#------------------------------------------------------------------------------ #$Date: 2023-10-27 05:06:30 +0300 (Fri, 27 Oct 2023) $ #$Revision: 287136 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/02/29/2022926.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2022926 _cell_angle_alpha 90.000 _cell_angle_beta 111.554 _cell_angle_gamma 90.000 _cell_length_a 12.7613 _cell_length_b 7.7054 _cell_length_c 13.4641 _exptl_crystal_F_000 620.00 _reflns_d_resolution_high 0.8141 _cod_data_source_file wm5701Isup2.hkl _cod_data_source_block I _shelx_title ' I' _shelx_refln_list_code 4 _shelx_f_calc_maximum 185.86 _shelx_f_squared_multiplier 1.000 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 2805.45 2706.16 43.83 o 4 0 0 11.62 5.56 1.87 o 6 0 0 2145.39 2046.90 40.89 o 8 0 0 338.80 366.17 11.78 o 10 0 0 994.47 975.78 79.15 o 12 0 0 21.13 41.31 5.58 o 14 0 0 278.25 285.74 16.64 o 1 1 0 13122.21 12509.89 158.80 o 2 1 0 7398.03 7507.87 78.08 o 3 1 0 43.72 44.40 1.62 o 4 1 0 400.76 347.65 6.41 o 5 1 0 2135.91 1856.53 39.91 o 6 1 0 532.66 551.54 11.36 o 7 1 0 1370.57 1371.14 26.65 o 8 1 0 16.26 7.72 1.45 o 9 1 0 111.11 115.22 5.87 o 10 1 0 61.62 54.90 3.35 o 11 1 0 308.01 273.42 12.05 o 12 1 0 3.91 6.00 2.52 o 13 1 0 18.37 19.24 4.42 o 14 1 0 81.52 78.60 4.34 o 0 2 0 857.68 767.31 14.26 o 1 2 0 3424.89 3300.12 46.86 o 2 2 0 234.78 259.69 6.68 o 3 2 0 170.93 146.58 3.73 o 4 2 0 5.70 2.27 1.04 o 5 2 0 254.95 257.21 9.10 o 6 2 0 380.40 332.64 12.65 o 7 2 0 74.57 71.62 3.76 o 8 2 0 27.33 26.25 2.17 o 9 2 0 432.29 409.13 9.97 o 10 2 0 251.03 263.41 11.77 o 11 2 0 559.41 553.05 20.27 o 12 2 0 0.31 4.69 2.82 o 13 2 0 2.65 1.04 2.12 o 14 2 0 24.36 24.74 2.53 o 1 3 0 1297.76 1251.66 32.40 o 2 3 0 1049.25 1002.92 27.33 o 3 3 0 4689.85 4670.09 67.13 o 4 3 0 213.75 178.95 6.57 o 5 3 0 117.48 98.11 6.07 o 6 3 0 10.79 10.43 2.28 o 7 3 0 682.09 607.16 15.71 o 8 3 0 29.62 35.80 3.25 o 9 3 0 28.40 20.82 3.08 o 10 3 0 5.23 4.06 2.15 o 11 3 0 21.27 24.26 3.81 o 12 3 0 228.16 245.85 12.84 o 13 3 0 205.72 206.09 10.23 o 0 4 0 4065.82 4663.54 183.79 o 1 4 0 224.61 218.61 9.40 o 2 4 0 3062.40 3158.74 64.81 o 3 4 0 1372.47 1369.49 33.06 o 4 4 0 1971.91 2021.60 45.86 o 5 4 0 0.19 0.35 1.27 o 6 4 0 353.85 342.51 10.02 o 7 4 0 648.75 661.88 22.27 o 8 4 0 1243.62 1165.60 28.90 o 9 4 0 237.05 