1 343.69 411.15 27.03 o -2 10 1 411.95 388.80 22.44 o -1 10 1 22.16 14.74 4.70 o 0 10 1 275.45 282.50 18.14 o 1 10 1 0.11 -0.80 3.68 o 2 10 1 917.70 993.91 40.64 o 3 10 1 0.17 -7.91 5.27 o -3 11 1 47.78 95.07 30.28 o -2 11 1 510.98 508.33 26.90 o -1 11 1 201.77 218.94 22.00 o 0 11 1 0.10 5.94 5.57 o 1 11 1 2.49 0.45 7.28 o 2 11 1 99.94 83.35 12.40 o -1 12 1 39.95 20.90 21.86 o 0 12 1 778.92 811.18 84.78 o -6 0 2 3252.35 3519.35 92.26 o -4 0 2 3704.15 3685.96 32.68 o -2 0 2 377.27 279.42 10.09 o 0 0 2 156.09 133.93 5.20 o 2 0 2 61.69 52.63 6.88 o 4 0 2 100.02 107.09 10.75 o 6 0 2 1487.55 1562.18 61.03 o -6 1 2 171.14 172.18 12.77 o -5 1 2 1447.71 1444.70 27.57 o -4 1 2 4038.39 4097.14 34.69 o -3 1 2 5232.56 4960.09 40.44 o -2 1 2 1489.35 1397.97 12.99 o -1 1 2 15080.92 15717.34 84.98 o 0 1 2 1492.73 1578.90 14.91 o 1 1 2 8324.03 7827.37 49.68 o 2 1 2 78.46 83.25 5.33 o 3 1 2 9532.93 9268.06 61.13 o 4 1 2 1306.26 1276.93 33.68 o 5 1 2 2312.49 2206.14 51.00 o 6 1 2 546.06 552.54 25.70 o -7 2 2 33.07 18.38 14.61 o -6 2 2 559.78 532.75 29.76 o -5 2 2 336.62 336.61 14.79 o -4 2 2 3036.96 3018.67 32.90 o -3 2 2 2886.76 2818.58 23.15 o -2 2 2 9597.96 9509.44 43.80 o -1 2 2 118.74 179.75 5.11 o 0 2 2 15441.15 15817.09 123.30 o 1 2 2 2517.13 2717.34 21.86 o 2 2 2 13202.75 13486.06 96.81 o 3 2 2 519.39 531.75 18.27 o 4 2 2 4120.81 4090.57 57.32 o 5 2 2 161.91 157.61 13.09 o 6 2 2 1424.58 1473.73 42.63 o -6 3 2 83.02 82.81 11.20 o -5 3 2 3012.95 3107.36 46.76 o -4 3 2 214.22 204.58 9.06 o -3 3 2 2665.02 2579.66 28.19 o -2 3 2 35.71 39.55 2.96 o -1 3 2 2300.69 2230.63 21.71 o 0 3 2 0.11 2.57 1.56 o 1 3 2 2270.34 2227.37 20.42 o 2 3 2 28.12 40.03 3.60 o 3 3 2 284.44 264.40 11.87 o 4 3 2 17.61 12.72 4.17 o 5 3 2 977.37 1065.92 37.50 o 6 3 2 1.57 -0.64 5.36 o -6 4 2 594.84 614.04 35.41 o -5 4 2 601.83 608.35 26.81 o -4 4 2 2319.00 2303.24 38.66 o -3 4 2 886.92 879.00 22.13 o -2 4 2 10089.03 9910.49 56.23 o -1 4 2 745.28 742.75 16.29 o 0 4 2 12821.15 13007.79 144.56 o 1 4 2 177.37 197.00 8.93 o 2 4 2 9165.00 8828.60 86.30 o 3 4 2 391.15 387.14 15.93 o 4 4 2 5170.84 5078.88 90.29 o 5 4 2 262.55 269.12 19.43 o 6 4 2 691.64 674.50 39.19 o -6 5 2 136.60 118.37 15.40 o -5 5 2 864.97 848.73 32.54 o -4 5 2 2219.15 2224.52 49.57 o -3 5 2 4462.46 4351.33 56.94 o -2 5 2 634.64 611.52 18.29 o -1 5 2 5705.22 5391.61 61.73 o 0 5 2 779.69 