#------------------------------------------------------------------------------
#$Date: 2023-04-05 14:15:34 +0300 (Wed, 05 Apr 2023) $
#$Revision: 282400 $
#$URL: file:///home/coder/svn-repositories/cod/cif/2/02/27/2022715.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/. The original data for this entry
# were provided by IUCr Journals, http://journals.iucr.org/.
#
# The file may be used within the scientific community so long as
# proper attribution is given to the journal article from which the
# data were obtained.
#
data_2022715
loop_
_publ_author_name
Vinaya,
'Basavaraju, Yeriyur B.'
'Yathirajan, Hemmige S.'
'Parkin, Sean'
_publ_section_title
;
Syntheses and crystal structures of four
4-(4-methoxyphenyl)piperazin-1-ium salts: trifluoroacetate,
2,3,4,5,6-pentafluorobenzoate, 4-iodobenzoate, and a polymorph with
4-methylbenzoate
;
_journal_coeditor_code VM2279
_journal_issue 4
_journal_name_full
'Acta Crystallographica Section E Crystallographic Communications'
_journal_page_first 380
_journal_page_last 385
_journal_paper_doi 10.1107/S2056989023002529
_journal_volume 79
_journal_year 2023
_chemical_formula_iupac 'C11 H17 N2 O +, C7 H4 I O2 -, H2 O'
_chemical_formula_moiety 'C11 H17 N2 O +, C7 H4 I O2 -, H2 O'
_chemical_formula_sum 'C18 H23 I N2 O4'
_chemical_formula_weight 458.28
_chemical_name_systematic
;
4-(4-Methoxyphenyl)piperazin-1-ium 4-iodobenzoate monohydrate
;
_space_group_crystal_system monoclinic
_space_group_IT_number 14
_space_group_name_Hall '-P 2ybc'
_space_group_name_H-M_alt 'P 1 21/c 1'
_atom_sites_solution_hydrogens mixed
_atom_sites_solution_primary direct
_atom_sites_solution_secondary difmap
_audit_creation_method 'SHELXL-2019/2 and CIFFIX'
_cell_angle_alpha 90
_cell_angle_beta 92.970(3)
_cell_angle_gamma 90
_cell_formula_units_Z 12
_cell_length_a 20.4117(18)
_cell_length_b 7.4255(6)
_cell_length_c 36.796(3)
_cell_measurement_reflns_used 9052
_cell_measurement_temperature 90.0(2)
_cell_measurement_theta_max 27.49
_cell_measurement_theta_min 2.33
_cell_volume 5569.6(8)
_computing_cell_refinement
;
APEX3 (Bruker, 2016)
;
_computing_data_collection
;
APEX3 (Bruker, 2016)
;
_computing_data_reduction
;
APEX3 (Bruker, 2016)
;
_computing_molecular_graphics
;
XP in SHELXTL (Sheldrick, 2008),
Mercury (Macrae et al., 2020)
;
_computing_publication_material
;
SHELX (Sheldrick, 2008) and publCIF (Westrip,
2010)
;
_computing_structure_refinement
;
SHELXL2019/2 (Sheldrick, 2015b)
;
_computing_structure_solution
;
SHELXT (Sheldrick, 2015a)
;
_diffrn_ambient_temperature 90.0(2)
_diffrn_detector_area_resol_mean 7.41
_diffrn_measured_fraction_theta_full 0.999
