#------------------------------------------------------------------------------ #$Date: 2023-12-23 04:56:48 +0200 (Sat, 23 Dec 2023) $ #$Revision: 288525 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/02/29/2022990.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2022990 _cell_angle_alpha 90.000 _cell_angle_beta 105.400 _cell_angle_gamma 90.000 _cell_length_a 12.3588 _cell_length_b 12.7942 _cell_length_c 12.2759 _exptl_crystal_F_000 992.00 _reflns_d_resolution_high 0.7997 _cod_data_source_file wm57062sup4.hkl _cod_data_source_block 2 _shelx_title ' saba2low_a.res in Cc' _shelx_refln_list_code 4 _shelx_f_calc_maximum 384.74 _shelx_f_squared_multiplier 1.000 loop_ _space_group_symop_operation_xyz 'x, y, z' 'x, -y, z+1/2' 'x+1/2, y+1/2, z' 'x+1/2, -y+1/2, z+1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 1 -15 46.67 52.23 5.10 o 3 1 -15 33.12 30.16 1.25 o 5 1 -15 189.67 198.07 7.22 o 2 2 -15 23.54 18.39 0.94 o 4 2 -15 26.12 17.12 1.13 o 6 2 -15 19.33 17.04 1.07 o 3 3 -15 203.86 213.42 7.22 o 5 3 -15 51.22 49.15 2.14 o -2 0 -14 341.92 300.79 13.00 o 0 0 -14 68.66 45.43 5.56 o 2 0 -14 581.59 658.13 65.47 o 6 0 -14 52.55 38.01 3.71 o 8 0 -14 16.23 16.69 2.78 o -1 1 -14 764.42 772.13 18.52 o 1 1 -14 664.66 678.27 16.24 o 3 1 -14 1315.76 1250.27 37.51 o 5 1 -14 210.08 166.60 7.21 o 7 1 -14 144.41 139.11 8.35 o -2 2 -14 89.90 94.59 2.62 o 2 2 -14 47.80 51.22 1.54 o 4 2 -14 216.67 204.48 10.40 o 6 2 -14 40.89 42.08 2.90 o 8 2 -14 19.77 22.25 2.78 o -1 3 -14 226.15 216.56 5.02 o 1 3 -14 1463.41 1339.19 33.65 o 3 3 -14 161.47 152.87 3.80 o 5 3 -14 792.56 702.16 18.19 o 7 3 -14 809.19 837.03 26.95 o 0 4 -14 22.08 23.18 0.93 o 2 4 -14 182.87 246.20 7.13 o 4 4 -14 28.51 25.96 1.61 o 6 4 -14 25.11 24.57 1.97 o 8 4 -14 77.83 39.87 3.71 o 1 5 -14 209.83 219.26 5.26 o 3 5 -14 1133.51 1024.84 31.80 o 5 5 -14 205.71 210.09 5.61 o 7 5 -14 220.50 222.68 11.13 o 2 6 -14 59.34 79.34 3.28 o 4 6 -14 21.25 19.66 0.60 o 6 6 -14 12.36 27.81 2.78 o -3 1 -13 44.96 44.68 0.67 o -1 1 -13 37.90 38.39 0.71 o 1 1 -13 629.18 660.03 14.58 o 3 1 -13 503.12 520.21 11.87 o 5 1 -13 0.59 2.78 1.97 o 7 1 -13 161.79 169.75 7.87 o 9 1 -13 5.28 5.14 0.66 o 11 1 -13 53.11 30.60 1.85 o -4 2 -13 62.64 52.47 1.28 o -2 2 -13 24.59 25.34 0.59 o 0 2 -13 227.44 239.16 3.93 o 2 2 -13 39.98 39.26 1.19 o 4 2 -13 166.38 193.00 8.52 o 6 2 -13 125.38 126.03 7.88 o 8 2 -13 82.68 84.87 5.10 o 10 2 -13 153.30 152.10 7.42 o -3 3 -13 153.90 144.95 2.55 o -1 3 -13 73.92 74.32 1.40 o 1 3 -13 54.25 58.42 1.23 o 3 3 -13 217.34 198.96 5.96 o 5 3 -13 56.78 63.04 5.56 o 7 3 -13 41.75 24.58 2.62 o 9 3 -13 45.46 40.79 1.85 o -2 4 -13 64.16 56.93 1.22 o 0 4 -13 49.00 48.73 1.31 o 2 4 -13 17.98 12.91 0.79 o 4 4 -13 17.85 9.36 1.97 o 6 4 -13 159.19 181.36 7.87 o 8 4 -13 79.88 79.56 2.88 o -1 5 -13 302.49 319.98 8.97 o 1 5 -13 95.96 93.32 3.74 o 3 5 -13 154.67 132.95 4.36 o 5 5 -13 17.56 21.35 1.61 o 7 5 -13 246.57 237.04 7.50 o -2 6 -13 22.62 22.25 0.93 o 0 6 -13 21.04 16.74 0.93 o 2 6 -13 81.72 57.08 1.77 o 4 6 -13 52.44 64.62 2.82 o 6 6 -13 23.62 21.02 1.61 o 8 6 -13 77.63 80.67 5.56 o -1 7 -13 263.41 246.69 17.63 o 1 7 -13 266.01 251.32 13.93 o 3 7 -13 167.25 137.40 6.53 o 5 7 -13 296.47 244.37 7.31 o 7 7 -13 90.72 66.77 4.64 o 4 8 -13 13.88 6.98 1.31 o 6 8 -13 82.71 76.04 4.64 o -6 0 -12 234.29 305.58 6.50 o -4 0 -12 39.75 49.22 1.61 o -2 0 -12 59.42 61.40 1.37 o 0 0 -12 203.24 226.01 6.29 o 2 0 -12 87.89 79.50 16.01 o 4 0 -12 705.00 662.02 27.86 o 6 0 -12 552.56 529.96 36.67 o 8 0 -12 9.68 6.49 0.93 o 10 0 -12 35.70 28.74 1.85 o 12 0 -12 22.06 16.69 0.93 o -5 1 -12 263.95 329.60 5.31 o -3 1 -12 109.83 104.72 1.51 o -1 1 -12 158.93 142.39 2.12 o 1 1 -12 458.57 499.31 11.74 o 3 1 -12 8.06 119.49 124.06 o 5 1 -12 122.97 77.14 5.25 o 7 1 -12 20.93 21.90 2.90 o 9 1 -12 195.11 183.18 5.90 o 11 1 -12 228.72 191.56 5.90 o -4 2 -12 91.63 93.64 1.64 o -2 2 -12 88.86 82.70 1.46 o 0 2 -12 58.19 44.44 1.03 o 2 2 -12 97.41 106.40 13.51 o 4 2 -12 291.04 306.78 14.52 o 6 2 -12 367.08 355.58 17.14 o 8 2 -12 179.65 206.36 6.56 o 10 2 -12 380.84 324.01 10.50 o 12 2 -12 171.00 158.63 5.25 o -5 3 -12 129.82 163.18 2.46 o -3 3 -12 69.89 71.08 1.20 o -1 3 -12 68.71 59.90 0.99 o 1 3 -12 56.69 68.68 3.19 o 3 3 -12 574.78 597.67 18.09 o 5 3 -12 274.63 295.45 11.81 o 7 3 -12 655.07 544.04 14.34 o 9 3 -12 1202.27 1094.12 32.89 o 11 3 -12 68.43 41.26 1.97 o -4 4 -12 10.61 10.63 0.48 o -2 4 -12 52.20 61.15 0.99 o 0 4 -12 163.09 161.34 3.81 o 2 4 -12 236.58 200.90 5.02 o 4 4 -12 26.90 38.01 3.28 o 6 4 -12 404.63 319.83 12.47 o 8 4 -12 286.62 253.07 18.55 o 10 4 -12 563.85 478.17 20.43 o -3 5 -12 92.25 91.89 1.65 o -1 5 -12 31.92 32.40 0.76 o 1 5 -12 196.73 202.34 4.44 o 3 5 -12 37.14 21.91 2.37 o 5 5 -12 442.07 406.50 15.09 o 7 5 -12 136.31 127.09 7.88 o 9 5 -12 142.65 95.52 4.64 o 11 5 -12 161.97 141.93 6.49 o -4 6 -12 20.64 22.01 0.86 o -2 6 -12 184.89 182.23 4.04 o 0 6 -12 98.95 92.09 1.82 o 2 6 -12 78.58 70.69 2.77 o 4 6 -12 183.15 151.73 5.48 o 6 6 -12 194.40 173.47 4.37 o 8 6 -12 230.62 191.15 8.35 o 10 6 -12 325.45 281.24 12.07 o -3 7 -12 52.53 62.38 1.36 o -1 7 -12 149.00 131.63 2.16 o 1 7 -12 207.48 229.11 4.94 o 3 7 -12 101.48 105.11 4.44 o 5 7 -12 52.63 46.51 2.46 o 7 7 -12 82.81 53.78 2.78 o 9 7 -12 20.64 