#------------------------------------------------------------------------------
#$Date: 2023-10-11 05:11:06 +0300 (Wed, 11 Oct 2023) $
#$Revision: 286890 $
#$URL: file:///home/coder/svn-repositories/cod/hkl/2/02/29/2022908.hkl $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/. The original data for this entry
# were provided by IUCr Journals, http://journals.iucr.org/.
#
# The file may be used within the scientific community so long as
# proper attribution is given to the journal article from which the
# data were obtained.
#
data_2022908
_cell_angle_alpha                90.000
_cell_angle_beta                 90.000
_cell_angle_gamma                120.000
_cell_length_a                   9.1318
_cell_length_b                   9.1318
_cell_length_c                   17.1558
_exptl_crystal_F_000             1398.00
_reflns_d_resolution_high        0.6000
_cod_data_source_file            wm5695Isup2.hkl
_cod_data_source_block           I
_shelx_title                     ' Cs2GdNb6Cl15O3(P-31c)'
_shelx_refln_list_code           4
_shelx_f_calc_maximum            513.05
_shelx_f_squared_multiplier      1.000
loop_
_space_group_symop_operation_xyz
'x, y, z'
'-y, x-y, z'
'-x+y, -x, z'
'y, x, z+1/2'
'-x, -x+y, z+1/2'
'x-y, -y, z+1/2'
'-x, -y, -z'
'y, -x+y, -z'
'x-y, x, -z'
'-y, -x, -z-1/2'
'x, x-y, -z-1/2'
'-x+y, y, -z-1/2'
loop_
_refln_index_h
_refln_index_k
_refln_index_l
_refln_F_squared_calc
_refln_F_squared_meas
_refln_F_squared_sigma
_refln_observed_status
0 1 0 13531.93 13122.25 227.45 o
-1 2 0 50814.53 51890.32 889.00 o
0 2 0 43027.62 42484.91 618.34 o
-1 3 0 102241.12 105484.76 1354.35 o
0 3 0 6795.39 6676.80 99.35 o
-2 4 0 10402.41 10305.20 146.79 o
-1 4 0 37555.88 36836.78 364.29 o
0 4 0 4610.19 4343.97 65.55 o
-2 5 0 44282.22 43499.52 405.55 o
-1 5 0 186158.38 198343.67 2789.92 o
0 5 0 82119.21 83814.09 1932.40 o
-3 6 0 11017.82 10420.58 160.27 o
-2 6 0 23838.18 23207.81 242.13 o
-1 6 0 8609.16 8451.23 84.13 o
0 6 0 101790.34 104851.72 1450.06 o
-3 7 0 26647.22 26531.52 301.43 o
-2 7 0 11844.82 11673.38 131.46 o
-1 7 0 972.33 945.38 13.63 o
0 7 0 24770.13 24886.72 407.39 o
-4 8 0 4585.40 4520.16 93.11 o
-3 8 0 33386.50 33711.54 401.77 o
-2 8 0 24740.10 25039.71 317.89 o
-1 8 0 3289.73 3168.00 42.72 o
0 8 0 24490.46 25627.69 480.74 o
-4 9 0 1367.40 1279.64 42.38 o
-3 9 0 17111.27 17289.46 243.60 o
-2 9 0 26539.39 27427.37 391.67 o
-1 9 0 7440.58 7704.02 120.05 o
0 9 0 21806.32 22827.46 562.67 o
