#------------------------------------------------------------------------------ #$Date: 2023-03-16 05:14:01 +0200 (Thu, 16 Mar 2023) $ #$Revision: 281909 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/02/27/2022705.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2022705 _cell_angle_alpha 90.000 _cell_angle_beta 97.125 _cell_angle_gamma 90.000 _cell_length_a 9.7839 _cell_length_b 10.2313 _cell_length_c 18.2717 _exptl_crystal_F_000 984.00 _reflns_d_resolution_high 0.7282 _cod_data_source_file dv30211sup2.hkl _cod_data_source_block 1 _shelx_title ' MS20182020_0m_a.res in P2(1)' _shelx_refln_list_code 4 _shelx_f_calc_maximum 643.93 _shelx_f_squared_multiplier 1.000 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y+1/2, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 -13 0 131.50 88.87 35.64 o 2 -13 0 163.51 142.83 30.42 o 3 -13 0 36.53 34.51 19.76 o 0 -12 0 4873.12 4883.70 176.31 o 1 -12 0 83.54 101.28 33.76 o 2 -12 0 94.62 65.65 21.22 o 3 -12 0 3265.25 3659.91 153.80 o 4 -12 0 42.18 27.41 17.09 o 5 -12 0 58.09 59.60 23.43 o 6 -12 0 990.55 1132.87 108.79 o 1 -11 0 13.01 20.80 33.76 o 2 -11 0 44.59 40.11 17.09 o 3 -11 0 476.76 461.69 44.86 o 4 -11 0 11.17 -0.68 14.41 o 5 -11 0 119.08 121.94 26.53 o 6 -11 0 654.47 576.25 65.65 o 7 -11 0 57.16 37.28 20.73 o 0 -10 0 15.29 18.76 15.00 o 1 -10 0 22.29 28.30 18.76 o 2 -10 0 69.58 90.56 18.57 o 3 -10 0 21.11 44.73 17.09 o 4 -10 0 13.42 -1.25 11.72 o 5 -10 0 69.86 102.76 26.26 o 6 -10 0 53.38 46.89 18.57 o 7 -10 0 18.55 0.34 14.41 o 8 -10 0 85.96 37.51 30.01 o 1 -9 0 35.85 46.89 13.26 o 2 -9 0 38.07 24.76 16.88 o 3 -9 0 103.01 109.55 19.76 o 4 -9 0 121.52 135.13 30.01 o 5 -9 0 339.94 346.19 35.74 o 6 -9 0 227.91 260.69 33.08 o 7 -9 0 314.36 308.34 35.74 o 8 -9 0 569.17 416.38 63.77 o 9 -9 0 202.98 176.46 33.08 o 0 -8 0 13250.87 13060.60 277.59 o 1 -8 0 313.02 316.53 27.76 o 2 -8 0 40.42 50.64 13.26 o 3 -8 0 9085.28 9052.32 126.42 o 4 -8 0 726.54 753.77 41.05 o 5 -8 0 40.63 22.51 13.26 o 6 -8 0 2991.54 2982.19 87.41 o 7 -8 0 542.26 557.14 75.02 o 8 -8 0 113.85 106.49 45.01 o 9 -8 0 443.06 523.08 86.28 o 10 -8 0 155.67 163.51 33.08 o 1 -7 0 157.19 189.21 19.76 o 2 -7 0 34.17 25.19 9.00 o 3 -7 0 985.27 992.29 56.17 o 4 -7 0 256.68 244.93 19.25 o 5 -7 0 24.53 22.51 10.61 o 6 -7 0 1470.55 1494.26 58.17 o 7 -7 0 270.23 304.42 69.40 o 8 -7 0 62.67 60.28 33.76 o 9 -7 0 634.98 656.14 53.05 o 10 -7 0 154.67 143.33 28.82 o 11 -7 0 69.21 22.51 30.01 o 0 -6 0 103.58 100.31 6.97 o 1 -6 0 55.10 50.71 10.61 o 2 -6 0 634.43 619.27 28.82 o 3 -6 0 46.57 57.06 9.23 o 4 -6 0 274.93 251.84 18.14 o 5 -6 0 720.35 683.80 37.51 o 6 -6 0 83.76 75.02 17.09 o 7 -6 0 482.86 457.34 35.74 o 8 -6 0 440.70 504.26 43.71 o 9 -6 0 52.73 51.02 22.51 o 10 -6 0 144.70 133.83 26.53 o 11 -6 0 148.58 99.41 29.18 o 1 -5 0 145.64 227.34 18.57 o 2 -5 0 602.68 601.53 25.09 o 3 -5 0 52.75 62.52 6.14 o 4 -5 0 85.00 63.10 8.12 o 5 -5 0 822.06 813.37 30.21 o 6 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490.96 451.15 41.05 o 10 3 0 29.34 22.51 15.92 o 11 3 0 867.75 