244.17 17.28 o 10 4 0 0.39 2.51 2.22 o 11 4 0 1.61 1.46 2.00 o 12 4 0 367.18 417.79 17.32 o 13 4 0 2.78 2.36 1.41 o 1 5 0 188.02 209.26 17.89 o 2 5 0 113.39 124.11 6.11 o 3 5 0 819.48 782.04 18.66 o 4 5 0 210.91 206.94 8.35 o 5 5 0 11.63 12.16 1.86 o 6 5 0 7.41 3.57 1.37 o 7 5 0 1665.00 1839.80 35.95 o 8 5 0 336.03 347.74 17.76 o 9 5 0 10.09 8.56 2.65 o 10 5 0 19.06 10.67 2.83 o 11 5 0 79.24 78.62 6.50 o 12 5 0 19.68 15.65 2.21 o 0 6 0 154.66 121.83 35.77 o 1 6 0 789.40 814.91 19.45 o 2 6 0 0.51 1.35 1.94 o 3 6 0 16.36 14.31 3.59 o 4 6 0 131.84 118.82 6.43 o 5 6 0 26.91 33.37 5.49 o 6 6 0 409.10 444.78 28.18 o 7 6 0 13.64 8.13 3.37 o 8 6 0 55.15 69.74 6.11 o 9 6 0 89.61 90.32 6.50 o 10 6 0 44.96 47.36 3.58 o 11 6 0 0.45 2.77 1.28 o 1 7 0 1181.62 1222.54 38.89 o 2 7 0 83.33 83.44 8.23 o 3 7 0 47.88 38.83 4.46 o 4 7 0 10.83 8.51 2.73 o 5 7 0 39.36 40.87 4.20 o 6 7 0 108.52 104.22 6.29 o 7 7 0 3.79 4.48 1.74 o 8 7 0 134.46 138.82 9.70 o 9 7 0 75.62 93.61 4.81 o 0 8 0 404.33 444.35 22.53 o 1 8 0 47.52 43.47 4.30 o 2 8 0 3.35 4.36 1.82 o 3 8 0 19.67 16.31 3.16 o 4 8 0 314.98 357.06 19.22 o 5 8 0 0.27 0.88 1.59 o 6 8 0 163.28 145.82 5.66 o 7 8 0 120.73 115.25 4.52 o 1 9 0 26.52 26.57 3.55 o 2 9 0 31.42 30.51 2.96 o 3 9 0 8.75 5.87 1.40 o 4 9 0 44.44 36.14 2.80 o -13 0 1 607.25 570.10 22.17 o -11 0 1 1336.57 1251.76 58.78 o -9 0 1 423.26 414.87 11.44 o -7 0 1 1081.25 914.76 21.23 o -5 0 1 39.10 33.12 2.75 o -3 0 1 171.37 156.31 5.02 o -1 0 1 3272.43 3474.72 55.12 o 1 0 1 251.35 166.39 3.82 o 3 0 1 34545.20 33623.24 691.67 o 5 0 1 1266.82 1317.60 24.31 o 7 0 1 1.31 0.15 1.48 o 9 0 1 4.31 3.38 2.87 o 11 0 1 3.31 2.48 4.11 o 13 0 1 328.76 339.40 20.55 o -14 1 1 12.51 12.26 2.07 o -13 1 1 249.10 248.15 9.75 o -12 1 1 1484.37 1460.56 38.16 o -11 1 1 238.44 213.64 11.53 o -10 1 1 8.71 11.89 1.80 o -9 1 1 2.03 1.33 0.84 o -8 1 1 946.97 899.30 13.58 o -7 1 1 101.59 98.03 3.51 o -6 1 1 149.99 113.13 3.76 o -5 1 1 962.51 920.82 23.52 o -4 1 1 83.05 79.98 2.47 o -3 1 1 6713.58 6815.39 77.97 o -2 1 1 10922.03 10277.87 102.18 o -1 1 1 14.57 43.66 1.31 o 0 1 1 166.27 201.17 4.18 o 1 1 1 2355.22 2296.55 30.06 o 2 1 1 216.44 187.95 2.88 o 3 1 1 3796.23 3889.42 58.65 o 4 1 1 1279.13 1205.83 29.32 o 5 1 1 129.44 127.64 4.49 o 6 1 1 408.48 383.10 11.09 o 7 1 1 33.98 33.22 3.04 o 8 1 1 196.89 