778.95 22.94 o 1 5 2 12985.40 13029.66 179.89 o 2 5 2 68.94 65.96 7.24 o 3 5 2 4042.05 3849.34 70.95 o 4 5 2 700.73 664.02 29.51 o 5 5 2 1906.09 1878.44 53.18 o -6 6 2 1847.74 1807.34 60.97 o -5 6 2 185.28 174.50 17.95 o -4 6 2 1523.70 1540.74 43.45 o -3 6 2 1.55 0.08 3.26 o -2 6 2 1151.82 1150.40 28.75 o -1 6 2 686.79 657.17 21.39 o 0 6 2 788.11 714.33 32.39 o 1 6 2 385.63 383.45 16.79 o 2 6 2 57.64 61.49 5.78 o 3 6 2 10.08 15.35 5.95 o 4 6 2 830.60 846.81 38.94 o 5 6 2 200.81 191.48 19.93 o -5 7 2 981.92 1050.12 57.43 o -4 7 2 161.24 145.52 14.16 o -3 7 2 2217.64 2200.51 40.80 o -2 7 2 476.50 437.38 25.09 o -1 7 2 2750.40 2748.64 51.70 o 0 7 2 228.39 223.60 14.37 o 1 7 2 2726.40 2694.10 52.59 o 2 7 2 70.29 70.11 7.85 o 3 7 2 2692.22 2711.94 69.56 o 4 7 2 136.20 141.98 17.06 o 5 7 2 978.97 983.75 41.96 o -5 8 2 172.38 152.26 20.71 o -4 8 2 1077.12 1150.26 47.55 o -3 8 2 89.51 122.21 15.16 o -2 8 2 2059.44 2069.11 44.40 o -1 8 2 125.56 135.61 12.43 o 0 8 2 3147.26 3083.86 57.36 o 1 8 2 85.36 81.17 9.62 o 2 8 2 3459.95 3507.10 84.03 o 3 8 2 82.82 76.04 19.87 o 4 8 2 1087.69 1167.17 50.70 o 5 8 2 4.44 2.52 9.97 o -4 9 2 7.94 9.77 5.49 o -3 9 2 534.03 587.79 30.27 o -2 9 2 99.06 72.32 9.97 o -1 9 2 1389.15 1450.36 58.08 o 0 9 2 10.18 9.94 4.06 o 1 9 2 132.65 131.32 13.64 o 2 9 2 0.12 -0.42 4.96 o 3 9 2 645.23 576.69 35.62 o 4 9 2 0.67 26.58 20.66 o -3 10 2 99.22 107.66 14.00 o -2 10 2 1368.39 1386.09 38.31 o -1 10 2 324.36 333.21 20.07 o 0 10 2 1370.96 1417.82 47.02 o 1 10 2 30.67 23.20 6.24 o 2 10 2 2058.59 2134.34 72.16 o 3 10 2 37.43 35.70 11.11 o -2 11 2 19.48 10.67 11.89 o -1 11 2 2160.23 2209.46 66.14 o 0 11 2 36.45 29.68 12.54 o 1 11 2 2399.29 2625.43 89.88 o 2 11 2 7.64 1.05 9.63 o -5 0 3 111.47 121.58 12.39 o -3 0 3 1645.05 1637.03 27.13 o -1 0 3 970.66 1093.56 23.94 o 1 0 3 794.62 859.05 25.84 o 3 0 3 958.41 965.42 33.45 o 5 0 3 405.50 392.91 49.10 o -7 1 3 80.71 83.70 25.96 o -6 1 3 198.41 219.30 17.73 o -5 1 3 157.65 159.70 9.69 o -4 1 3 109.27 104.65 5.96 o -3 1 3 4.46 10.81 2.25 o -2 1 3 638.29 635.54 9.70 o -1 1 3 1267.45 1392.97 17.23 o 0 1 3 0.18 6.14 1.50 o 1 1 3 8.38 11.97 2.20 o 2 1 3 156.94 175.95 7.83 o 3 1 3 1204.02 1201.86 28.42 o 4 1 3 19.86 20.38 6.06 o 5 1 3 37.61 45.56 8.14 o 6 1 3 16.88 7.15 7.29 o -6 2 3 4.99 5.29 5.29 o -5 2 3 49.55 60.86 7.53 o -4 2 3 222.78 209.13 9.77 o -3 2 3 340.31 