10.20 0.93 o -2 8 -12 1.77 2.78 0.93 o 0 8 -12 135.20 154.87 6.49 o 2 8 -12 1.45 2.78 1.31 o 4 8 -12 213.09 202.90 6.59 o 6 8 -12 74.60 74.17 5.56 o 1 9 -12 23.66 19.18 0.76 o 3 9 -12 53.60 63.88 2.01 o 7 9 -12 22.79 23.18 2.78 o -7 1 -11 2.12 2.97 0.34 o -5 1 -11 14.23 13.04 0.42 o -3 1 -11 135.29 115.01 1.71 o -1 1 -11 11.39 13.84 1.75 o 1 1 -11 86.43 105.23 3.72 o 3 1 -11 1110.83 1163.81 33.60 o 5 1 -11 1248.32 1174.26 28.42 o 7 1 -11 19.61 12.83 0.76 o 9 1 -11 68.93 54.08 1.49 o 11 1 -11 24.17 14.58 0.76 o 13 1 -11 44.12 27.81 1.31 o -6 2 -11 2.40 7.85 0.35 o -4 2 -11 61.45 58.43 0.96 o -2 2 -11 267.87 258.14 4.01 o 0 2 -11 15.30 -26.69 42.90 o 2 2 -11 446.42 384.12 7.23 o 4 2 -11 59.54 64.00 3.07 o 6 2 -11 344.16 314.36 15.13 o 8 2 -11 272.82 272.15 6.25 o 10 2 -11 100.08 98.31 2.52 o 12 2 -11 139.57 141.04 3.75 o -7 3 -11 109.40 107.84 1.66 o -5 3 -11 21.61 16.79 0.38 o -3 3 -11 12.55 20.14 0.56 o -1 3 -11 125.92 115.41 2.93 o 1 3 -11 31.45 23.91 1.50 o 3 3 -11 48.65 56.37 2.32 o 5 3 -11 265.60 280.73 25.32 o 7 3 -11 119.03 96.93 3.56 o 9 3 -11 82.60 65.71 1.91 o 11 3 -11 6.92 12.34 2.32 o -6 4 -11 10.12 7.43 0.38 o -4 4 -11 20.07 17.24 0.39 o -2 4 -11 19.71 15.45 0.43 o 0 4 -11 209.76 192.02 6.41 o 2 4 -11 130.91 135.94 14.22 o 4 4 -11 198.18 156.79 8.10 o 8 4 -11 498.90 421.20 10.53 o 10 4 -11 118.35 87.81 2.57 o 12 4 -11 78.66 85.30 4.64 o -5 5 -11 178.09 155.02 2.09 o -3 5 -11 76.71 76.79 1.24 o -1 5 -11 45.53 59.49 1.13 o 1 5 -11 522.82 520.28 9.46 o 3 5 -11 74.90 56.56 21.28 o 5 5 -11 677.28 638.16 58.57 o 7 5 -11 135.38 144.00 4.88 o 9 5 -11 655.45 570.50 14.29 o 11 5 -11 992.67 798.00 24.00 o -4 6 -11 3.90 8.26 0.41 o -2 6 -11 111.99 105.45 1.94 o 0 6 -11 62.66 49.74 2.12 o 2 6 -11 512.65 590.60 23.58 o 4 6 -11 41.17 27.26 1.66 o 6 6 -11 162.65 107.17 5.59 o 8 6 -11 9.01 9.76 0.66 o 10 6 -11 203.39 158.18 5.25 o -5 7 -11 12.46 11.71 0.53 o -3 7 -11 510.57 483.23 7.25 o -1 7 -11 109.14 116.60 2.45 o 1 7 -11 323.76 299.10 7.01 o 3 7 -11 495.00 439.80 11.44 o 5 7 -11 290.06 251.79 6.90 o 7 7 -11 829.78 781.73 24.86 o 9 7 -11 312.27 270.01 12.06 o 11 7 -11 117.16 106.66 4.64 o -4 8 -11 223.37 234.15 8.44 o -2 8 -11 302.78 316.88 4.78 o 0 8 -11 185.52 153.65 3.58 o 2 8 -11 32.51 21.80 2.78 o 4 8 -11 266.94 326.31 9.81 o 6 8 -11 100.89 110.01 10.20 o 8 8 -11 250.64 212.74 7.42 o 10 8 -11 1.72 8.34 0.93 o -3 9 -11 73.07 73.91 3.71 o -1 9 -11 666.99 649.25 20.52 o 1 9 -11 131.64 106.50 2.21 o 3 9 -11 636.49 599.79 14.11 o 5 9 -11 156.52 147.48 6.56 o 7 9 -11 145.72 134.37 5.12 o 9 9 -11 89.84 72.33 3.71 o 0 10 -11 153.22 175.68 5.69 o 2 10 -11 87.25 79.91 6.49 o 