-5 10 0 78594.43 84982.58 2022.58 o
-4 10 0 996.13 994.22 35.84 o
-3 10 0 9488.20 9685.21 179.72 o
-2 10 0 6787.43 6973.58 145.01 o
-1 10 0 73.09 71.10 13.50 o
0 10 0 12510.58 13082.60 579.64 o
-5 11 0 3187.70 3327.41 85.22 o
-4 11 0 10854.32 11202.36 261.16 o
-3 11 0 2149.83 2130.06 66.36 o
-2 11 0 3796.00 3814.26 118.59 o
-1 11 0 24419.11 25739.88 850.59 o
0 11 0 865.99 918.45 97.72 o
-6 12 0 13891.58 15137.20 477.50 o
-5 12 0 5030.54 5265.66 139.75 o
-4 12 0 6894.08 7248.28 177.99 o
-3 12 0 447.18 443.72 35.79 o
-2 12 0 751.08 652.84 53.42 o
-1 12 0 449.99 295.29 57.62 o
0 12 0 2754.84 2337.22 259.74 o
-6 13 0 6782.45 7037.97 259.62 o
-5 13 0 425.33 354.58 36.53 o
-4 13 0 5589.52 5598.50 241.86 o
-3 13 0 3475.96 3337.73 170.30 o
-2 13 0 2376.97 2358.18 162.21 o
-1 13 0 4910.38 4963.40 309.12 o
0 13 0 3881.18 3617.65 409.44 o
-7 14 0 1091.00 891.52 133.83 o
-6 14 0 3235.50 3155.89 146.37 o
-5 14 0 43.67 64.32 38.28 o
-4 14 0 6670.27 7469.68 583.88 o
-3 14 0 2223.29 2157.11 131.00 o
-2 14 0 2962.94 2887.59 216.39 o
-7 15 0 997.48 733.05 68.25 o
-6 15 0 4546.03 4154.05 336.36 o
0 1 1 4651.76 4555.31 49.33 o
0 2 1 947.18 886.34 10.43 o
1 2 1 8068.54 7759.90 81.47 o
-1 3 1 181.86 237.75 4.69 o
0 3 1 20129.00 18839.12 191.39 o
1 3 1 2644.48 2551.31 29.05 o
2 3 1 1882.95 1858.01 25.80 o
-1 4 1 3110.17 2981.87 30.93 o
0 4 1 8963.67 8587.39 88.48 o
1 4 1 5789.13 5631.88 57.22 o
2 4 1 1029.78 1006.86 13.32 o
3 4 1 703.46 716.73 15.44 o
-2 5 1 2620.85 2557.04 32.62 o
-1 5 1 14970.37 14575.53 140.62 o
0 5 1 1826.85 1830.89 23.24 o
1 5 1 2853.90 2731.03 36.57 o
2 5 1 1965.22 1961.69 23.73 o
3 5 1 18500.65 18512.04 236.47 o
4 5 1 391.27 436.21 17.54 o
-2 6 1 4866.13 4720.11 57.12 o
-1 6 1 766.62 705.95 12.20 o
0 6 1 0.45 37.33 5.45 o
1 6 1 138.28 145.19 6.53 o
2 6 1 397.32 377.55 11.76 o
3 6 1 5927.73 6005.34 93.47 o
4 6 1 9060.32 9196.75 171.67 o
5 6 1 1381.96 1436.39 53.24 o
-3 7 1 1847.60 1795.35 30.63 o
-2 7 1 4496.23 4396.47 56.82 o
-1 7 1 8775.53 8674.69 97.80 o
0 7 1 3121.26 3172.73 41.56 o
1 7 1 3851.14 3940.18 55.22 o
2 7 1 5714.32 5748.87 91.28 o
3 7 1 178.34 197.97 20.29 o
4 7 1 2569.67 2632.44 70.74 o
5 7 1 79.38 77.60 23.52 o
6 7 1 7229.69 7399.76 245.53 o
-3 8 1 6716.41 6910.89 100.06 o
-2 8 1 173.94 190.06 10.41 o
-1 8 1 2709.15 2696.78 36.67 o
0 8 1 8128.35 8354.99 103.37 o
1 8 1 6966.36 7217.89 119.45 o
2 8 1 1017.03 1024.67 33.97 o
3 8 1 4208.26 4323.18 114.13 o
4 8 1 3959.43 4107.55 123.35 o