343.90 8.64 o -2 2 3 151.37 167.19 6.72 o -1 2 3 206.90 217.07 6.37 o 0 2 3 1541.22 1645.50 19.46 o 1 2 3 29.41 36.70 3.15 o 2 2 3 50.51 52.12 4.42 o 3 2 3 18.96 20.18 3.82 o 4 2 3 59.87 55.81 7.10 o 5 2 3 94.70 123.83 13.99 o 6 2 3 151.03 145.67 15.83 o -6 3 3 84.33 79.85 10.62 o -5 3 3 12.03 5.90 4.52 o -4 3 3 217.56 210.99 11.39 o -3 3 3 8.99 10.46 2.92 o -2 3 3 151.16 163.21 5.85 o -1 3 3 51.72 56.12 3.65 o 0 3 3 18.05 17.68 2.48 o 1 3 3 865.63 873.53 14.43 o 2 3 3 48.32 45.81 5.82 o 3 3 3 30.39 21.68 4.46 o 4 3 3 204.56 191.19 13.43 o 5 3 3 204.84 201.12 19.84 o 6 3 3 17.67 9.23 8.56 o -6 4 3 51.48 49.85 17.90 o -5 4 3 8.99 12.41 4.18 o -4 4 3 82.04 79.08 8.48 o -3 4 3 150.70 139.43 7.83 o -2 4 3 61.13 68.15 4.56 o -1 4 3 1103.90 1093.95 21.72 o 0 4 3 110.38 106.37 6.95 o 1 4 3 293.74 286.45 9.31 o 2 4 3 264.17 276.71 14.06 o 3 4 3 188.76 179.65 12.42 o 4 4 3 87.39 95.26 11.85 o 5 4 3 1.90 -0.21 4.68 o 6 4 3 2.40 -3.80 6.09 o -6 5 3 309.15 279.93 56.65 o -5 5 3 50.78 54.44 8.74 o -4 5 3 92.84 107.10 10.34 o -3 5 3 0.48 5.20 2.85 o -2 5 3 1784.30 1763.12 26.58 o -1 5 3 296.31 296.42 13.60 o 0 5 3 151.13 156.91 11.15 o 1 5 3 78.83 73.71 6.39 o 2 5 3 4.49 6.76 3.56 o 3 5 3 311.64 310.02 16.27 o 4 5 3 77.94 66.99 10.40 o 5 5 3 66.93 85.95 14.96 o -6 6 3 196.36 151.15 37.50 o -5 6 3 22.62 24.53 7.61 o -4 6 3 0.40 -0.89 3.83 o -3 6 3 283.51 281.10 15.85 o -2 6 3 6.70 6.35 3.05 o -1 6 3 45.52 53.83 7.43 o 0 6 3 1573.10 1501.62 37.47 o 1 6 3 6.24 2.99 3.36 o 2 6 3 957.76 958.49 31.06 o 3 6 3 81.82 78.87 12.24 o 4 6 3 142.56 140.28 16.79 o 5 6 3 192.54 190.84 20.50 o -5 7 3 62.28 67.91 14.83 o -4 7 3 130.34 141.33 16.19 o -3 7 3 0.24 3.84 4.18 o -2 7 3 650.10 631.79 22.91 o -1 7 3 68.41 82.32 9.48 o 0 7 3 178.50 162.46 12.98 o 1 7 3 754.13 737.69 26.97 o 2 7 3 52.03 37.78 7.43 o 3 7 3 65.65 68.71 11.47 o 4 7 3 48.87 42.73 10.76 o 5 7 3 127.92 140.40 25.59 o -5 8 3 133.17 79.56 26.22 o -4 8 3 32.00 75.81 18.79 o -3 8 3 199.66 205.12 17.14 o -2 8 3 6.49 3.04 3.28 o -1 8 3 996.88 995.99 31.46 o 0 8 3 100.63 100.86 10.73 o 1 8 3 1.37 1.77 4.19 o 2 8 3 41.34 36.54 9.05 o 3 8 3 19.12 19.02 6.86 o 4 8 3 18.39 24.41 8.50 o -4 9 3 1.08 4.70 13.33 o -3 9 3 1.50 1.43 4.13 o -2 9 3 272.76 255.12 21.74 o -1 9 3 8.85 20.50 6.06 o 0 9 3 6.95 8.56 4.11 o 1 9 3 547.99 556.07 31.35 o 2 9 3 1.88 2.27 5.66 o 3 9 3 112.32 130.23 17.79 o -3 10 3 58.89 60.84 13.60 o -2 10 3 54.77 73.19 12.48 o -1 10 3 115.18 117.72 14.27 o 0 10 3 476.20 487.40 27.41 o 1 10 3 43.90 36.59 9.20 o 2 10 3 469.54 453.64 32.84 o -2 11 3 684.22 665.86 74.62 o -1 11 3 29.29 27.95 9.64 o 0 11 3 232.25 205.06 23.94 o 1 11 3 1.05 11.48 12.68 o -6 0 4 80.86 108.21 20.25 o -4 0 4 779.37 717.74 29.25 o -2 0 4 7245.31 7156.14 63.60 o 0 0 4 15679.80 15862.11 104.64 o 2 0 4 14231.51 14122.95 118.37 o 4 0 4 7769.26 7400.06 153.87 o 6 0 4 1396.96 1350.73 105.50 o -6 1 4 162.07 141.87 15.06 o -5 1 4 1950.15 1997.26 46.41 o -4 1 4 1738.98 1670.75 31.58 o -3 1 4 4803.29 4707.50 46.08 o -2 1 4 2211.04 2206.47 29.48 o -1 1 4 3652.42 3495.96 37.03 o 0 1 4 2299.69 2322.32 23.50 o 1 1 4 4623.20 4623.91 53.21 o 2 1 4 30.38 35.49 4.17 o 3 1 4 845.90 818.20 24.91 o 4 1 4 171.70 171.55 18.55 o 5 1 4 1058.53 1091.02 45.51 o 6 1 4 418.10 394.23 40.57 o -6 2 4 1733.64 1840.69 54.18 o -5 2 4 265.97 255.95 16.61 o -4 2 4 3382.33 3370.50 52.56 o -3 2 4 647.14 652.11 19.07 o -2 2 4 3514.42 3289.13 39.16 o -1 2 4 1013.17 970.75 17.13 o 0 2 4 2266.36 2126.05 31.06 o 1 2 4 1082.65 1112.66 18.85 o 2 2 4 1624.55 1536.25 28.03 o 3 2 4 3.18 8.86 2.90 o 4 2 4 618.72 609.93 25.14 o 5 2 4 22.18 18.45 6.54 o 6 2 4 599.91 597.68 50.53 o -6 3 4 0.05 1.39 6.79 o -5 3 4 548.01 568.42 30.83 o -4 3 4 145.92 139.20 9.66 o -3 3 4 1163.61 1157.03 28.73 o -2 3 4 94.65 101.06 6.39 o -1 3 4 8152.78 7941.83 77.20 o 0 3 4 272.47 260.35 9.01 o 1 3 4 6527.15 6274.12 54.50 o 2 3 4 44.22 51.72 6.25 o 3 3 4 8112.32 7925.43 84.77 o 4 3 4 0.01 -2.38 4.30 o 5 3 4 2671.84 2644.51 74.84 o -6 4 4 1284.47 1243.71 50.27 o -5 4 4 157.92 142.66 16.21 o -4 4 4 2447.13 2450.51 53.60 o -3 4 4 1254.54 1282.05 26.98 o -2 4 4 2070.77 2046.24 24.85 o -1 4 4 1374.77 1384.99 16.45 o 0 4 4 1663.25 1598.99 24.56 o 1 4 4 177.98 187.82 11.73 o 2 4 4 977.79 915.17 27.53 o 3 4 4 40.03 40.85 6.64 o 4 4 4 481.71 535.52 27.96 o 5 4 4 258.68 262.41 24.03 o -6 5 4 68.81 55.15 22.54 o -5 5 4 2147.66 2223.66 66.07 o -4 5 4 664.96 675.84 29.65 o -3 5 4 2372.47 2385.61 47.96 o -2 5 4 1215.79 1190.12 28.24 o -1 5 4 1849.67 1821.38 27.70 o 0 5 4 696.15 670.71 22.16 o 1 5 4 818.71 811.28 25.67 o 2 5 4 24.18 21.40 5.84 o 3 5 4 972.32 945.52 39.03 o 4 5 4 50.62 54.47 9.51 o 5 5 4 252.50 262.65 28.75 o -5 6 4 1.02 3.99 5.98 o -4 6 4 453.05 448.15 25.39 o -3 6 4 95.84 