#------------------------------------------------------------------------------ #$Date: 2023-04-15 04:52:11 +0300 (Sat, 15 Apr 2023) $ #$Revision: 282652 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/02/27/2022747.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2022747 _cell_angle_alpha 90.000 _cell_angle_beta 98.429 _cell_angle_gamma 90.000 _cell_length_a 12.4059 _cell_length_b 10.9893 _cell_length_c 20.5806 _exptl_crystal_F_000 1080.00 _reflns_d_resolution_high 0.7884 _cod_data_source_file zn2027Isup2.hkl _cod_data_source_block I _shelx_title ' Sample14 in P2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 256.17 _shelx_f_squared_multiplier 1.000 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 3455.51 3209.03 73.27 o 2 0 0 169.19 197.82 5.46 o 3 0 0 1355.07 1279.53 30.72 o 4 0 0 3248.31 3157.50 61.18 o 5 0 0 2083.86 2199.63 44.15 o 6 0 0 1019.00 1092.97 43.66 o 7 0 0 240.93 311.99 12.20 o 8 0 0 328.17 433.69 16.12 o 9 0 0 165.04 157.24 2.39 o 10 0 0 1220.04 1055.29 11.46 o 11 0 0 1114.88 1090.44 13.73 o 12 0 0 819.17 894.29 10.87 o 13 0 0 80.43 83.15 3.08 o 1 1 0 1310.88 1214.95 13.33 o 2 1 0 12652.65 11611.52 132.15 o 3 1 0 3578.93 3486.36 38.20 o 4 1 0 3356.30 3253.03 38.06 o 5 1 0 2667.19 2830.35 42.81 o 6 1 0 998.05 905.10 15.15 o 7 1 0 1451.03 1549.33 33.79 o 8 1 0 474.16 435.18 4.88 o 9 1 0 10.81 15.50 0.47 o 10 1 0 1251.23 1229.44 7.78 o 11 1 0 91.57 104.57 1.11 o 12 1 0 188.31 204.57 3.91 o 13 1 0 177.72 160.08 2.27 o 14 1 0 1.63 10.19 6.04 o 0 2 0 3957.15 3547.51 143.96 o 1 2 0 34276.84 29873.87 470.24 o 2 2 0 3038.65 2878.54 29.86 o 3 2 0 259.60 227.36 3.33 o 4 2 0 5977.68 5972.82 61.83 o 5 2 0 197.68 224.33 8.56 o 6 2 0 2117.12 2253.25 31.94 o 7 2 0 278.09 308.60 8.59 o 8 2 0 290.97 332.51 2.84 o 9 2 0 559.18 563.37 5.05 o 10 2 0 264.91 213.14 2.08 o 11 2 0 22.38 24.26 1.14 o 12 2 0 646.79 691.79 6.42 o 13 2 0 1.78 1.42 0.78 o 14 2 0 18.73 13.03 1.48 o 1 3 0 10187.22 9916.67 160.31 o 2 3 0 27.59 26.43 1.06 o 3 3 0 4360.94 4482.76 52.06 o 4 3 0 723.90 725.59 12.04 o 5 3 0 506.63 604.08 9.54 o 6 3 0 111.11 120.50 4.12 o 7 3 0 10.50 1.85 1.05 o 8 3 0 14.20 8.70 0.43 o 9 3 0 83.32 63.67 1.21 o 10 3 0 266.56 283.94 2.46 o 11 3 0 214.27 206.15 1.94 o 12 3 0 12.14 13.13 0.83 o 13 3 0 32.38 40.05 1.22 o 14 3 0 1094.56 1160.26 32.04 o 0 4 0 9329.24 9712.24 223.78 o 1 4 0 1004.59 1065.62 31.86 o 2 4 0 46.83 32.07 2.22 o 3 4 0 302.92 319.89 6.52 o 4 4 0 