5 8 1 3744.93 3796.79 135.94 o
6 8 1 1449.24 1394.09 75.80 o
7 8 1 2244.47 1738.73 109.14 o
-4 9 1 1263.50 1219.94 39.64 o
-3 9 1 774.59 704.57 23.81 o
-2 9 1 4424.15 4501.68 72.18 o
-1 9 1 2041.43 2119.86 41.95 o
0 9 1 256.91 244.16 14.36 o
1 9 1 2429.70 2501.65 83.28 o
2 9 1 2969.94 2966.34 89.47 o
3 9 1 128.36 89.27 22.52 o
4 9 1 210.43 215.57 37.40 o
5 9 1 4611.26 4491.52 222.88 o
6 9 1 4840.20 4349.54 217.43 o
-4 10 1 203.94 207.96 19.70 o
-3 10 1 2629.63 2667.22 63.08 o
-2 10 1 3061.38 3147.72 76.96 o
-1 10 1 2519.12 2514.32 69.68 o
0 10 1 809.10 810.79 50.02 o
1 10 1 256.31 261.00 32.85 o
2 10 1 1042.68 955.92 62.54 o
3 10 1 1467.42 1449.44 96.01 o
4 10 1 533.76 457.89 69.67 o
-5 11 1 1642.28 1666.14 55.56 o
-4 11 1 231.77 198.38 24.02 o
-3 11 1 678.20 642.58 33.38 o
-2 11 1 447.47 399.11 32.40 o
-1 11 1 1028.55 1061.64 52.44 o
0 11 1 4433.34 4539.35 173.04 o
1 11 1 1253.23 1050.16 82.36 o
2 11 1 1011.26 920.49 84.88 o
3 11 1 4905.10 4827.38 263.38 o
-5 12 1 1184.08 1204.10 49.43 o
-4 12 1 2730.04 2825.39 107.23 o
-3 12 1 808.84 689.36 44.85 o
-2 12 1 11352.34 12145.05 418.35 o
-1 12 1 170.14 84.44 39.79 o
0 12 1 1120.48 863.10 109.46 o
1 12 1 333.46 196.89 63.73 o
2 12 1 119.64 123.52 68.23 o
-6 13 1 3392.31 3276.81 121.97 o
-5 13 1 5018.80 5295.21 159.87 o
-4 13 1 113.69 94.21 32.23 o
-3 13 1 67.53 113.34 48.02 o
-2 13 1 317.95 269.53 56.67 o
-1 13 1 11.19 -20.79 63.86 o
0 13 1 8387.12 8884.28 484.02 o
-6 14 1 790.27 615.06 49.45 o
-5 14 1 2103.95 2091.50 134.59 o
-4 14 1 7.25 39.16 43.63 o
-3 14 1 161.06 133.90 58.57 o
-2 14 1 8.38 18.20 71.69 o
-7 15 1 147.00 174.83 64.88 o
-6 15 1 132.13 117.21 67.33 o
0 0 2 78246.07 68327.27 2503.05 o
0 1 2 19359.95 19017.47 216.15 o
1 1 2 4251.91 4059.57 67.62 o
-1 2 2 26604.08 25243.95 406.06 o
0 2 2 3565.02 3480.19 38.39 o
1 2 2 1465.11 1384.42 15.70 o
2 2 2 9551.82 9247.58 130.23 o
-1 3 2 751.81 482.61 6.87 o
0 3 2 18435.15 17774.08 180.68 o
1 3 2 7798.01 7404.40 77.43 o
2 3 2 145.03 193.07 4.92 o
3 3 2 2529.85 2529.93 56.73 o
-2 4 2 53256.86 50735.27 846.79 o
-1 4 2 31280.15 30126.50 313.41 o
0 4 2 3102.92 2903.49 33.14 o
1 4 2 344.40 345.58 7.58 o
2 4 2 322.86 284.22 10.40 o
3 4 2 18454.69 18754.94 191.13 o
4 4 2 8388.46 8432.18 152.59 o
-2 5 2 6757.76 6642.64 79.09 o
-1 5 2 1932.80 1890.73 22.62 o
0 5 2 36881.38 36860.80 369.81 o
1 5 2 3956.62 3904.46 43.93 o
2 5 2 6711.03 6435.63 69.26 o
3 5 2 18379.59 18734.97 218.92 o
4 5 2 202.98 219.72 14.50 o