984.57 114.41 o 12 3 0 142.72 155.47 33.08 o 0 4 0 26.28 22.88 4.51 o 1 4 0 184.97 172.52 8.70 o 2 4 0 59.83 57.03 5.86 o 3 4 0 39.87 70.38 17.17 o 4 4 0 1708.17 1745.32 42.86 o 5 4 0 405.73 410.19 26.65 o 6 4 0 90.01 98.39 10.48 o 7 4 0 2352.07 2450.85 72.91 o 8 4 0 1452.59 1553.00 61.01 o 9 4 0 46.81 20.63 13.26 o 10 4 0 1556.41 1631.72 71.62 o 11 4 0 1621.50 1602.48 76.92 o 12 4 0 12.92 1.88 15.92 o 1 5 0 145.58 150.05 9.00 o 2 5 0 602.87 597.79 20.39 o 3 5 0 53.06 60.50 8.26 o 4 5 0 85.16 89.61 8.39 o 5 5 0 821.96 818.98 28.01 o 6 5 0 157.37 148.55 13.31 o 7 5 0 339.31 403.42 35.74 o 8 5 0 484.21 454.02 39.79 o 9 5 0 215.49 223.31 30.42 o 10 5 0 302.52 377.90 42.19 o 11 5 0 133.74 75.02 26.53 o 0 6 0 103.51 111.03 14.41 o 1 6 0 55.09 55.99 6.45 o 2 6 0 635.54 602.96 17.60 o 3 6 0 46.41 42.68 8.77 o 4 6 0 274.84 282.64 22.03 o 5 6 0 722.72 699.11 25.45 o 6 6 0 83.07 82.50 11.91 o 7 6 0 483.00 484.84 32.49 o 8 6 0 442.30 406.52 38.39 o 9 6 0 52.11 51.77 41.26 o 10 6 0 144.91 174.30 30.42 o 11 6 0 148.90 141.69 31.50 o 1 7 0 157.21 157.50 18.95 o 2 7 0 34.40 28.25 6.21 o 3 7 0 985.27 980.16 25.19 o 4 7 0 256.23 259.24 17.74 o 5 7 0 24.54 28.55 8.29 o 6 7 0 1471.24 1484.94 89.34 o 7 7 0 269.91 290.70 39.35 o 8 7 0 62.84 76.12 19.76 o 9 7 0 635.96 598.47 50.40 o 10 7 0 154.60 150.25 30.42 o 11 7 0 69.66 62.46 31.89 o 0 8 0 13254.86 13091.79 201.38 o 1 8 0 313.18 288.11 23.28 o 2 8 0 40.29 50.97 9.76 o 3 8 0 9088.78 9090.02 112.49 o 4 8 0 726.83 780.77 35.24 o 5 8 0 40.34 33.59 10.19 o 6 8 0 2993.57 3002.32 60.43 o 7 8 0 542.19 533.22 36.82 o 8 8 0 114.01 106.23 20.14 o 9 8 0 443.62 525.20 50.40 o 10 8 0 155.59 108.43 27.76 o 1 9 0 35.75 20.21 8.29 o 2 9 0 37.99 33.45 9.09 o 3 9 0 103.45 114.48 16.50 o 4 9 0 121.30 112.92 16.50 o 5 9 0 339.78 296.17 27.01 o 6 9 0 228.94 229.47 27.56 o 7 9 0 313.66 321.02 36.85 o 8 9 0 569.18 518.10 47.75 o 9 9 0 204.00 142.55 41.26 o 10 9 0 312.29 273.84 60.02 o 0 10 0 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23.43 o -6 -8 1 258.63 308.32 34.18 o -5 -8 1 2747.67 2849.65 83.27 o -4 -8 1 290.99 287.27 26.32 o -3 -8 1 315.90 336.77 30.42 o -2 -8 1 3246.45 3246.38 80.61 o -1 -8 1 349.76 372.92 30.42 o 0 -8 1 304.16 281.34 26.53 o 1 -8 1 1250.60 1249.14 46.36 o 2 -8 1 261.46 248.01 21.44 o 3 -8 1 268.47 301.83 23.63 o 4 -8 1 58.28 49.79 14.41 o 5 -8 1 168.01 153.30 22.43 o 6 -8 1 237.70 246.33 69.40 o 7 -8 1 85.87 81.43 28.13 o 8 -8 1 106.96 105.03 33.76 o 9 -8 1 146.21 140.29 82.53 o 10 -8 1 160.00 167.29 33.08 o -11 -7 1 77.67 75.02 37.51 o -10 -7 1 166.89 158.03 76.90 o -9 -7 1 1136.00 1346.15 64.95 o -8 -7 1 249.69 274.04 34.48 o -7 -7 1 283.56 303.85 31.50 o -6 -7 1 1958.49 2000.19 86.28 o -5 -7 1 316.87 349.71 32.45 o -4 -7 1 417.88 375.22 32.69 o -3 -7 1 1769.99 1759.77 53.94 o -2 -7 1 160.74 151.25 19.76 o -1 -7 1 470.30 376.16 27.76 o 0 -7 1 490.47 495.16 29.73 o 1 -7 1 106.21 76.71 13.26 o 2 -7 1 408.10 392.47 28.82 o 3 -7 1 53.58 55.44 10.39 o 4 -7 1 170.14 146.51 28.13 o 5 -7 1 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