Crystallography Open Database

Information card for entry 2022751

2022750 << 2022751 >> 2022752

Preview

Structure parameters

Chemical name	Bis(isoselenocyanato-κ<i>N</i>)tetrakis(pyridine-κ<i>N</i>)manganese(II)
Formula	C22 H20 Mn N6 Se2
Calculated formula	C22 H20 Mn N6 Se2
Title of publication	Synthesis, crystal structure and thermal decomposition pathway of bis-(iso-seleno-cyanato-κ<i>N</i>)tetra-kis-(pyridine-κ<i>N</i>)manganese(II).
Authors of publication	Näther, Christian; Mangelsen, Sebastian; Boeckmann, Jan
Journal of publication	Acta crystallographica. Section E, Crystallographic communications
Year of publication	2023
Journal volume	79
Journal issue	Pt 5
Pages of publication	482 - 487
a	12.5335 ± 0.0009 Å
b	13.4331 ± 0.0008 Å
c	15.13 ± 0.0012 Å
α	90°
β	108.608 ± 0.008°
γ	90°
Cell volume	2414.2 ± 0.3 Å³
Cell temperature	170 ± 2 K
Ambient diffraction temperature	170 ± 2 K
Number of distinct elements	5
Space group number	15
Hermann-Mauguin space group symbol	C 1 2/c 1
Hall space group symbol	-C 2yc
Residual factor for all reflections	0.0568
Residual factor for significantly intense reflections	0.0425
Weighted residual factors for significantly intense reflections	0.0831
Weighted residual factors for all reflections included in the refinement	0.0881
Goodness-of-fit parameter for all reflections included in the refinement	1.028
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	Yes

Version history

Revision	Date	Message	Files
284382 (current)	2023-06-06	cif/ Updating files of 2022751 Original log message: Adding full bibliography for 2022751.cif.	2022751.cif 2022751.hkl
282796	2023-04-22	cif/ hkl/ Adding structures of 2022751 via cif-deposit CGI script.	2022751.cif 2022751.hkl