173.35 6.74 o 9 1 1 285.06 276.77 9.34 o 10 1 1 0.40 1.25 2.71 o 11 1 1 0.75 11.61 3.73 o 12 1 1 466.51 511.00 18.58 o 13 1 1 1.66 1.84 2.25 o 14 1 1 122.07 96.15 8.32 o -14 2 1 121.10 110.81 8.11 o -13 2 1 426.01 455.68 15.04 o -12 2 1 13.03 14.41 3.55 o -11 2 1 409.58 456.04 20.35 o -10 2 1 58.33 57.21 3.33 o -9 2 1 343.63 371.28 7.74 o -8 2 1 650.21 647.28 11.67 o -7 2 1 780.37 675.87 17.03 o -6 2 1 1387.66 1368.71 29.44 o -5 2 1 957.16 952.38 19.54 o -4 2 1 53.09 76.49 2.85 o -3 2 1 2320.51 2404.32 32.96 o -2 2 1 14.93 10.59 1.09 o -1 2 1 5529.95 5757.57 80.10 o 0 2 1 4661.44 4702.15 65.40 o 1 2 1 2114.20 2137.18 34.14 o 2 2 1 1174.46 1105.68 19.03 o 3 2 1 96.99 96.90 3.80 o 4 2 1 13.43 25.51 2.54 o 5 2 1 2390.53 2388.93 43.85 o 6 2 1 201.27 194.75 6.62 o 7 2 1 119.16 117.44 4.80 o 8 2 1 26.34 27.70 2.83 o 9 2 1 63.05 60.72 3.87 o 10 2 1 48.76 39.31 5.33 o 11 2 1 269.50 259.60 23.40 o 12 2 1 312.43 288.33 13.52 o 13 2 1 327.33 307.06 11.31 o -14 3 1 308.10 344.49 20.67 o -13 3 1 32.51 34.83 4.26 o -12 3 1 199.93 193.65 11.45 o -11 3 1 329.27 353.83 12.31 o -10 3 1 133.39 127.06 5.73 o -9 3 1 393.81 374.59 9.14 o -8 3 1 34.01 24.38 2.07 o -7 3 1 488.91 527.33 11.69 o -6 3 1 1434.78 1373.93 32.25 o -5 3 1 2238.67 2421.90 44.41 o -4 3 1 2250.64 2190.42 36.30 o -3 3 1 92.65 151.08 5.41 o -2 3 1 264.12 239.72 7.81 o -1 3 1 170.69 137.13 12.36 o 0 3 1 2581.75 2324.83 47.19 o 1 3 1 157.93 158.16 6.19 o 2 3 1 1540.14 1456.37 37.99 o 3 3 1 347.84 383.42 13.71 o 4 3 1 123.81 105.44 4.27 o 5 3 1 172.98 171.05 6.84 o 6 3 1 3821.54 3936.76 59.14 o 7 3 1 639.18 682.08 13.82 o 8 3 1 7.45 5.03 1.50 o 9 3 1 18.01 11.68 3.43 o 10 3 1 71.77 57.62 6.95 o 11 3 1 288.13 319.75 12.94 o 12 3 1 195.22 180.50 11.73 o 13 3 1 0.54 2.17 1.55 o -13 4 1 45.43 60.14 5.20 o -12 4 1 60.18 55.75 4.67 o -11 4 1 108.98 105.85 7.06 o -10 4 1 56.88 60.06 3.99 o -9 4 1 170.89 167.59 6.80 o -8 4 1 30.33 30.47 2.86 o -7 4 1 85.25 88.41 5.12 o -6 4 1 0.32 0.85 1.18 o -5 4 1 3062.78 3270.59 50.32 o -4 4 1 174.60 199.87 10.81 o -3 4 1 230.85 259.40 11.04 o -2 4 1 0.04 1.28 1.78 o -1 4 1 1445.30 1533.97 50.41 o 0 4 1 210.63 245.54 11.79 o 1 4 1 1709.59 1503.73 35.06 o 2 4 1 1.42 5.27 2.04 o 3 4 1 8.33 5.79 1.79 o 4 4 1 1.06 1.75 2.04 o 5 4 1 3786.09 3841.34 60.98 o 6 4 1 330.41 362.00 12.34 o 7 4 1 360.80 