_diffrn_measured_fraction_theta_max 0.990
_diffrn_measurement_device_type 'Bruker D8 Venture dual source'
_diffrn_measurement_method '\f and \w scans'
_diffrn_radiation_type MoK\a
_diffrn_radiation_wavelength 0.71073
_diffrn_reflns_av_R_equivalents 0.0556
_diffrn_reflns_av_unetI/netI 0.0489
_diffrn_reflns_limit_h_max 26
_diffrn_reflns_limit_h_min -26
_diffrn_reflns_limit_k_max 6
_diffrn_reflns_limit_k_min -9
_diffrn_reflns_limit_l_max 47
_diffrn_reflns_limit_l_min -47
_diffrn_reflns_number 72181
_diffrn_reflns_theta_full 25.242
_diffrn_reflns_theta_max 27.658
_diffrn_reflns_theta_min 1.998
_diffrn_source microsource
_exptl_absorpt_coefficient_mu 1.750
_exptl_absorpt_correction_T_max 0.862
_exptl_absorpt_correction_T_min 0.726
_exptl_absorpt_correction_type multi-scan
_exptl_absorpt_process_details
;
(SADABS; Krause et al., 2015)
;
_exptl_crystal_colour colourless
_exptl_crystal_density_diffrn 1.640
_exptl_crystal_description plate
_exptl_crystal_F_000 2760
_exptl_crystal_size_max 0.300
_exptl_crystal_size_mid 0.130
_exptl_crystal_size_min 0.030
_refine_diff_density_max 0.839
_refine_diff_density_min -0.805
_refine_ls_extinction_coef 0.00017(3)
_refine_ls_extinction_expression Fc^*^=kFc[1+0.001xFc^2^\l^3^/sin(2\q)]^-1/4^
_refine_ls_extinction_method
;
SHELXL-2019/2 (Sheldrick 2015b)
;
_refine_ls_goodness_of_fit_ref 1.029
_refine_ls_hydrogen_treatment mixed
_refine_ls_matrix_type full
_refine_ls_number_parameters 729
_refine_ls_number_reflns 12876
_refine_ls_number_restraints 12
_refine_ls_restrained_S_all 1.029
_refine_ls_R_factor_all 0.0507
_refine_ls_R_factor_gt 0.0328
_refine_ls_shift/su_max 0.002
_refine_ls_shift/su_mean 0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[\s^2^(Fo^2^)+(0.0216P)^2^+1.7628P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme calc
_refine_ls_wR_factor_gt 0.0637
_refine_ls_wR_factor_ref 0.0687
_reflns_number_gt 10003
_reflns_number_total 12876
_reflns_threshold_expression 'I > 2\s(I)'
_cod_data_source_file vm2279sup1.cif
_cod_data_source_block III
_cod_original_sg_symbol_H-M 'P 21/c'
_cod_database_code 2022715
_shelx_space_group_comment
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;
_shelx_estimated_absorpt_t_min 0.622
_shelx_estimated_absorpt_t_max 0.949
_shelx_hkl_file
;
-2 0 0 186.064 10.0627 2
-2 0 0 190.756 10.2333 3
-2 0 0 188.601 10.6511 4
2 0 0 190.103 10.1330 2
2 0 0 180.447 10.5225 3
2 0 0 212.977 10.9713 4
3 0 0 16.4716 2.19118 4
3 0 0 15.0024 1.77366 2
-3 0 0 13.9758 1.58840 2
-3 0 0 14.4533 1.79019 2
-3 0 0 15.5741 1.78824 3
-3 0 0 15.2679 2.08208 4
3 0 0 13.2476 1.61173 2