279.31 313.15 7.10 o 5 4 0 3193.61 3219.07 41.72 o 6 4 0 21.58 30.82 1.65 o 7 4 0 110.09 116.12 1.73 o 8 4 0 1117.17 1095.14 8.14 o 9 4 0 10.42 11.26 0.55 o 10 4 0 10.36 11.52 0.59 o 11 4 0 11.35 16.53 0.77 o 12 4 0 609.74 530.54 7.96 o 13 4 0 849.65 834.72 20.12 o 14 4 0 0.79 0.84 0.99 o 1 5 0 234.53 222.31 5.07 o 2 5 0 4469.56 4776.20 71.44 o 3 5 0 69.10 74.61 4.08 o 4 5 0 13.00 17.32 1.87 o 5 5 0 115.33 112.31 4.41 o 6 5 0 72.30 69.45 1.70 o 7 5 0 1.26 1.52 0.56 o 8 5 0 151.51 176.15 3.25 o 9 5 0 9.91 13.61 0.65 o 10 5 0 116.58 110.56 1.82 o 11 5 0 79.99 65.10 1.86 o 12 5 0 41.96 31.26 1.27 o 13 5 0 25.46 21.52 1.39 o 14 5 0 510.79 580.24 40.29 o 0 6 0 1824.05 1810.78 31.59 o 1 6 0 668.11 828.52 14.37 o 2 6 0 11.89 6.10 1.19 o 3 6 0 122.99 105.36 3.47 o 4 6 0 753.16 740.96 21.35 o 5 6 0 0.02 1.76 0.62 o 6 6 0 60.96 46.77 1.41 o 7 6 0 277.66 262.85 4.74 o 8 6 0 70.30 54.51 1.42 o 9 6 0 484.73 474.04 4.53 o 10 6 0 66.86 68.37 1.44 o 11 6 0 32.74 47.12 1.30 o 12 6 0 155.19 166.47 2.78 o 13 6 0 0.61 -0.04 0.90 o 14 6 0 379.97 293.55 53.72 o 1 7 0 17.33 12.72 1.31 o 2 7 0 1267.90 1253.29 16.14 o 3 7 0 615.19 617.65 9.05 o 4 7 0 79.61 84.90 1.64 o 5 7 0 352.89 308.09 6.49 o 6 7 0 148.94 150.81 2.75 o 7 7 0 16.32 17.92 1.09 o 8 7 0 4.42 6.96 0.84 o 9 7 0 81.93 78.44 1.65 o 10 7 0 23.30 22.71 1.06 o 11 7 0 175.01 175.18 4.08 o 12 7 0 182.22 194.15 5.72 o 13 7 0 111.41 92.22 4.66 o 0 8 0 3746.88 3614.66 69.66 o 1 8 0 95.96 95.75 2.33 o 2 8 0 503.97 554.19 7.04 o 3 8 0 398.70 366.60 5.98 o 4 8 0 1429.54 1364.16 23.35 o 5 8 0 172.90 168.37 5.85 o 6 8 0 319.54 297.39 4.69 o 7 8 0 54.04 38.13 1.51 o 8 8 0 102.69 106.04 2.20 o 9 8 0 15.40 18.39 1.07 o 10 8 0 60.36 58.94 1.37 o 11 8 0 128.33 138.48 3.95 o 12 8 0 5.33 5.06 1.26 o 1 9 0 135.94 136.94 3.00 o 2 9 0 3.14 7.42 0.93 o 3 9 0 485.25 463.90 6.72 o 4 9 0 513.05 461.91 9.47 o 5 9 0 34.87 29.49 1.18 o 6 9 0 33.79 32.81 1.64 o 7 9 0 0.74 1.22 1.29 o 8 9 0 121.35 132.53 3.37 o 9 9 0 53.04 54.82 1.41 o 10 9 0 208.02 214.08 4.37 o 11 9 0 39.09 44.39 1.77 o 0 10 0 239.65 213.95 5.23 o 1 10 0 26.92 19.32 1.38 o 2 10 0 550.31 599.63 7.39 o 3 10 0 167.54 162.13 3.84 o 4 10 0 232.13 225.55 5.16 o 5 10 0 211.20 196.62 4.52 o 6 10 0 123.14 133.38 3.14 o 7 10 0 233.49 267.68 5.43 o 8 10 0 208.11 212.59 4.96 o 9 10 0 72.35 76.57 2.41 o 10 10 0 49.03 56.04 1.72 o 1 11 0 1004.05 1031.05 14.37 o 2 11 0 147.68 126.13 4.10 o 3 11 0 138.34 133.03 5.33 o 4 11 