368.40 12.65 o 8 4 1 95.30 104.03 9.21 o 9 4 1 3.46 1.65 2.43 o 10 4 1 25.92 21.01 3.65 o 11 4 1 310.24 351.42 13.12 o 12 4 1 80.12 65.28 4.46 o -12 5 1 9.51 5.27 2.24 o -11 5 1 89.51 79.36 6.66 o -10 5 1 292.05 317.97 9.27 o -9 5 1 26.75 20.13 2.64 o -8 5 1 185.05 210.33 8.33 o -7 5 1 80.27 83.99 6.76 o -6 5 1 89.51 102.13 4.27 o -5 5 1 15.34 12.26 2.03 o -4 5 1 1501.02 1533.39 33.45 o -3 5 1 39.42 51.32 5.71 o -2 5 1 327.86 337.49 10.91 o -1 5 1 117.69 94.42 10.28 o 0 5 1 707.46 642.27 23.70 o 1 5 1 2.85 8.39 1.63 o 2 5 1 84.20 77.62 4.88 o 3 5 1 106.32 103.82 4.96 o 4 5 1 340.41 365.09 9.82 o 5 5 1 411.78 406.04 11.84 o 6 5 1 828.88 862.05 30.93 o 7 5 1 332.87 340.87 13.02 o 8 5 1 42.52 50.36 5.44 o 9 5 1 122.82 126.39 6.86 o 10 5 1 257.93 306.54 10.73 o 11 5 1 66.82 66.05 5.67 o -11 6 1 34.25 38.31 4.35 o -10 6 1 154.72 172.16 7.91 o -9 6 1 195.11 209.44 8.73 o -8 6 1 38.33 34.01 4.79 o -7 6 1 94.58 105.39 6.31 o -6 6 1 297.41 294.24 12.00 o -5 6 1 379.87 398.66 37.85 o -4 6 1 692.33 730.36 25.73 o -3 6 1 1059.00 1049.55 40.29 o -2 6 1 127.31 126.54 6.72 o -1 6 1 461.38 517.46 15.99 o 0 6 1 495.50 535.52 15.35 o 1 6 1 0.71 -0.98 1.79 o 2 6 1 384.95 362.61 10.71 o 3 6 1 100.79 98.65 5.32 o 4 6 1 2817.38 3190.69 92.68 o 5 6 1 565.26 669.45 27.51 o 6 6 1 6.41 14.38 3.37 o 7 6 1 10.28 9.18 3.78 o 8 6 1 1.12 -1.89 2.22 o 9 6 1 166.41 158.02 7.07 o 10 6 1 8.90 11.42 1.88 o -10 7 1 0.35 0.60 2.19 o -9 7 1 26.41 27.45 2.59 o -8 7 1 178.12 163.62 7.38 o -7 7 1 25.83 35.76 3.57 o -6 7 1 398.56 411.02 13.33 o -5 7 1 3.01 4.81 2.40 o -4 7 1 95.03 92.19 7.19 o -3 7 1 240.82 264.88 16.55 o -2 7 1 710.73 765.80 24.13 o -1 7 1 18.14 20.00 5.35 o 0 7 1 57.96 79.29 12.36 o 1 7 1 296.06 327.37 18.87 o 2 7 1 1780.59 1777.99 41.67 o 3 7 1 52.67 59.48 5.40 o 4 7 1 1023.22 1040.52 29.13 o 5 7 1 336.87 335.16 11.43 o 6 7 1 75.03 91.41 5.22 o 7 7 1 1.36 1.60 2.48 o 8 7 1 152.16 132.56 10.26 o 9 7 1 42.23 48.63 3.27 o -8 8 1 12.67 12.04 3.32 o -7 8 1 373.60 337.98 9.30 o -6 8 1 2.33 0.59 1.61 o -5 8 1 46.18 50.53 4.16 o -4 8 1 4.78 7.18 1.93 o -3 8 1 218.00 207.19 9.28 o -2 8 1 81.59 82.76 6.89 o -1 8 1 407.39 424.40 21.80 o 0 8 1 2.59 -0.75 2.44 o 1 8 1 60.52 61.71 4.98 o 2 8 1 3.66 2.22 2.33 o 3 8 1 468.47 434.51 15.90 o 4 8 1 2.64 7.29 2.63 o 5 8 1 22.20 21.82 2.41 o 6 8 1 2.51 1.29 1.32 o 