3 0 0 15.3237 1.95923 3
-4 0 0 1133.97 57.8131 2
-4 0 0 1151.24 58.2196 3
4 0 0 1159.40 57.8093 2
4 0 0 1141.54 58.0897 2
4 0 0 1213.34 58.3523 3
4 0 0 1187.51 58.8225 4
-4 0 0 1178.00 58.1722 2
5 0 0 313.219 17.0508 2
-5 0 0 324.643 18.1539 4
-5 0 0 311.310 17.4040 2
-5 0 0 296.318 16.9266 2
5 0 0 332.606 18.2899 4
5 0 0 327.178 17.6565 3
5 0 0 326.473 18.0700 2
6 0 0 5638.91 270.950 3
-6 0 0 5314.76 270.734 3
6 0 0 5650.83 271.742 4
7 0 0 2211.08 108.996 2
7 0 0 2261.03 109.869 3
7 0 0 2236.75 110.753 4
-7 0 0 2211.15 109.965 3
-7 0 0 2152.05 109.581 2
7 0 0 2146.38 110.339 2
8 0 0 3033.50 152.734 3
8 0 0 2932.74 149.915 2
8 0 0 3148.13 152.099 4
-8 0 0 3057.74 150.769 2
9 0 0 185.133 12.2355 3
9 0 0 181.243 11.4290 2
-9 0 0 172.822 11.9282 2
9 0 0 181.616 13.1961 4
10 0 0 15.8536 3.05938 2
10 0 0 11.7746 3.04941 3
10 0 0 10.9213 4.03509 4
-10 0 0 8.54356 2.99435 2
11 0 0 336.810 20.4189 2
11 0 0 372.708 21.8555 3
-11 0 0 358.403 21.4758 2
11 0 0 361.892 23.0017 4
12 0 0 838.039 45.9220 4
12 0 0 826.689 44.4744 3
-12 0 0 788.000 43.9949 2
12 0 0 788.321 42.9260 2
13 0 0 1659.09 84.7652 2
13 0 0 1694.03 86.3753 3
-13 0 0 1631.68 85.7223 2
14 0 0 531.227 30.6949 2
-14 0 0 567.420 38.0601 2
14 0 0 535.302 32.1134 3
15 0 0 246.176 23.4842 3
15 0 0 228.718 16.0265 2
-15 0 0 253.888 18.2707 2
-16 0 0 35.3697 6.34491 2
16 0 0 25.2742 5.90061 3
16 0 0 26.0515 4.78625 2
17 0 0 79.1614 8.51812 2
-17 0 0 74.7599 9.48988 2
17 0 0 89.3578 9.66906 3
18 0 0 265.185 19.3612 2
18 0 0 268.383 20.6597 3
-18 0 0 294.135 22.2457 2
19 0 0 166.141 13.7824 2
19 0 0 186.628 15.5894 3
-19 0 0 139.780 16.3138 2
-20 0 0 315.806 28.8048 2
20 0 0 423.263 26.1124 2
20 0 0 402.571 27.2119 3
21 0 0 152.420 15.4076 3
21 0 0 156.226 17.3083 2
-22 0 0 43.6949 10.5002 2
22 0 0 26.4350 7.38222 3
22 0 0 24.3897 7.19959 2
23 0 0 4.84242 4.73095 2
23 0 0 3.72139 4.70158 3
24 0 0 25.5081 7.87471 2
-24 0 0 37.2340 12.9073 2
24 0 0 38.7038 9.22000 3
-25 0 0 14.7003 10.7346 2
25 0 0 6.29465 6.34572 3
25 0 0 8.24762 5.93298 2
26 0 0 23.9139 8.68744 3
26 0 0 14.7865 6.94661 2
0 -1 0 -0.0620 0.47461 4
0 1 0 -0.0698 0.46850 4
1 -1 0 114.505 6.71687 2
1 -1 0 124.545 6.96008 4
-1 -1 0 124.035 6.40032 5
1 -1 0 122.708 7.24352 3
1 -1 0 119.795 6.25704 2
-1 -1 0 128.192 6.98122 4
1 1 0 122.648 6.40775 5
-1 1 0 119.844 7.19977 3
-1 1 0 121.981 6.94676 4
-2 -1 0 643.255 31.9165 5
2 -1 0 627.898 32.1230 2
2 -1 0 666.659 32.6047 4
-2 -1 0 662.566 31.8935 2
-2 -1 0 625.499 32.4008 3
2 -1 0 651.327 32.1086 2
2 -1 0 645.160 32.8729 3
-2 1 0 640.287 31.9809 2
2 1 0 626.607 31.9306 5
-2 1 0 637.395 31.9990 2