0 0.02 0.76 1.11 o 5 11 0 13.66 17.85 1.31 o 6 11 0 57.78 63.25 1.77 o 7 11 0 202.06 239.60 5.40 o 8 11 0 134.02 150.26 3.16 o 9 11 0 2.61 3.76 1.00 o 0 12 0 498.59 546.97 14.45 o 1 12 0 153.50 180.60 4.18 o 2 12 0 61.94 62.18 2.80 o 3 12 0 32.79 33.76 2.27 o 4 12 0 57.90 68.53 2.49 o 5 12 0 1.87 4.80 1.25 o 6 12 0 226.56 270.53 6.49 o 7 12 0 212.49 214.68 4.64 o 1 13 0 16.26 14.97 1.40 o 2 13 0 147.96 156.71 4.42 o 3 13 0 90.97 97.55 3.84 o 4 13 0 275.10 293.30 5.51 o 5 13 0 172.53 167.72 4.37 o -14 1 1 10.11 4.60 1.07 o -13 1 1 23.94 35.25 1.65 o -12 1 1 1518.10 1507.41 12.21 o -11 1 1 337.70 342.68 2.81 o -10 1 1 231.00 202.64 2.25 o -9 1 1 13.92 15.95 0.46 o -8 1 1 233.55 241.51 3.10 o -7 1 1 785.73 871.79 13.41 o -6 1 1 78.50 63.03 1.95 o -5 1 1 149.88 137.04 4.14 o -4 1 1 505.02 479.66 6.64 o -3 1 1 1535.26 1500.91 18.03 o -2 1 1 1415.70 1327.21 14.89 o -1 1 1 11269.63 9913.08 157.30 o 0 1 1 4426.10 3962.72 128.53 o 1 1 1 2503.34 2300.39 28.46 o 2 1 1 3582.58 3361.80 49.24 o 3 1 1 7612.07 7188.36 116.45 o 4 1 1 213.69 193.47 4.41 o 5 1 1 3771.25 3886.92 57.65 o 6 1 1 98.12 129.37 5.48 o 7 1 1 0.23 1.50 1.80 o 8 1 1 604.30 570.56 6.29 o 9 1 1 36.56 44.42 0.62 o 10 1 1 175.40 153.12 1.57 o 11 1 1 3.72 2.83 0.48 o 12 1 1 141.70 149.18 1.95 o 13 1 1 16.46 19.63 0.97 o 14 1 1 0.30 7.42 5.15 o -14 2 1 146.36 145.52 5.77 o -13 2 1 0.73 1.74 0.96 o -12 2 1 275.03 252.42 2.61 o -11 2 1 3090.96 2993.21 20.43 o -10 2 1 1218.40 1157.65 7.06 o -9 2 1 11.64 7.49 0.43 o -8 2 1 14.45 12.16 0.44 o -7 2 1 1968.94 2085.32 82.55 o -6 2 1 1966.29 1947.57 26.51 o -5 2 1 341.32 342.26 5.49 o -4 2 1 221.00 199.94 3.50 o -3 2 1 444.44 468.38 5.84 o -2 2 1 609.85 540.75 6.90 o -1 2 1 6625.33 6059.84 85.48 o 0 2 1 558.70 470.38 8.61 o 1 2 1 65621.20 52851.83 757.66 o 2 2 1 3065.12 3059.96 41.18 o 3 2 1 1991.33 2035.84 24.40 o 4 2 1 201.90 198.19 3.49 o 5 2 1 1005.81 1118.72 10.99 o 6 2 1 334.45 314.09 6.53 o 7 2 1 716.31 790.44 16.91 o 8 2 1 68.14 73.27 0.97 o 9 2 1 2297.52 2220.12 18.56 o 10 2 1 262.35 283.47 3.24 o 11 2 1 926.64 864.63 7.22 o 12 2 1 0.46 1.23 0.64 o 13 2 1 21.76 20.70 1.03 o 14 2 1 179.34 174.77 7.34 o -14 3 1 76.55 68.69 3.38 o -13 3 1 726.11 735.52 12.96 o -12 3 1 1465.44 1358.46 11.78 o -11 3 1 42.17 52.05 1.10 o -10 3 1 549.89 519.53 4.05 o -9 3 1 675.28 679.48 5.20 o -8 3 1 0.19 1.18 0.38 o -7 3 1 27.24 31.03 3.20 o -6 3 1 1128.89 1135.16 17.58 o -5 3 1 460.72 465.39 6.24 o -4 