7 8 1 139.38 120.28 6.77 o -4 9 1 0.97 0.50 0.93 o -3 9 1 23.98 18.89 2.06 o -2 9 1 41.47 42.08 3.41 o -1 9 1 43.62 41.38 4.30 o 0 9 1 20.53 14.85 3.59 o 1 9 1 17.33 18.89 2.49 o 2 9 1 80.47 81.59 4.69 o 3 9 1 0.78 0.99 1.31 o 4 9 1 23.83 17.97 3.67 o -14 0 2 478.23 471.18 26.17 o -12 0 2 305.44 323.61 13.26 o -10 0 2 1151.97 1195.42 36.59 o -8 0 2 2169.20 2088.94 43.23 o -6 0 2 279.92 318.65 8.78 o -4 0 2 5970.44 5714.64 101.98 o -2 0 2 657.32 762.74 11.99 o 0 0 2 14125.79 13417.61 169.76 o 2 0 2 15847.18 16352.48 260.27 o 4 0 2 24298.92 25413.53 643.24 o 6 0 2 3972.61 3904.46 178.10 o 8 0 2 2.85 6.55 2.54 o 10 0 2 519.22 589.85 34.20 o 12 0 2 185.51 153.15 10.63 o -15 1 2 17.23 22.10 3.06 o -14 1 2 1.38 6.52 2.39 o -13 1 2 257.73 283.97 12.26 o -12 1 2 4.20 2.80 2.28 o -11 1 2 59.81 56.36 6.05 o -10 1 2 489.10 446.29 10.84 o -9 1 2 1689.61 1610.66 21.52 o -8 1 2 272.83 284.54 8.07 o -7 1 2 1296.71 1333.76 22.01 o -6 1 2 2155.53 2220.28 42.61 o -5 1 2 444.17 419.17 8.61 o -4 1 2 488.40 422.57 7.19 o -3 1 2 1781.69 1748.72 20.13 o -2 1 2 5614.10 5771.53 69.13 o -1 1 2 318.04 308.60 5.81 o 0 1 2 11029.18 10885.02 112.82 o 1 1 2 16728.11 17047.11 215.11 o 2 1 2 7072.10 7620.21 87.19 o 3 1 2 1287.80 1336.44 21.65 o 4 1 2 855.49 892.32 19.88 o 5 1 2 2041.01 2024.00 46.45 o 6 1 2 2256.85 2377.80 48.08 o 7 1 2 504.01 480.94 10.56 o 8 1 2 16.51 19.08 2.42 o 9 1 2 0.57 3.79 1.86 o 10 1 2 194.63 179.64 13.91 o 11 1 2 616.04 639.63 19.84 o 12 1 2 76.27 72.55 6.14 o 13 1 2 26.24 30.47 2.96 o -14 2 2 32.02 41.17 6.13 o -13 2 2 68.92 56.34 4.19 o -12 2 2 3.36 5.58 2.66 o -11 2 2 351.94 353.86 15.73 o -10 2 2 98.69 88.96 4.10 o -9 2 2 4.20 5.62 1.27 o -8 2 2 341.01 329.82 8.62 o -7 2 2 4.16 8.88 2.36 o -6 2 2 2554.52 2554.18 59.33 o -5 2 2 1729.19 1670.77 33.26 o -4 2 2 2984.78 3400.80 52.74 o -3 2 2 1382.12 1310.81 20.15 o -2 2 2 1452.96 1673.84 26.87 o -1 2 2 99.62 113.12 3.21 o 0 2 2 3.07 3.59 0.84 o 1 2 2 86.56 104.60 3.53 o 2 2 2 151.47 159.53 4.60 o 3 2 2 443.08 445.99 12.87 o 4 2 2 1511.56 1406.96 35.15 o 5 2 2 14.41 12.03 1.99 o 6 2 2 294.59 286.98 9.24 o 7 2 2 409.98 419.04 9.23 o 8 2 2 18.08 14.15 2.10 o 9 2 2 455.71 494.97 17.80 o 10 2 2 67.12 72.64 7.36 o 11 2 2 5.14 1.58 3.32 o 12 2 2 10.85 9.34 2.58 o 13 2 2 159.07 147.67 6.39 o -14 3 2 41.76 45.25 4.15 o -13 3 2 87.43 