-2 1 0 650.252 32.9014 3
-2 1 0 670.441 32.6055 4
-3 -1 0 854.950 41.7773 2
-3 -1 0 858.834 41.6647 5
3 -1 0 886.868 42.6604 3
-3 -1 0 821.141 41.9675 3
3 -1 0 802.863 41.7803 2
3 -1 0 824.062 42.0151 2
3 -1 0 864.593 42.3513 4
-3 -1 0 831.167 41.4701 2
-3 1 0 836.960 41.8923 2
-3 1 0 855.245 42.3326 4
3 1 0 820.285 42.0687 3
3 1 0 847.919 41.5186 2
-3 1 0 822.615 41.7714 2
-3 1 0 853.238 42.6551 3
3 1 0 832.051 41.6510 5
3 1 0 838.283 41.4085 2
4 -1 0 1071.17 54.1959 2
4 -1 0 1106.41 55.0027 3
4 -1 0 1103.98 54.8600 4
-4 -1 0 1072.83 54.3399 3
4 -1 0 1100.79 54.6399 2
-4 -1 0 1077.79 53.8522 2
-4 -1 0 1100.57 54.3397 2
4 1 0 1107.96 53.8385 2
-4 1 0 1059.00 54.1789 2
4 1 0 1079.26 54.0738 5
4 1 0 1088.00 54.0630 2
-4 1 0 1110.19 54.8426 4
4 1 0 1097.30 54.4857 3
-4 1 0 1107.04 55.1070 3
-4 1 0 1076.81 54.4099 2
5 -1 0 1196.37 58.7043 4
-5 -1 0 1158.12 58.0549 2
5 -1 0 1105.76 58.1997 2
-5 -1 0 1169.04 58.7879 3
5 -1 0 1184.04 58.6358 3
-5 -1 0 1191.92 57.8581 2
5 -1 0 1147.38 57.8041 2
5 1 0 1174.00 58.1035 3
-5 1 0 1165.80 58.5263 4
-5 1 0 1168.08 58.7500 3
5 1 0 1125.42 57.7137 2
-5 1 0 1114.35 58.0492 2
5 1 0 1126.69 57.7280 5
-5 1 0 1147.91 58.3799 2
5 1 0 1201.21 57.4534 2
6 -1 0 141.297 9.40482 4
6 -1 0 127.001 8.77587 2
6 -1 0 150.742 9.34543 3
-6 -1 0 136.633 8.73800 2
6 -1 0 144.805 8.57046 2
-6 -1 0 129.481 9.42213 4
-6 -1 0 137.933 8.12383 2
-6 -1 0 136.255 8.59740 3
6 1 0 132.385 8.29490 5
-6 1 0 128.343 8.93546 4
6 1 0 139.820 8.76035 3
-6 1 0 130.762 8.71817 2
-6 1 0 130.307 9.21468 3
6 1 0 141.090 8.10962 2
-6 1 0 127.038 8.30079 2
7 -1 0 357.758 20.0077 4
-7 -1 0 340.499 18.9727 2
-7 -1 0 328.922 18.7646 3
7 1 0 352.529 19.0362 3
7 1 0 326.835 18.5254 2
7 1 0 349.683 18.2024 2
7 1 0 299.015 18.2174 5
8 -1 0 134.672 9.23846 2
-8 -1 0 138.496 9.66341 2
8 -1 0 146.574 10.1976 3
8 -1 0 141.882 10.5335 4
-8 1 0 146.682 9.74883 2
8 1 0 131.870 9.27962 2
-9 -1 0 3381.24 169.513 2
9 -1 0 3359.04 169.044 2
9 -1 0 3557.32 170.256 3
9 -1 0 3487.52 171.148 4
9 1 0 3390.65 168.445 2
-9 1 0 3394.20 169.499 2
9 1 0 3391.42 169.458 3
-10 -1 0 3045.26 150.608 2
10 -1 0 3119.74 151.571 3
10 -1 0 3180.76 150.413 2
-10 1 0 2965.46 150.463 2
10 1 0 2882.38 149.306 2
10 1 0 2943.53 150.473 3
-11 -1 0 136.295 10.5564 2
11 -1 0 140.438 11.7592 4
11 -1 0 136.053 10.3211 2
11 -1 0 147.498 11.3497 3
11 1 0 140.841 10.5966 3
11 1 0 144.866 9.83549 2
-11 1 0 144.241 10.6888 2
12 -1 0 156.943 11.4188 2
12 -1 0 166.931 13.6933 4
12 -1 0 167.253 12.7032 3
-12 -1 0 161.611 11.9969 2
12 1 0 148.068 11.6661 3
12 1 0 156.552 10.8843 2
-12 1 0 165.275 12.0026 2
-13 -1 0 13.7902 3.84430 2
