Crystallography Open Database

Information card for entry 2022984

2022983 << 2022984 >> 2022985

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Structure parameters

Chemical name	Poly[(μ-2-methylpyridine <i>N</i>-oxide-κ^2^<i>O</i>:<i>O</i>)bis(μ-thiocyanato-κ^2^<i>N</i>:<i>S</i>)cobalt(II)]
Formula	C8 H7 Co N3 O S2
Calculated formula	C8 H7 Co N3 O S2
Title of publication	Synthesis, crystal structure and properties of poly[(μ-2-methyl-pyridine <i>N</i>-oxide-κ<sup>2</sup><i>O</i>:<i>O</i>)bis-(μ-thio-cyanato-κ<sup>2</sup><i>N</i>:<i>S</i>)cobalt(II)].
Authors of publication	Näther, Christian; Jess, Inke
Journal of publication	Acta crystallographica. Section E, Crystallographic communications
Year of publication	2024
Journal volume	80
Journal issue	Pt 1
Pages of publication	67 - 71
a	7.67386 ± 0.00011 Å
b	7.66462 ± 0.00009 Å
c	18.8755 ± 0.0002 Å
α	90°
β	97.4258 ± 0.0012°
γ	90°
Cell volume	1100.89 ± 0.02 Å³
Cell temperature	100 ± 0.1 K
Ambient diffraction temperature	100 ± 0.1 K
Number of distinct elements	6
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/c 1
Hall space group symbol	-P 2ybc
Residual factor for all reflections	0.029
Residual factor for significantly intense reflections	0.0287
Weighted residual factors for significantly intense reflections	0.0654
Weighted residual factors for all reflections included in the refinement	0.0655
Goodness-of-fit parameter for all reflections included in the refinement	1.173
Diffraction radiation probe	x-ray
Diffraction radiation wavelength	1.54184 Å
Diffraction radiation type	CuKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	Yes

Version history

Revision	Date	Message	Files
289686 (current)	2024-02-05	cif/ Updating files of 2022984 Original log message: Adding full bibliography for 2022984.cif.	2022984.cif 2022984.hkl
288522	2023-12-23	cif/ hkl/ Adding structures of 2022984 via cif-deposit CGI script.	2022984.cif 2022984.hkl