68.23 8.69 o -2 6 4 2927.58 2841.97 51.09 o -1 6 4 62.21 58.65 7.77 o 0 6 4 6659.93 6553.67 82.32 o 1 6 4 41.00 39.39 6.19 o 2 6 4 4826.29 4903.00 76.58 o 3 6 4 5.14 18.09 7.08 o 4 6 4 3853.02 3886.74 94.91 o -5 7 4 650.09 621.80 52.61 o -4 7 4 88.78 94.32 14.02 o -3 7 4 2343.45 2430.64 69.11 o -2 7 4 1530.65 1460.49 48.55 o -1 7 4 1525.99 1521.79 41.19 o 0 7 4 42.04 53.61 8.38 o 1 7 4 2929.00 2921.12 55.90 o 2 7 4 153.72 151.33 18.06 o 3 7 4 991.07 960.99 44.82 o 4 7 4 55.74 57.08 14.34 o -4 8 4 1338.47 1427.80 55.97 o -3 8 4 134.91 138.70 14.28 o -2 8 4 1670.72 1607.03 53.69 o -1 8 4 154.36 145.67 13.49 o 0 8 4 1128.05 1139.83 37.86 o 1 8 4 1.15 1.95 6.43 o 2 8 4 762.92 780.20 40.28 o 3 8 4 135.37 136.17 18.71 o -4 9 4 6.10 0.33 10.93 o -3 9 4 716.09 782.77 41.63 o -2 9 4 1.92 -6.40 4.27 o -1 9 4 2123.33 2095.51 56.54 o 0 9 4 5.81 7.08 4.82 o 1 9 4 2496.00 2512.59 73.47 o 2 9 4 4.65 9.47 6.07 o -3 10 4 390.13 383.63 59.77 o -2 10 4 733.67 690.34 38.84 o -1 10 4 320.68 316.09 30.61 o 0 10 4 631.92 645.10 36.59 o 1 10 4 9.08 11.38 8.77 o 2 10 4 1129.03 1105.92 101.12 o -1 11 4 572.69 593.36 74.70 o 0 11 4 60.81 77.26 25.52 o -5 0 5 357.77 384.03 29.98 o -3 0 5 18.38 24.00 6.10 o -1 0 5 1501.40 1513.77 30.05 o 1 0 5 29.72 19.64 4.61 o 3 0 5 99.48 87.41 12.94 o 5 0 5 25.22 27.54 11.69 o -6 1 5 7.43 6.25 4.92 o -5 1 5 2.51 -0.74 2.58 o -4 1 5 17.47 10.86 5.16 o -3 1 5 130.60 118.13 10.26 o -2 1 5 184.61 186.55 8.99 o -1 1 5 188.15 218.83 12.99 o 0 1 5 159.48 157.95 6.79 o 1 1 5 495.72 502.85 13.86 o 2 1 5 358.68 390.50 14.36 o 3 1 5 177.96 174.79 17.84 o 4 1 5 52.76 80.83 15.77 o 5 1 5 74.64 73.41 13.03 o -6 2 5 0.56 2.95 6.36 o -5 2 5 40.23 41.66 8.13 o -4 2 5 7.21 3.84 3.54 o -3 2 5 158.90 159.62 10.07 o -2 2 5 308.74 283.82 14.69 o -1 2 5 222.86 219.11 11.67 o 0 2 5 28.46 29.28 4.41 o 1 2 5 7.51 9.67 2.72 o 2 2 5 19.85 20.97 4.27 o 3 2 5 1.41 1.36 2.77 o 4 2 5 0.73 2.33 4.24 o 5 2 5 98.49 96.14 12.94 o -6 3 5 0.60 3.39 7.22 o -5 3 5 177.40 157.66 15.53 o -4 3 5 6.04 -3.38 2.73 o -3 3 5 0.25 3.26 2.98 o -2 3 5 0.81 7.55 2.76 o -1 3 5 4.38 7.98 2.70 o 0 3 5 334.94 352.34 13.54 o 1 3 5 4.88 8.79 2.48 o 2 3 5 95.77 89.37 8.46 o 3 3 5 66.74 68.53 8.49 o 4 3 5 93.10 93.26 14.34 o 5 3 5 65.66 91.91 16.48 o -6 4 5 139.96 129.65 23.19 o -5 4 5 135.95 137.21 14.50 o -4 4 5 107.66 128.05 15.33 o -3 4 5 277.17 283.39 15.71 o -2 4 5 33.68 29.31 5.08 o -1 4 5 96.70 87.23 6.19 o 0 4 5 142.79 145.12 9.73 o 1 4 5 301.38 308.60 13.78 o 2 4 5 97.47 93.09 10.02 o 3 4 5 167.59 148.09 12.80 o 4 4 5 241.05 215.83 18.73 o -5 5 5 31.61 32.62 11.92 o -4 5 5 213.47 235.16 21.35 o -3 5 5 19.22 12.69 4.18 o -2 5 5 1049.73 1036.39 27.94 o -1 5 5 140.77 143.79 9.72 o 0 5 5 22.58 25.86 4.69 o 1 5 5 121.06 98.90 10.95 o 2 5 5 283.87 301.89 19.75 o 3 5 5 8.34 18.44 5.24 o 4 5 5 182.48 176.42 17.35 o -5 6 5 12.74 0.12 6.29 o -4 6 5 150.22 148.55 15.88 o -3 6 5 125.64 126.99 12.08 o -2 6 5 78.39 76.51 8.09 o -1 6 5 237.53 224.41 12.87 o 0 6 5 157.13 155.55 13.68 o 1 6 5 1.39 4.88 3.46 o 2 6 5 530.83 557.02 27.65 o 3 6 5 11.32 11.48 8.66 o 4 6 5 339.98 371.97 29.57 o -5 7 5 295.53 311.31 52.72 o -4 7 5 224.45 271.57 24.07 o -3 7 5 41.26 36.56 8.54 o -2 7 5 429.99 410.80 22.09 o -1 7 5 5.33 9.19 5.33 o 0 7 5 118.65 116.47 12.32 o 1 7 5 155.33 158.19 13.49 o 2 7 5 225.00 224.43 22.02 o 3 7 5 194.90 198.79 22.58 o 4 7 5 85.84 90.83 30.09 o -4 8 5 11.00 14.21 8.57 o -3 8 5 536.29 528.08 29.70 o -2 8 5 5.01 10.37 4.99 o -1 8 5 148.90 177.15 18.44 o 0 8 5 1.53 -2.96 3.88 o 1 8 5 272.48 308.40 22.44 o 2 8 5 92.26 88.53 14.52 o 3 8 5 37.82 42.73 14.98 o -3 9 5 9.40 4.43 10.10 o -2 9 5 244.95 240.06 22.98 o -1 9 5 6.43 8.11 5.07 o 0 9 5 3.10 0.87 5.73 o 1 9 5 94.17 74.17 13.33 o 2 9 5 106.96 135.88 35.50 o -2 10 5 0.48 -1.37 7.30 o -1 10 5 107.79 110.96 19.34 o 0 10 5 117.66 91.14 30.53 o 1 10 5 235.49 228.72 44.73 o -4 0 6 3575.35 3602.76 111.97 o -2 0 6 4131.80 4176.96 76.33 o 0 0 6 772.47 771.82 26.16 o 2 0 6 118.44 130.99 15.24 o 4 0 6 152.56 165.82 31.47 o -6 1 6 44.15 18.12 13.88 o -5 1 6 696.41 706.48 29.55 o -4 1 6 442.95 423.66 21.64 o -3 1 6 750.42 729.01 29.82 o -2 1 6 986.93 985.97 24.71 o -1 1 6 2174.99 2139.90 34.98 o 0 1 6 2617.19 2598.62 37.07 o 1 1 6 3410.01 3430.11 48.43 o 2 1 6 17.53 16.76 3.89 o 3 1 6 2298.43 2331.14 45.31 o 4 1 6 72.63 69.49 13.71 o 5 1 6 1599.21 1532.77 102.60 o -6 2 6 134.53 104.87 31.24 o -5 2 6 209.61 177.05 16.71 o -4 2 6 645.35 629.07 26.42 o -3 2 6 1.95 1.80 2.69 o -2 2 6 1692.80 1714.62 37.88 o -1 2 6 2229.12 2134.77 45.82 o 0 2 6 3338.48 3300.72 62.31 o 1 2 6 349.79 347.86 14.09 o 2 2 6 3850.84 3901.16 60.88 o 3 2 6 166.01 165.44 12.19 o 4 2 6 2377.66 2403.18 54.92 o -5 3 6 2184.72 2371.26 83.54 o -4 3 6 2.58 10.54 5.13 