3 1 1.79 2.64 0.76 o -3 3 1 2057.44 1995.83 25.43 o -2 3 1 572.11 497.96 16.18 o -1 3 1 8300.56 7875.45 129.45 o 0 3 1 1074.21 1036.20 18.17 o 1 3 1 20669.02 19025.38 232.05 o 2 3 1 246.76 304.61 5.00 o 3 3 1 417.67 487.56 7.24 o 4 3 1 699.05 710.67 10.19 o 5 3 1 1935.99 1988.15 29.46 o 6 3 1 1.56 12.54 1.15 o 7 3 1 382.87 342.14 4.26 o 8 3 1 0.05 1.45 0.34 o 9 3 1 138.02 138.50 1.59 o 10 3 1 23.77 26.06 0.71 o 11 3 1 54.75 55.10 1.17 o 12 3 1 191.88 189.39 2.37 o 13 3 1 145.63 154.99 3.23 o 14 3 1 12.63 12.25 1.66 o -14 4 1 32.84 38.42 1.95 o -13 4 1 31.62 29.00 1.28 o -12 4 1 8.56 9.92 0.95 o -11 4 1 24.10 35.19 1.07 o -10 4 1 587.06 527.60 3.88 o -9 4 1 281.72 236.25 1.97 o -8 4 1 0.11 2.22 0.43 o -7 4 1 84.41 68.62 1.36 o -6 4 1 644.54 636.16 30.32 o -5 4 1 19.58 30.37 1.75 o -4 4 1 240.92 253.90 6.67 o -3 4 1 295.27 360.36 9.46 o -2 4 1 10110.21 9940.31 161.78 o -1 4 1 4.94 5.54 1.51 o 0 4 1 1229.34 1065.66 19.17 o 1 4 1 125.15 145.23 4.72 o 2 4 1 2748.40 2761.98 37.24 o 3 4 1 164.29 194.46 3.49 o 4 4 1 5339.48 5757.46 77.42 o 5 4 1 918.06 1084.04 16.39 o 6 4 1 239.56 231.10 5.10 o 7 4 1 386.35 357.16 3.63 o 8 4 1 90.91 84.65 1.25 o 9 4 1 0.86 1.09 0.46 o 10 4 1 1311.33 1230.04 8.49 o 11 4 1 917.88 886.58 8.32 o 12 4 1 254.05 243.04 3.37 o 13 4 1 46.96 48.60 1.99 o 14 4 1 488.09 494.77 12.97 o -14 5 1 158.35 160.01 5.13 o -13 5 1 268.24 294.65 5.13 o -12 5 1 11.86 9.26 1.09 o -11 5 1 170.34 182.01 2.65 o -10 5 1 0.47 1.92 0.59 o -9 5 1 466.55 461.98 6.79 o -8 5 1 785.49 807.73 7.17 o -7 5 1 58.66 60.76 1.49 o -6 5 1 1584.22 1583.48 18.03 o -5 5 1 165.05 178.95 7.25 o -4 5 1 2815.83 2734.09 49.02 o -3 5 1 1229.71 1321.30 21.37 o -2 5 1 494.85 533.87 10.28 o -1 5 1 905.65 967.65 16.08 o 0 5 1 7.32 5.16 1.66 o 1 5 1 1218.68 1297.54 23.18 o 2 5 1 444.79 493.21 10.04 o 3 5 1 468.59 537.42 15.85 o 4 5 1 38.14 31.77 1.91 o 5 5 1 15.10 14.30 1.96 o 6 5 1 139.60 127.06 2.42 o 7 5 1 242.53 231.26 3.10 o 8 5 1 168.72 169.69 1.95 o 9 5 1 494.96 429.74 5.74 o 10 5 1 288.09 276.28 3.77 o 11 5 1 96.56 97.17 1.56 o 12 5 1 135.98 120.34 3.37 o 13 5 1 758.56 782.60 13.74 o 14 5 1 52.88 48.06 3.51 o -14 6 1 110.11 80.33 7.82 o -13 6 1 13.96 12.01 1.49 o -12 6 1 99.93 98.12 2.17 o -11 6 1 252.51 224.58 3.16 o -10 6 1 172.84 175.54 2.40 o -9 6 1 12.34 7.30 0.78 o -8 6 1 272.73 291.74 3.86 o -7 6 1 1591.75 1566.36 15.65 o -6 6 1 131.13 122.28 2.30 o -5 6 1 257.06 243.30 3.62 o -4 6 1 24.11 35.16 