5 5 2 3649.22 3751.90 108.99 o
-3 6 2 1297.14 1322.34 34.34 o
-2 6 2 25.05 30.45 6.06 o
-1 6 2 11590.29 11515.67 117.54 o
0 6 2 6954.89 7114.18 75.00 o
1 6 2 688.36 720.27 14.20 o
2 6 2 2373.72 2337.11 41.16 o
3 6 2 161.83 197.57 14.85 o
4 6 2 5655.97 5904.93 112.86 o
5 6 2 3772.59 3945.35 117.99 o
6 6 2 281.65 294.53 123.48 o
-3 7 2 5382.17 5172.01 76.27 o
-2 7 2 896.15 896.12 16.25 o
-1 7 2 2269.41 2272.79 28.30 o
0 7 2 43.57 74.53 7.81 o
1 7 2 52.54 77.37 8.07 o
2 7 2 2752.82 2739.92 48.35 o
3 7 2 1168.22 1100.58 33.50 o
4 7 2 2020.94 2074.44 64.37 o
5 7 2 2242.89 2358.27 77.97 o
6 7 2 29.07 28.07 32.49 o
7 7 2 379.83 273.43 64.24 o
-4 8 2 1015.75 884.84 34.27 o
-3 8 2 567.65 602.48 19.81 o
-2 8 2 2459.73 2490.79 39.50 o
-1 8 2 3317.77 3470.84 63.02 o
0 8 2 4579.42 4707.60 68.75 o
1 8 2 7.46 18.02 6.81 o
2 8 2 1737.58 1868.47 47.82 o
3 8 2 189.21 169.81 23.60 o
4 8 2 6273.40 6814.27 193.08 o
5 8 2 1548.92 1370.14 64.90 o
6 8 2 364.32 274.79 39.39 o
7 8 2 1867.01 1555.13 109.00 o
-4 9 2 108.66 125.58 17.33 o
-3 9 2 7741.91 7753.11 137.92 o
-2 9 2 15424.98 16144.11 259.04 o
-1 9 2 11473.88 11682.97 184.28 o
0 9 2 104.16 90.13 20.57 o
1 9 2 1316.33 1268.57 42.77 o
2 9 2 391.80 356.21 27.63 o
3 9 2 3893.97 4068.01 122.94 o
4 9 2 5901.02 6462.95 230.69 o
5 9 2 30.58 97.18 46.12 o
6 9 2 1613.83 1386.90 99.54 o
-5 10 2 15308.15 15856.56 486.58 o
-4 10 2 184.57 194.21 19.49 o
-3 10 2 1911.99 1992.85 50.90 o
-2 10 2 6010.01 6222.11 131.14 o
-1 10 2 271.75 225.18 31.19 o
0 10 2 3431.03 3536.57 101.44 o
1 10 2 139.34 156.30 30.57 o
2 10 2 2512.26 2515.36 124.04 o
3 10 2 4381.85 4715.22 304.13 o
4 10 2 8.47 -20.20 53.90 o
-5 11 2 2242.17 2382.08 64.94 o
-4 11 2 426.42 370.02 28.66 o
-3 11 2 118.34 89.36 21.11 o
-2 11 2 133.17 111.61 37.17 o
-1 11 2 6812.44 7309.71 212.65 o
0 11 2 2123.04 2046.83 110.27 o
1 11 2 1137.47 893.81 79.23 o
2 11 2 18.89 -53.66 53.66 o
3 11 2 120.16 118.85 66.98 o
-6 12 2 6220.07 6132.43 253.63 o
-5 12 2 2018.27 1947.01 67.24 o
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-2 12 2 3093.82 3233.20 173.54 o
-1 12 2 674.15 586.58 65.46 o
0 12 2 167.50 145.66 53.78 o
1 12 2 572.76 537.32 80.01 o
2 12 2 43.17 71.58 77.86 o
-6 13 2 1129.03 1048.69 54.50 o
-5 13 2 493.83 432.01 37.50 o
-4 13 2 18.43 24.20 28.29 o
-3 13 2 37.88 21.19 39.13 o
-2 13 2 336.04 246.14 51.85 o
-1 13 2 549.37 438.01 91.11 o
0 13 2 1935.61 1728.60 139.12 o
-7 14 2 3243.93 2985.62 259.36 o
-6 14 2 3136.27 3030.60 124.15 o
