#------------------------------------------------------------------------------ #$Date: 2022-09-13 04:48:08 +0300 (Tue, 13 Sep 2022) $ #$Revision: 277787 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/02/26/2022662.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2022662 _cell_angle_alpha 102.194 _cell_angle_beta 91.589 _cell_angle_gamma 95.875 _cell_length_a 8.5037 _cell_length_b 12.2290 _cell_length_c 15.8336 _exptl_crystal_F_000 696.00 _reflns_d_resolution_high 0.6539 _cod_data_source_file zo30267sup3.hkl _cod_data_source_block 7 _shelx_title ' a_a.res in P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 236.92 _shelx_f_squared_multiplier 1.000 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 55.24 57.84 18.59 o 3 0 0 16.73 -4.20 15.02 o 4 0 0 918.81 1191.94 53.59 o 5 0 0 2415.53 2614.97 66.29 o 6 0 0 49.83 22.23 22.94 o 7 0 0 2802.49 2916.95 82.08 o 8 0 0 419.65 478.41 47.29 o 9 0 0 1029.38 1226.39 95.11 o 10 0 0 200.82 223.41 97.84 o 11 0 0 3.12 40.97 54.60 o 12 0 0 210.85 194.06 90.51 o -12 1 0 2.94 29.94 65.78 o -11 1 0 4.01 25.89 52.71 o -10 1 0 34.07 93.40 54.04 o -9 1 0 39.58 -8.15 66.86 o -8 1 0 716.81 761.14 58.54 o -7 1 0 34.29 5.70 27.35 o -6 1 0 10.40 3.07 20.95 o -5 1 0 46.01 34.24 30.17 o -4 1 0 66.95 62.73 19.05 o -3 1 0 385.11 568.44 55.45 o -2 1 0 227.52 277.17 16.69 o -1 1 0 67.54 61.82 8.37 o 0 1 0 0.08 -2.19 2.19 o 1 1 0 1.31 -6.41 9.20 o 2 1 0 50.38 51.87 22.42 o 3 1 0 1229.61 1228.88 37.63 o 4 1 0 23.20 82.94 38.00 o 5 1 0 1000.05 973.58 42.93 o 6 1 0 18.73 -20.77 23.17 o 7 1 0 505.19 589.17 46.98 o 8 1 0 1.79 -6.77 32.18 o 9 1 0 27.01 -29.66 45.45 o 10 1 0 107.54 69.05 58.35 o 11 1 0 4.02 73.23 59.55 o 12 1 0 44.70 12.23 73.38 o -12 2 0 25.10 120.29 90.10 o -11 2 0 16.21 -30.42 51.86 o -10 2 0 454.67 531.41 107.59 o -9 2 0 121.34 164.51 53.43 o -8 2 0 890.67 954.56 65.54 o -7 2 0 16.78 33.51 27.85 o -6 2 0 454.77 501.13 37.03 o -5 2 0 13.61 4.68 19.01 o -4 2 0 691.54 705.55 31.12 o -3 2 0 1642.00 2166.01 96.12 o -2 2 0 2408.23 2744.78 60.27 o -1 2 0 1124.34 1187.31 28.26 o 0 2 0 595.85 537.52 18.19 o 1 2 0 702.89 556.31 54.08 o 2 2 0 5482.89 5194.02 127.04 o 3 2 0 846.71 795.38 36.02 o 4 2 0 8278.07 8476.46 147.71 o 5 2 0 413.68 474.82 54.09 o 6 2 0 2014.92 1975.78 64.01 o 7 2 0 355.20 407.53 42.78 o 8 2 0 55.14 78.21 35.79 o 9 2 0 35.43 17.53 38.33 o 10 2 0 3.04 65.09 57.48 o 12 2 0 141.02 361.21 105.18 o -12 3 0 126.44 157.46 67.36 o -11 3 0 148.79 178.78 66.40 o -10 3 0 80.63 83.49 51.56 o -9 3 0 112.74 87.12 46.91 o -8 3 0 60.74 95.24 48.66 o -7 3 0 19.45 18.13 26.68 o -6 3 0 83.45 106.50 25.76 o -5 3 0 255.08 333.26 50.15 o -4 3 0 677.26 742.19 33.82 o -3 3 0 1293.15 1434.94 42.09 o -2 3 0 4.31 9.38 14.03 o -1 3 0 17.49 27.63 13.53 o 0 3 0 189.32 158.71 38.12 o 1 3 0 3169.70 2917.43 68.50 o 2 3 0 1351.59 1339.50 38.23 o 3 3 0 578.50 512.75 30.47 o 4 3 0 697.10 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