3.69 o -3 6 1 1723.92 1871.38 54.29 o -2 6 1 280.24 313.81 12.61 o -1 6 1 42.55 41.11 3.14 o 0 6 1 434.77 432.72 7.41 o 1 6 1 102.81 90.13 3.53 o 2 6 1 429.83 451.83 12.45 o 3 6 1 29.62 30.79 2.12 o 4 6 1 4.82 5.91 1.63 o 5 6 1 0.30 0.57 0.66 o 6 6 1 507.52 512.32 6.12 o 7 6 1 123.49 124.14 2.50 o 8 6 1 288.80 233.62 2.95 o 9 6 1 25.06 27.09 0.94 o 10 6 1 54.50 58.66 1.26 o 11 6 1 216.98 221.48 3.17 o 12 6 1 15.65 15.75 1.16 o 13 6 1 0.73 1.56 0.78 o -13 7 1 39.57 38.20 1.57 o -12 7 1 3.80 7.47 0.86 o -11 7 1 11.70 8.58 0.87 o -10 7 1 44.56 34.85 1.24 o -9 7 1 15.24 17.01 1.06 o -8 7 1 31.85 34.41 1.45 o -7 7 1 430.22 434.25 5.74 o -6 7 1 80.93 87.53 3.79 o -5 7 1 372.43 384.33 7.14 o -4 7 1 344.05 334.00 5.30 o -3 7 1 294.55 293.93 4.68 o -2 7 1 390.72 393.08 7.59 o -1 7 1 643.58 592.00 19.88 o 0 7 1 397.63 356.78 15.71 o 1 7 1 3.36 3.89 0.79 o 2 7 1 174.62 166.16 3.42 o 3 7 1 2624.02 2727.15 38.80 o 4 7 1 583.61 558.65 10.52 o 5 7 1 134.55 114.59 3.02 o 6 7 1 77.98 82.47 1.98 o 7 7 1 4.74 4.62 0.82 o 8 7 1 9.05 5.77 0.90 o 9 7 1 0.81 2.16 0.71 o 10 7 1 5.97 4.51 0.77 o 11 7 1 91.24 104.33 3.27 o 12 7 1 46.02 36.27 1.62 o 13 7 1 110.94 111.66 2.63 o -12 8 1 113.71 110.73 4.79 o -11 8 1 30.43 23.57 1.14 o -10 8 1 59.20 44.78 1.21 o -9 8 1 19.78 22.51 1.18 o -8 8 1 34.93 35.04 1.71 o -7 8 1 152.62 147.05 3.47 o -6 8 1 6.52 5.19 0.85 o -5 8 1 106.40 95.95 2.82 o -4 8 1 169.09 145.69 3.03 o -3 8 1 68.14 71.01 1.83 o -2 8 1 22.24 31.78 1.28 o -1 8 1 218.63 262.78 4.43 o 0 8 1 51.54 45.79 2.30 o 1 8 1 227.79 186.51 3.65 o 2 8 1 122.69 112.91 2.59 o 3 8 1 342.90 306.53 5.65 o 4 8 1 518.49 538.99 9.86 o 5 8 1 28.04 24.96 1.16 o 6 8 1 88.47 84.72 2.38 o 7 8 1 15.67 23.49 1.27 o 8 8 1 2.45 3.14 0.98 o 9 8 1 1.96 2.38 0.79 o 10 8 1 167.47 167.66 3.52 o 11 8 1 37.89 39.72 3.35 o 12 8 1 117.53 120.60 2.93 o -11 9 1 160.88 168.28 4.28 o -10 9 1 7.30 7.37 0.96 o -9 9 1 138.50 141.48 2.59 o -8 9 1 1.93 3.13 1.25 o -7 9 1 13.71 17.81 1.54 o -6 9 1 296.03 309.58 5.11 o -5 9 1 439.65 415.49 11.33 o -4 9 1 95.83 98.57 2.95 o -3 9 1 18.01 18.72 1.16 o -2 9 1 43.74 41.09 1.52 o -1 9 1 10.52 7.15 1.08 o 0 9 1 107.46 101.94 2.72 o 1 9 1 1086.34 1125.84 14.18 o 2 9 1 784.36 856.21 11.52 o 3 9 1 63.88 51.82 1.62 o 4 9 1 629.49 584.84 12.87 o 5 9 1 6.18 6.24 1.04 o 6 9 1 118.34 112.37 2.99 o 7 9 1 18.92 19.55 1.42 o 8 9 1 1.94 2.31 1.04 o 9 9 1 27.96 24.16 1.15 o 10 9 1 131.74 148.55 4.19 o 11 9 1 48.00 39.42 