-5 14 2 292.07 237.22 45.81 o
-4 14 2 337.63 262.38 53.04 o
-3 14 2 3084.39 2782.50 204.59 o
-2 14 2 3363.62 2741.18 225.24 o
-7 15 2 2041.82 1566.87 100.10 o
-6 15 2 12.61 21.24 52.38 o
0 1 3 27375.05 26450.38 290.55 o
0 2 3 39733.61 38904.75 436.66 o
1 2 3 104001.99 105574.50 1242.97 o
-1 3 3 57970.99 56994.53 667.11 o
0 3 3 1027.67 983.56 13.42 o
1 3 3 22939.81 22267.31 215.81 o
2 3 3 13823.68 13832.52 137.96 o
-1 4 3 30506.76 29646.44 285.54 o
0 4 3 23685.17 23083.67 224.98 o
1 4 3 13377.81 13094.66 130.69 o
2 4 3 8730.73 8541.65 88.08 o
3 4 3 18813.39 18966.34 205.21 o
-2 5 3 8983.94 8822.50 94.02 o
-1 5 3 7189.15 6989.40 71.64 o
0 5 3 21413.39 21100.47 228.90 o
1 5 3 35680.70 35903.10 379.30 o
2 5 3 324.37 330.15 14.60 o
3 5 3 39683.32 40572.83 455.09 o
4 5 3 4251.66 4204.95 71.13 o
-2 6 3 54924.77 55384.91 575.13 o
-1 6 3 13240.97 13115.16 139.84 o
0 6 3 1909.10 1855.34 27.11 o
1 6 3 3231.78 3197.49 38.91 o
2 6 3 4586.53 4541.86 58.55 o
3 6 3 2883.39 2998.39 51.16 o
4 6 3 21276.75 21874.73 387.16 o
5 6 3 895.33 900.78 34.65 o
-3 7 3 2807.07 2752.89 43.58 o
-2 7 3 3847.37 3846.77 72.51 o
-1 7 3 26433.21 26755.84 286.44 o
0 7 3 44672.19 45911.21 519.18 o
1 7 3 1333.87 1363.03 30.22 o
2 7 3 8952.90 9433.28 117.02 o
3 7 3 166.46 161.85 14.85 o
4 7 3 2830.05 2841.43 74.51 o
5 7 3 2788.15 2825.00 89.45 o
6 7 3 4688.62 5047.28 160.20 o
-3 8 3 29029.16 29086.58 403.75 o
-2 8 3 2237.49 2139.89 32.69 o
-1 8 3 594.68 564.66 15.42 o
0 8 3 1564.67 1580.55 29.27 o
1 8 3 9466.80 9588.09 134.83 o
2 8 3 2.14 35.32 12.11 o
3 8 3 9574.63 10133.69 261.82 o
4 8 3 8216.67 8917.94 242.31 o
5 8 3 1671.79 1553.07 73.26 o
6 8 3 158.57 177.56 40.24 o
7 8 3 4463.85 3882.16 199.88 o
-4 9 3 15206.75 15204.48 244.36 o
-3 9 3 4027.98 4086.27 79.78 o
-2 9 3 4731.76 4678.38 90.08 o
-1 9 3 3620.53 3715.30 64.44 o
0 9 3 1817.43 1766.86 38.90 o
1 9 3 1154.66 1103.98 34.45 o
2 9 3 17446.30 18815.89 439.17 o
3 9 3 128.33 113.38 27.95 o
4 9 3 4902.20 5166.35 181.42 o
5 9 3 4078.78 4328.51 192.81 o
6 9 3 1013.51 798.85 79.24 o
-4 10 3 414.48 397.38 22.59 o
-3 10 3 14499.20 15509.81 288.64 o
-2 10 3 5069.72 5188.95 129.43 o
-1 10 3 20925.79 22202.87 407.50 o
0 10 3 4495.80 4664.75 134.05 o
1 10 3 2236.51 2220.44 91.95 o
2 10 3 147.46 139.22 34.14 o
3 10 3 120.98 31.87 64.36 o
4 10 3 19.20 67.30 53.58 o
-5 11 3 17559.99 18412.48 426.66 o
-4 11 3 4730.68 4807.13 125.61 o
-3 11 3 2906.32 2821.35 81.78 o
-2 11 3 176.48 172.06 25.51 o