13 -1 0 16.2773 4.43658 3
13 -1 0 11.9372 4.44409 4
13 -1 0 18.6506 3.87935 2
13 1 0 6.34388 2.61139 2
13 1 0 12.1926 3.36390 3
-13 1 0 11.5188 3.85087 2
14 -1 0 141.940 13.1118 3
14 -1 0 160.605 15.0160 4
-14 -1 0 159.842 13.0647 2
14 -1 0 168.220 13.7506 2
14 1 0 157.812 11.6008 2
14 1 0 168.161 12.7963 3
15 -1 0 330.493 22.3567 3
-15 -1 0 345.467 21.7122 2
15 -1 0 313.678 20.6409 2
15 -1 0 313.598 23.2154 4
15 1 0 359.843 22.4001 3
15 1 0 309.938 21.3653 2
-15 1 0 317.610 21.6672 2
16 -1 0 387.359 29.0417 4
16 -1 0 427.034 27.1392 3
16 -1 0 405.314 25.6275 2
-16 -1 0 398.091 27.1324 2
-16 1 0 436.318 27.1848 2
16 1 0 423.368 25.4588 2
16 1 0 437.780 26.8364 3
-17 -1 0 466.392 31.9027 2
17 -1 0 493.168 30.5213 2
17 -1 0 508.733 33.5709 4
17 -1 0 447.469 31.1857 3
17 1 0 539.125 31.6582 3
-17 1 0 496.264 32.1725 2
17 1 0 514.884 29.7857 2
18 -1 0 258.070 19.0665 2
18 -1 0 256.054 22.0530 4
18 -1 0 238.546 19.6233 3
-18 -1 0 254.982 20.3364 2
18 1 0 276.833 19.7346 3
18 1 0 250.499 17.9142 2
-18 1 0 224.149 21.6445 2
19 -1 0 111.564 12.7580 3
-19 -1 0 140.702 13.8364 2
19 -1 0 102.220 11.1871 2
19 1 0 111.689 11.0531 2
-19 1 0 110.898 13.7381 2
19 1 0 131.249 12.3900 3
20 -1 0 17.1447 6.20971 3
20 -1 0 20.6917 6.09994 2
20 1 0 28.4711 6.26801 3
-20 1 0 35.0489 8.59917 2
20 1 0 18.5584 5.49752 2
-21 -1 0 18.4738 8.32900 2
21 -1 0 24.5887 7.21209 2
21 1 0 14.6351 5.18420 2
21 1 0 19.5770 6.56094 3
-21 1 0 26.6861 9.72275 2
22 -1 0 63.9700 10.2044 3
-22 -1 0 91.1572 14.5849 2
22 -1 0 60.6098 9.81243 2
22 1 0 71.3764 11.5716 3
-22 1 0 84.7883 15.3375 2
23 -1 0 139.394 16.8046 3
23 -1 0 181.097 16.7590 2
23 1 0 192.877 17.3777 3
23 1 0 185.269 16.3725 2
24 -1 0 23.9479 8.54353 3
-24 -1 0 37.0985 11.4583 2
24 -1 0 30.4056 8.17518 2
24 1 0 25.1153 8.40086 3
-24 1 0 27.9992 11.7140 2
24 1 0 26.7405 7.47884 2
25 -1 0 139.463 16.5206 3
-25 -1 0 189.302 24.9034 2
25 -1 0 139.023 16.0431 2
25 1 0 148.879 15.7116 2
25 1 0 144.676 16.0597 3
26 -1 0 31.3667 10.7922 3
26 1 0 51.9652 10.3690 3
26 1 0 40.7436 9.66662 2
0 -2 0 9999.99 485.909 4
0 -2 0 9996.14 486.463 3
0 2 0 9950.43 485.792 4
1 -2 0 13.1327 2.40042 3
-1 -2 0 10.6919 1.40625 5
1 -2 0 17.9764 2.27521 4
-1 -2 0 13.7232 2.16793 4
1 2 0 12.1835 2.02950 4
-2 -2 0 122.614 6.80941 5
-2 -2 0 123.091 7.88993 4
2 -2 0 126.588 8.46444 3
2 -2 0 119.253 6.79466 2
2 -2 0 124.358 7.87831 4
2 -2 0 116.507 6.74594 2
-2 2 0 119.371 8.30148 3
-2 2 0 125.380 8.43575 4
2 2 0 122.601 6.86172 5
3 -2 0 225.219 12.4052 2
3 -2 0 233.321 13.8635 3
-3 -2 0 222.458 11.7459 2
3 -2 0 230.536 13.2828 4
3 -2 0 224.065 12.3806 2