97.97 7.80 o -12 3 2 7.54 5.65 2.08 o -11 3 2 75.17 69.05 4.33 o -10 3 2 236.59 227.93 8.02 o -9 3 2 577.35 560.65 10.97 o -8 3 2 26.53 18.62 1.98 o -7 3 2 1258.14 1201.49 23.02 o -6 3 2 15.24 22.92 2.54 o -5 3 2 1343.93 1583.24 27.93 o -4 3 2 65.48 79.04 3.90 o -3 3 2 1276.02 1219.47 22.20 o -2 3 2 1667.24 1701.04 35.61 o -1 3 2 10761.58 10841.33 199.43 o 0 3 2 1.74 0.26 1.17 o 1 3 2 1387.66 1486.46 24.15 o 2 3 2 1050.83 1104.84 23.45 o 3 3 2 985.12 926.11 18.50 o 4 3 2 1.01 1.23 1.37 o 5 3 2 564.94 560.48 19.86 o 6 3 2 116.14 126.99 5.31 o 7 3 2 44.65 52.57 3.47 o 8 3 2 293.02 289.57 9.31 o 9 3 2 1287.00 1277.61 30.84 o 10 3 2 195.68 239.18 12.76 o 11 3 2 17.00 20.07 3.23 o 12 3 2 216.70 215.31 10.33 o 13 3 2 3.70 0.94 1.63 o -13 4 2 1.14 3.30 2.24 o -12 4 2 609.94 640.89 16.97 o -11 4 2 0.26 0.94 1.54 o -10 4 2 81.39 92.10 5.54 o -9 4 2 401.20 421.94 12.88 o -8 4 2 856.59 850.66 19.55 o -7 4 2 23.05 21.58 2.58 o -6 4 2 1466.30 1407.35 25.86 o -5 4 2 103.72 104.71 4.42 o -4 4 2 186.56 197.36 8.01 o -3 4 2 685.53 819.71 23.42 o -2 4 2 5534.29 5987.47 161.04 o -1 4 2 0.80 0.46 1.71 o 0 4 2 5132.01 5468.95 106.33 o 1 4 2 1552.74 1669.24 34.30 o 2 4 2 240.53 264.04 11.31 o 3 4 2 122.72 109.47 7.36 o 4 4 2 4842.07 4817.85 87.65 o 5 4 2 2.28 -0.77 1.96 o 6 4 2 1.29 2.32 1.95 o 7 4 2 9.99 18.58 2.66 o 8 4 2 1655.92 1840.66 43.91 o 9 4 2 10.36 5.55 2.58 o 10 4 2 245.75 252.56 9.05 o 11 4 2 123.57 125.60 6.85 o 12 4 2 1.99 0.63 1.45 o -12 5 2 9.79 7.45 1.79 o -11 5 2 146.09 175.80 7.75 o -10 5 2 2.19 1.61 1.89 o -9 5 2 7.55 7.76 2.23 o -8 5 2 802.74 867.36 23.10 o -7 5 2 2012.13 2089.08 36.83 o -6 5 2 81.75 91.95 4.51 o -5 5 2 478.18 517.65 14.58 o -4 5 2 450.25 450.24 12.49 o -3 5 2 58.29 55.92 4.17 o -2 5 2 361.74 395.41 16.51 o -1 5 2 967.93 931.86 22.62 o 0 5 2 202.97 193.86 5.57 o 1 5 2 80.20 88.54 4.55 o 2 5 2 228.41 227.53 7.87 o 3 5 2 665.92 703.69 20.91 o 4 5 2 187.45 179.79 8.82 o 5 5 2 26.21 20.45 3.89 o 6 5 2 29.61 26.20 5.28 o 7 5 2 356.01 401.41 19.33 o 8 5 2 26.27 19.53 3.56 o 9 5 2 92.49 101.65 5.99 o 10 5 2 163.82 150.42 7.84 o 11 5 2 1.58 1.64 1.54 o -11 6 2 23.23 29.21 3.10 o -10 6 2 54.92 53.07 4.76 o -9 6 2 44.90 49.38 5.03 o -8 6 2 0.94 1.43 2.01 o -7 6 2 462.32 462.50 13.57 o -6 6 2 513.46 557.91 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