Crystallography Open Database

Information card for entry 2022740

2022739 << 2022740 >> 2022741

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Structure parameters

Chemical name	Bis[4-(allyloxy)-<i>N</i>'-(but-2-en-1-ylidene)benzohydrazidato]nickel(II)
Formula	C28 H30 N4 Ni O4
Calculated formula	C28 H30 N4 Ni O4
Title of publication	Crystal structure of bis-[4-(all-yloxy)-<i>N</i>'-(but-2-en-1-yl-idene)benzohydrazidato]nickel(II).
Authors of publication	Khan, Sultana Shakila; Howlader, Md Belayet Hossain; Sheikh, Md Chanmiya; Miyatake, Ryuta; Zangrando, Ennio
Journal of publication	Acta crystallographica. Section E, Crystallographic communications
Year of publication	2023
Journal volume	79
Journal issue	Pt 5
Pages of publication	465 - 468
a	8.0978 ± 0.0008 Å
b	9.2021 ± 0.0009 Å
c	9.3316 ± 0.001 Å
α	84.027 ± 0.006°
β	88.091 ± 0.006°
γ	84.17 ± 0.006°
Cell volume	687.83 ± 0.12 Å³
Cell temperature	173 ± 2 K
Ambient diffraction temperature	173 ± 2 K
Number of distinct elements	5
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0471
Residual factor for significantly intense reflections	0.0395
Weighted residual factors for significantly intense reflections	0.0943
Weighted residual factors for all reflections included in the refinement	0.0979
Goodness-of-fit parameter for all reflections included in the refinement	1.026
Diffraction radiation wavelength	0.71075 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	Yes

Version history

Revision	Date	Message	Files
284378 (current)	2023-06-06	cif/ Updating files of 2022740 Original log message: Adding full bibliography for 2022740.cif.	2022740.cif 2022740.hkl
282648	2023-04-15	cif/ hkl/ Adding structures of 2022740 via cif-deposit CGI script.	2022740.cif 2022740.hkl