-3 -2 0 240.347 11.8393 2
-3 -2 0 229.454 12.0842 5
3 2 0 231.143 12.2063 5
-3 2 0 222.743 11.6557 2
-3 2 0 220.182 13.7803 3
-3 2 0 233.765 11.7558 2
-4 -2 0 1.04134 0.72459 2
-4 -2 0 0.71256 0.84251 3
4 -2 0 1.05568 1.03394 2
4 -2 0 1.00631 1.19521 4
-4 -2 0 0.69665 0.71507 5
4 -2 0 -0.4422 0.95220 2
4 -2 0 0.98761 1.31563 3
-4 -2 0 0.87382 0.84968 2
4 2 0 0.00358 0.72533 5
-4 2 0 -0.3325 0.94102 4
-4 2 0 0.69666 0.90207 2
-4 2 0 1.14346 0.85433 2
5 -2 0 6.81884 1.80057 2
5 -2 0 5.75056 1.91443 2
-5 -2 0 8.58254 1.48803 5
-5 -2 0 6.83940 1.68985 2
-5 -2 0 6.58839 1.68812 3
5 -2 0 5.79424 2.12556 4
-5 2 0 6.50997 1.62450 2
5 2 0 7.09121 1.37961 5
-5 2 0 8.24321 1.62723 2
5 2 0 7.12980 1.45779 2
-5 2 0 6.01741 1.97008 4
-6 -2 0 142.820 8.83030 2
6 -2 0 140.635 9.98260 3
-6 -2 0 132.076 8.94994 3
-6 -2 0 134.268 8.13508 2
6 -2 0 155.654 9.87738 4
6 -2 0 137.225 8.81336 2
-6 2 0 139.991 8.76124 2
6 2 0 132.420 8.39942 5
6 2 0 140.414 9.31322 3
-6 2 0 139.142 8.64399 2
6 2 0 140.319 7.90194 2
-7 -2 0 72.5868 5.78152 2
7 -2 0 67.3377 6.46334 3
7 -2 0 72.2009 6.55564 4
7 -2 0 77.0149 6.07901 2
-7 2 0 69.6829 6.25349 2
7 2 0 80.9349 6.68696 3
7 2 0 67.3109 4.93962 2
-7 2 0 66.1628 5.40276 2
7 2 0 75.1614 4.95292 2
7 2 0 72.7614 5.37749 5
8 -2 0 547.099 30.5075 3
-8 -2 0 556.973 33.1890 2
8 -2 0 538.856 30.4327 4
8 -2 0 528.920 29.1962 2
8 2 0 555.982 29.8852 3
8 2 0 568.422 28.4230 2
-8 2 0 523.511 29.2667 2
9 -2 0 311.669 18.8958 3
9 -2 0 303.942 19.0257 4
9 -2 0 316.877 17.8510 2
-9 -2 0 300.557 17.8329 2
9 2 0 309.166 18.2040 3
9 2 0 288.598 16.8513 2
-9 2 0 296.958 17.7036 2
9 2 0 270.903 16.9541 2
10 -2 0 435.501 26.3573 4
-10 -2 0 443.827 25.2411 2
10 -2 0 432.386 24.9037 2
10 -2 0 444.459 26.3372 3
-10 2 0 421.177 24.9516 2
10 2 0 459.203 24.0868 2
10 2 0 456.728 25.5894 3
11 -2 0 39.3349 5.70194 3
11 -2 0 40.3512 6.04676 4
-11 -2 0 40.0000 5.16122 2
11 -2 0 39.1287 4.97670 2
11 2 0 41.0147 4.31481 2
11 2 0 41.4910 5.15656 3
-11 2 0 43.4349 5.15040 2
12 -2 0 12.7389 4.72240 4
12 -2 0 6.58431 3.18751 3
-12 -2 0 13.0079 3.44198 2
12 -2 0 7.17623 3.08840 2
12 2 0 8.16586 3.02257 3
12 2 0 11.0497 2.66500 2
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-4 -8 13 2.79505 2.97160 5
4 -8 -13 0.70072 3.43798 2
-4 -8 13 -1.5590 3.13678 4
-3 -8 13 49.0700 7.09529 4
-3 -8 13 43.2282 6.59035 5
3 -8 -13 45.3038 9.17742 4
3 -8 -13 48.7589 10.1582 3
-3 -8 13 47.2954 8.96755 3
3 -8 -13 48.8408 7.89768 2
-2 -8 13 20.8928 8.21959 3
-2 -8 13 15.0333 5.06195 4
2 -8 -13 14.8411 5.23613 2
2 -8 -13 17.0366 6.58560 4
-2 -8 13 14.9680 4.75974 5
2 -8 -13 23.3722 7.88540 3
1