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Information card for entry 2022960
Preview
| Coordinates | 2022960.cif |
|---|---|
| Structure factors | 2022960.hkl |
| Original IUCr paper | HTML |
| Chemical name | Chloridobis{<i>N</i>-[(4-methoxyphenyl)imino]pyrrolidine-1-carboxamide}zinc(II) (acetonitrile)trichloridozincate |
|---|---|
| Formula | C26 H33 Cl4 N7 O4 Zn2 |
| Calculated formula | C26 H33 Cl4 N7 O4 Zn2 |
| Title of publication | The synthesis and structural properties of a chlorido-bis-{<i>N</i>-[(4-meth-oxy-phen-yl)imino]-pyrrolidine-1-carboxamide}-zinc(II) (aceto-nitrile)-trichlorido-zincate coordination complex. |
| Authors of publication | Tiwari, Laxmi; Waynant, Kristopher V. |
| Journal of publication | Acta crystallographica. Section E, Crystallographic communications |
| Year of publication | 2024 |
| Journal volume | 80 |
| Journal issue | Pt 1 |
| Pages of publication | 14 - 17 |
| a | 28.4313 ± 0.0007 Å |
| b | 7.6516 ± 0.0002 Å |
| c | 29.5461 ± 0.0009 Å |
| α | 90° |
| β | 90° |
| γ | 90° |
| Cell volume | 6427.6 ± 0.3 Å3 |
| Cell temperature | 100 K |
| Ambient diffraction temperature | 100 K |
| Number of distinct elements | 6 |
| Space group number | 61 |
| Hermann-Mauguin space group symbol | P b c a |
| Hall space group symbol | -P 2ac 2ab |
| Residual factor for all reflections | 0.0673 |
| Residual factor for significantly intense reflections | 0.0457 |
| Weighted residual factors for significantly intense reflections | 0.0953 |
| Weighted residual factors for all reflections included in the refinement | 0.1039 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.151 |
| Diffraction radiation probe | x-ray |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | No |
| Has Fobs | Yes |
| Revision | Date | Message | Files |
|---|---|---|---|
| 289695 (current) | 2024-02-05 | cif/ Updating files of 2022960 Original log message: Adding full bibliography for 2022960.cif. |
2022960.cif 2022960.hkl |
| 288207 | 2023-12-09 | cif/ hkl/ Adding structures of 2022960 via cif-deposit CGI script. |
2022960.cif 2022960.hkl |
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Users of the data should acknowledge the original authors of the
structural data.