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0 11 3 2182.64 2289.34 115.68 o
1 11 3 9182.88 9744.94 468.00 o
2 11 3 129.55 124.35 47.64 o
3 11 3 5886.72 5993.20 345.88 o
-5 12 3 364.97 355.59 35.65 o
-4 12 3 12893.75 14035.50 318.64 o
-3 12 3 4222.59 4697.40 122.63 o
-2 12 3 21163.73 23464.08 704.20 o
-1 12 3 138.82 77.32 58.91 o
0 12 3 2645.25 2676.86 254.78 o
1 12 3 203.96 199.62 73.76 o
-6 13 3 3742.61 3782.87 152.77 o
-5 13 3 5399.51 5567.20 177.11 o
-4 13 3 3024.49 2878.88 110.63 o
-3 13 3 292.20 122.63 40.50 o
-2 13 3 661.90 571.57 65.61 o
-1 13 3 1185.36 819.59 103.02 o
0 13 3 6289.02 6053.99 374.94 o
-6 14 3 5008.54 5082.66 203.10 o
-5 14 3 1649.93 1423.92 88.03 o
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0 0 4 98.46 150.71 17.15 o
0 1 4 16450.98 15015.01 167.88 o
1 1 4 155223.95 152977.95 4472.67 o
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0 2 4 36535.72 36250.36 391.10 o
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-1 3 4 79000.11 77247.57 1055.07 o
0 3 4 23402.71 22512.55 237.40 o
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2 3 4 1799.81 1852.81 21.98 o
3 3 4 296.32 270.16 36.02 o
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2 5 4 5442.25 5416.03 69.05 o
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0 6 4 9450.81 9420.08 101.19 o
1 6 4 34.10 50.92 8.91 o
2 6 4 21351.64 22240.67 267.91 o
3 6 4 16376.51 16504.10 210.32 o
4 6 4 1840.29 1712.58 48.63 o
5 6 4 6070.13 6170.73 131.10 o
6 6 4 7480.75 7750.26 329.15 o
-3 7 4 23535.42 23635.50 297.78 o
-2 7 4 19639.39 19705.56 214.54 o
-1 7 4 21530.67 21657.46 275.88 o
0 7 4 578.33 544.87 15.30 o
1 7 4 65756.29 69270.78 781.75 o
2 7 4 19603.21 20520.58 273.75 o
3 7 4 1039.92 1072.70 34.77 o
4 7 4 850.14 761.27 37.78 o
5 7 4 1314.06 1300.11 70.84 o
6 7 4 1466.93 1483.31 76.16 o
7 7 4 9513.01 10154.44 658.18 o
-4 8 4 54432.28 55221.29 1110.14 o
-3 8 4 647.12 631.33 21.30 o
-2 8 4 10912.69 11003.38 150.28 o
-1 8 4 232.30 272.26 19.18 o
0 8 4 2772.77 2732.48 44.68 o
1 8 4 501.07 486.10 16.51 o
2 8 4 8154.25 8403.36 153.84 o
3 8 4 6289.42 6343.47 140.60 o
4 8 4 10964.86 11493.07 271.83 o
5 8 4 873.53 665.02 50.90 o
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7 8 4 444.34 244.00 59.57 o
-4 9 4 5106.17 5042.19 94.88 o
-3 9 4 3528.81 3620.54 74.37 o
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0 9 4 7843.48 7983.37 145.82 o
1 9 4 1729.27 1619.95 47.57 o
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