2.83 o -10 10 1 15.97 15.91 1.53 o -9 10 1 1.67 1.76 0.81 o -8 10 1 427.75 436.79 13.28 o -7 10 1 185.40 199.19 5.56 o -6 10 1 290.33 315.56 5.40 o -5 10 1 0.11 1.87 1.03 o -4 10 1 24.44 15.23 1.01 o -3 10 1 50.80 47.89 1.68 o -2 10 1 165.05 165.22 3.42 o -1 10 1 56.71 54.39 1.86 o 0 10 1 71.77 62.16 2.01 o 1 10 1 2.39 3.46 1.07 o 2 10 1 102.13 90.32 2.14 o 3 10 1 343.06 369.82 5.48 o 4 10 1 132.07 127.46 3.53 o 5 10 1 62.21 55.12 2.86 o 6 10 1 185.81 181.30 3.38 o 7 10 1 0.27 -0.29 1.19 o 8 10 1 154.33 183.46 4.16 o 9 10 1 20.11 19.36 1.21 o 10 10 1 0.61 1.44 0.79 o -9 11 1 6.50 6.48 0.95 o -8 11 1 249.84 264.05 5.50 o -7 11 1 102.37 109.24 2.73 o -6 11 1 34.00 38.56 2.36 o -5 11 1 156.15 150.77 4.51 o -4 11 1 150.02 158.19 6.27 o -3 11 1 144.06 135.35 5.51 o -2 11 1 3.78 5.89 1.15 o -1 11 1 594.62 612.78 9.25 o 0 11 1 88.40 84.00 2.61 o 1 11 1 245.58 263.55 4.88 o 2 11 1 22.42 16.66 1.68 o 3 11 1 73.88 72.46 2.73 o 4 11 1 30.48 29.53 1.46 o 5 11 1 22.11 21.50 1.36 o 6 11 1 185.49 199.95 5.24 o 7 11 1 33.57 41.63 1.92 o 8 11 1 8.87 5.75 0.99 o 9 11 1 57.45 51.79 2.43 o -7 12 1 0.04 0.26 0.82 o -6 12 1 107.87 112.91 4.41 o -5 12 1 86.05 74.57 2.80 o -4 12 1 38.65 39.02 2.05 o -3 12 1 522.47 630.74 14.48 o -2 12 1 260.33 294.34 6.75 o -1 12 1 125.95 139.26 3.64 o 0 12 1 67.06 63.46 2.50 o 1 12 1 11.63 10.98 1.49 o 2 12 1 53.74 46.12 1.87 o 3 12 1 28.25 27.25 1.70 o 4 12 1 19.96 24.23 1.77 o 5 12 1 15.64 19.05 1.49 o 6 12 1 25.75 30.98 2.01 o 7 12 1 114.58 111.34 3.81 o -5 13 1 46.62 40.29 3.13 o -4 13 1 57.53 62.12 3.55 o -3 13 1 90.63 95.89 2.84 o -2 13 1 71.87 73.94 4.01 o -1 13 1 31.68 34.18 2.23 o 0 13 1 2.02 2.65 1.14 o 1 13 1 37.40 36.65 2.12 o 2 13 1 27.11 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11.03 o -6 5 14 3.78 2.46 0.76 o -5 5 14 146.97 145.28 2.32 o -4 5 14 674.89 601.84 6.04 o -3 5 14 287.16 282.46 4.08 o -2 5 14 73.88 71.73 2.13 o -1 5 14 0.00 2.79 0.83 o 0 5 14 91.76 84.02 1.85 o 1 5 14 403.84 354.99 5.25 o 2 5 14 66.25 70.19 1.64 o 3 5 14 803.92 785.08 15.29 o 4 5 14 28.95 26.97 0.91 o 5 5 14 261.21 280.36 6.13 o 6 5 14 34.07 38.30 1.44 o 7 5 14 10.29 10.14 1.06 o 8 5 14 266.99 279.00 6.19 o 9 5 14 1.16 2.89 0.60 o 10 5 14 78.96 74.08 3.93 o -12 6 14 3.53 3.57 0.91 o -11 6 14 165.25 187.74 4.14 o -10 6 14 25.15 19.18 0.97 o -9 6 14 393.85 396.00 4.66 o -8 6 14 198.89 217.20 3.28 o -7 6 14 149.79 116.45 2.12 o -6 6 14 455.25 421.33 5.51 o -5 6 14 82.05 