o -3 3 6 3806.07 3891.61 61.77 o -2 3 6 6.22 11.67 3.90 o -1 3 6 3268.17 3286.33 50.88 o 0 3 6 88.77 89.14 8.12 o 1 3 6 882.32 908.66 29.57 o 2 3 6 190.08 193.51 13.90 o 3 3 6 441.80 449.30 24.63 o 4 3 6 72.97 80.88 12.43 o -5 4 6 51.89 44.62 11.39 o -4 4 6 736.27 754.31 33.53 o -3 4 6 311.38 330.59 20.73 o -2 4 6 1337.17 1372.20 33.75 o -1 4 6 693.63 664.83 23.40 o 0 4 6 3534.20 3459.76 50.52 o 1 4 6 650.59 633.75 28.76 o 2 4 6 3184.22 3232.23 55.30 o 3 4 6 55.83 47.52 10.29 o 4 4 6 1506.69 1548.67 67.35 o -5 5 6 82.43 66.78 18.47 o -4 5 6 378.22 394.39 29.07 o -3 5 6 1209.52 1229.68 41.90 o -2 5 6 483.96 482.12 20.69 o -1 5 6 1690.97 1679.72 38.24 o 0 5 6 1420.83 1384.91 31.22 o 1 5 6 3085.24 3075.24 58.19 o 2 5 6 6.19 10.18 5.61 o 3 5 6 2712.70 2865.06 78.94 o 4 5 6 39.11 50.30 15.49 o -4 6 6 1731.47 1906.62 65.97 o -3 6 6 466.80 476.75 24.91 o -2 6 6 1937.57 1978.16 48.52 o -1 6 6 3.97 4.57 4.87 o 0 6 6 974.68 989.90 32.78 o 1 6 6 97.46 97.54 12.08 o 2 6 6 200.12 187.84 17.23 o 3 6 6 11.26 16.54 7.05 o -3 7 6 739.35 774.81 33.03 o -2 7 6 254.90 257.02 18.22 o -1 7 6 748.05 681.68 36.16 o 0 7 6 184.93 181.76 18.76 o 1 7 6 1139.28 1139.98 48.53 o 2 7 6 343.40 325.98 27.38 o -3 8 6 52.84 53.49 15.72 o -2 8 6 703.01 750.07 36.93 o -1 8 6 91.79 77.55 13.24 o 0 8 6 1043.45 1043.89 46.50 o 1 8 6 195.06 172.63 20.07 o 2 8 6 1385.28 1563.81 119.17 o -2 9 6 67.36 40.09 14.08 o -1 9 6 1157.10 1213.66 59.64 o 0 9 6 0.55 -9.93 8.94 o -5 0 7 68.02 62.49 17.27 o -3 0 7 131.44 184.02 25.63 o -1 0 7 368.34 391.79 30.15 o 1 0 7 5.35 8.51 4.80 o 3 0 7 0.18 7.51 8.28 o -5 1 7 150.61 124.57 22.77 o -4 1 7 11.09 14.94 8.05 o -3 1 7 34.97 32.43 8.30 o -2 1 7 4.58 6.32 4.54 o -1 1 7 45.84 41.76 6.32 o 0 1 7 3.82 3.26 3.96 o 1 1 7 85.42 89.86 10.63 o 2 1 7 0.27 6.60 4.43 o 3 1 7 313.46 280.35 20.58 o 4 1 7 45.33 61.80 16.02 o -5 2 7 0.42 5.63 25.26 o -4 2 7 154.99 139.96 14.64 o -3 2 7 63.73 75.99 10.70 o -2 2 7 14.88 18.29 6.24 o -1 2 7 100.78 98.94 10.94 o 0 2 7 80.74 81.31 9.93 o 1 2 7 205.49 206.63 16.67 o 2 2 7 17.72 7.92 4.43 o 3 2 7 7.99 3.91 3.66 o 4 2 7 3.55 -0.40 4.92 o -5 3 7 50.46 60.80 24.24 o -4 3 7 15.29 15.20 10.65 o -3 3 7 18.35 18.24 7.49 o -2 3 7 1.72 6.63 4.05 o -1 3 7 137.56 133.12 16.16 o 0 3 7 85.79 92.30 9.66 o 1 3 7 18.61 20.25 5.38 o 2 3 7 5.39 13.62 4.31 o 3 3 7 4.21 4.01 4.32 o -4 4 7 77.83 87.75 14.14 o -3 4 7 2.46 5.10 4.67 o -2 4 7 24.09 17.31 8.95 o -1 4 7 8.33 2.65 3.57 o 0 4 7 3.43 6.15 4.11 o 1 4 7 85.92 91.01 10.40 o 2 4 7 202.08 208.69 17.92 o 3 4 7 2.37 -4.49 5.99 o -4 5 7 97.28 101.31 22.31 o -3 5 7 3.77 3.18 5.70 o -2 5 7 181.51 177.04 14.90 o -1 5 7 22.04 21.93 5.20 o 0 5 7 397.57 435.54 23.10 o 1 5 7 36.36 18.60 6.28 o 2 5 7 253.17 252.73 23.00 o 3 5 7 120.06 126.95 29.20 o -3 6 7 99.50 75.77 13.58 o -2 6 7 153.12 161.85 16.61 o -1 6 7 29.30 22.39 5.40 o 0 6 7 74.47 80.89 11.49 o 1 6 7 179.20 184.75 17.05 o 2 6 7 130.46 128.47 15.20 o -3 7 7 11.69 12.10 11.54 o -2 7 7 282.79 302.38 23.29 o -1 7 7 94.27 90.39 13.65 o 0 7 7 82.38 63.92 11.99 o 1 7 7 117.89 109.03 18.11 o 2 7 7 41.23 45.48 16.70 o -2 8 7 0.62 1.41 8.45 o -1 8 7 130.76 118.17 31.87 o 0 8 7 51.52 12.43 7.65 o -4 0 8 120.59 152.33 26.08 o -2 0 8 1110.65 1071.41 63.55 o 0 0 8 744.88 763.57 41.05 o 2 0 8 2667.92 2817.52 108.84 o -4 1 8 88.08 81.54 13.43 o -3 1 8 1881.71 1898.61 62.04 o -2 1 8 697.60 708.91 32.66 o -1 1 8 1476.04 1517.82 40.78 o 0 1 8 442.58 450.72 22.29 o 1 1 8 2173.42 2338.85 67.46 o 2 1 8 616.91 636.04 36.58 o -4 2 8 1605.35 1725.65 128.76 o -3 2 8 112.02 100.32 14.49 o -2 2 8 1798.96 1822.06 59.03 o -1 2 8 203.05 189.24 14.74 o 0 2 8 1394.55 1429.62 45.80 o 1 2 8 286.13 284.44 20.79 o 2 2 8 615.85 604.07 57.37 o -4 3 8 8.53 16.49 15.43 o -3 3 8 76.54 83.85 13.23 o -2 3 8 24.95 29.74 7.91 o -1 3 8 652.74 653.78 30.50 o 0 3 8 31.57 32.75 8.41 o 1 3 8 591.51 587.59 34.21 o 2 3 8 3.63 2.00 5.52 o -3 4 8 149.52 164.25 19.65 o -2 4 8 510.85 559.11 33.48 o -1 4 8 324.51 325.45 21.99 o 0 4 8 1570.95 1601.19 51.97 o 1 4 8 557.04 556.76 30.89 o 2 4 8 495.01 480.21 46.35 o -3 5 8 1348.04 1463.76 111.70 o -2 5 8 296.77 269.67 21.41 o -1 5 8 1533.90 1506.48 57.44 o 0 5 8 159.69 131.83 15.41 o 1 5 8 352.07 354.91 25.55 o -2 6 8 302.73 322.21 50.07 o -1 6 8 39.72 32.83 12.04 o 0 6 8 740.12 743.83 40.53 o 1 6 8 52.95 53.40 27.68 o -1 0 9 175.94 132.61 28.56 o 1 0 9 43.73 55.82 23.01 o -3 1 9 68.17 78.28 27.46 o -2 1 9 8.45 5.51 8.42 o -1 1 9 4.52 -7.06 6.86 o 0 1 9 15.56 10.22 12.25 o 1 1 9 1.39 5.63 10.74 o -3 2 9 22.33 27.84 16.02 o -2 2 9 19.66 6.58 6.26 o -1 2 9 87.87 130.86 24.57 o 0 2 9 93.63 54.59 15.35 o 1 2 9 46.13 48.31 14.89 o -2 3 9 48.94 46.52 14.10 o -1 3 9 50.55 53.67 16.69 o 0 3 9 5.64 -2.63 4.40 o 0 4 9 0.20 -3.53 8.46 o