67.55 1.68 o -4 6 14 798.14 813.69 8.67 o -3 6 14 515.71 544.41 8.87 o -2 6 14 17.09 21.10 1.25 o -1 6 14 245.49 249.57 4.60 o 0 6 14 365.08 354.32 5.18 o 1 6 14 241.81 244.45 4.44 o 2 6 14 0.00 0.84 0.81 o 3 6 14 3.73 5.78 0.85 o 4 6 14 3.49 5.47 0.74 o 5 6 14 290.27 293.28 4.23 o 6 6 14 44.46 43.48 1.36 o 7 6 14 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39.06 47.13 1.67 o -12 2 15 237.60 254.76 4.01 o -11 2 15 168.10 154.22 4.83 o -10 2 15 97.81 86.23 2.50 o -9 2 15 7.85 1.34 0.83 o -8 2 15 249.98 232.34 3.72 o -7 2 15 18.68 13.29 1.00 o -6 2 15 788.32 778.84 10.71 o -5 2 15 3363.56 3311.20 28.42 o -4 2 15 60.03 65.08 1.43 o -3 2 15 643.97 602.42 8.22 o -2 2 15 346.88 309.70 5.82 o -1 2 15 529.01 495.54 7.45 o 0 2 15 2.46 1.97 0.82 o 1 2 15 543.64 559.93 7.56 o 2 2 15 691.21 684.16 18.63 o 3 2 15 61.14 50.65 1.27 o 4 2 15 197.52 201.47 2.72 o 5 2 15 621.49 607.02 6.75 o 6 2 15 193.84 193.27 3.10 o 7 2 15 319.43 306.43 7.67 o 8 2 15 363.56 371.42 7.27 o 9 2 15 5.08 4.06 0.58 o 10 2 15 203.49 209.98 3.33 o 11 2 15 6.57 5.79 0.66 o -13 3 15 29.91 33.75 1.48 o -12 3 15 5.46 10.11 0.99 o -11 3 15 169.46 176.72 6.07 o -10 3 15 101.61 105.67 2.17 o -9 3 15 59.50 43.70 1.55 o -8 3 15 158.94 182.17 3.52 o -7 3 15 950.25 910.09 8.70 o -6 3 15 209.87 175.40 2.39 o -5 3 15 31.98 34.97 1.47 o -4 3 15 0.02 0.99 0.84 o -3 3 15 2459.66 2455.43 28.22 o -2 3 15 479.38 441.97 8.91 o -1 3 15 1949.87 1939.72 19.32 o 0 3 15 342.84 362.11 5.05 o 1 3 15 379.71 389.60 5.27 o 2 3 15 1086.85 1123.60 31.55 o 3 3 15 4.84 5.96 0.72 o 4 3 15 499.08 537.48 8.94 o 5 3 15 755.54 731.78 10.71 o 6 3 15 770.96 830.68 11.15 o 7 3 15 2006.89 1995.98 56.11 o 8 3 15 154.82 157.82 3.57 o 9 3 15 96.83 101.22 2.83 o 10 3 15 102.12 105.37 4.38 o -13 4 15 0.06 0.10 0.81 o -12 4 15 24.91 25.23 1.00 o -11 4 15 248.88 240.31 3.12 o -10 4 15 47.19 41.57 1.36 o -9 4 15 0.27 0.87 0.70 o -8 4 15 550.95 525.34 15.41 o -7 4 15 369.07 388.05 4.36 o -6 4 15 97.28 89.84 1.64 o -5 4 15 1314.16 1202.11 16.32 o -4 4 15 354.32 321.95 3.65 o -3 4 15 359.66 361.31 4.86 o -2 4 15 647.51 604.17 7.42 o -1 4 15 16.31 12.09 1.04 o 0 4 15 1469.81 1339.19 13.92 o 1 4 15 691.58 640.18 7.32 o 2 4 15 213.78 232.44 3.37 o 3 4 15 74.31 104.63 2.12 o 4 4 15 1162.23 1175.17 18.12 o 5 4 15 137.80 144.39 4.46 o 6 4 15 0.71 2.99 0.79 o 7 4 15 15.88 17.89 0.85 o 8 4 15 28.64 23.73 0.88 o 9 4 15 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