4 10 -11 30.45 16.78 0.84 o 6 10 -11 165.37 164.18 9.28 o 3 11 -11 55.81 66.57 2.90 o -8 0 -10 335.59 366.97 7.54 o -6 0 -10 29.33 25.11 0.98 o -4 0 -10 272.83 270.72 5.68 o -2 0 -10 68.45 49.11 1.87 o 0 0 -10 397.07 325.34 13.91 o 4 0 -10 731.46 750.99 32.97 o 6 0 -10 215.62 179.00 13.91 o 10 0 -10 650.02 477.01 14.76 o 12 0 -10 43.70 36.16 1.42 o -7 1 -10 302.29 296.77 4.07 o -5 1 -10 358.42 352.42 4.57 o -3 1 -10 131.34 117.33 2.04 o -1 1 -10 628.42 646.12 8.96 o 1 1 -10 3034.92 3521.37 89.01 o 3 1 -10 2191.65 2305.38 68.88 o 5 1 -10 397.77 420.85 12.78 o 7 1 -10 2320.90 1938.72 59.34 o 9 1 -10 951.48 876.87 14.00 o 11 1 -10 93.97 80.66 2.25 o 13 1 -10 76.75 73.30 2.14 o -8 2 -10 17.78 11.02 0.40 o -6 2 -10 115.70 143.87 2.24 o -4 2 -10 153.08 153.50 2.38 o -2 2 -10 83.75 90.46 1.52 o 0 2 -10 49.05 60.70 10.46 o 2 2 -10 767.99 720.31 19.34 o 4 2 -10 166.08 162.18 11.13 o 6 2 -10 2125.01 2273.81 68.20 o 8 2 -10 70.78 47.96 1.37 o 10 2 -10 1997.17 1818.23 38.77 o 12 2 -10 628.78 567.00 14.29 o -7 3 -10 180.98 171.76 2.44 o -5 3 -10 110.49 118.46 1.99 o -3 3 -10 7.21 11.67 1.23 o -1 3 -10 138.07 167.42 4.63 o 1 3 -10 1055.65 1162.88 18.79 o 3 3 -10 599.74 646.68 12.41 o 5 3 -10 1780.19 1600.73 40.08 o 7 3 -10 577.05 579.38 10.30 o 9 3 -10 2239.99 1831.92 56.04 o 11 3 -10 741.65 671.25 18.35 o 13 3 -10 6.08 2.78 0.54 o -8 4 -10 46.35 48.23 3.28 o -6 4 -10 2.67 1.30 0.31 o -4 4 -10 26.43 26.55 0.64 o -2 4 -10 170.91 164.22 2.78 o 0 4 -10 617.50 576.89 12.66 o 2 4 -10 99.16 107.30 15.59 o 4 4 -10 626.80 611.45 16.95 o 6 4 -10 135.44 143.32 4.74 o 10 4 -10 1635.48 1287.82 27.34 o 12 4 -10 1015.32 865.92 18.36 o -7 5 -10 169.03 158.38 2.59 o -5 5 -10 133.02 141.46 2.13 o -3 5 -10 22.08 20.04 0.57 o -1 5 -10 176.61 169.32 3.89 o 1 5 -10 310.59 321.05 6.93 o 3 5 -10 508.83 513.49 11.88 o 5 5 -10 32.12 35.60 4.22 o 7 5 -10 1612.65 1249.40 50.30 o 9 5 -10 448.46 406.10 8.20 o 11 5 -10 3.23 4.28 0.45 o -6 6 -10 1.36 5.13 0.42 o -4 6 -10 103.05 115.66 1.70 o -2 6 -10 18.32 16.04 1.70 o 0 6 -10 80.60 68.26 11.76 o 2 6 -10 1595.54 1568.67 46.24 o 4 6 -10 1598.70 1473.71 38.11 o 6 6 -10 900.42 815.89 22.87 o 8 6 -10 651.38 625.24 15.72 o 10 6 -10 1076.82 900.03 37.70 o 12 6 -10 312.09 253.38 11.14 o -5 7 -10 173.79 170.31 3.16 o -3 7 -10 224.59 271.17 4.02 o -1 7 -10 192.02 182.21 2.91 o 1 7 -10 552.29 561.04 10.08 o 3 7 -10 87.03 176.16 140.00 o 5 7 -10 62.91 33.21 3.24 o 7 7 -10 5.42 5.43 1.39 o 9 7 -10 24.08 7.23 1.39 o 11 7 -10 17.87 13.46 0.66 o -4 8 -10 15.95 10.70 0.53 o -2 8 -10 6.34 5.93 0.44 o 0 8 -10 277.49 298.19 4.87 o 2 8 -10 386.47 344.97 7.92 o 4 8 -10 362.29 331.95 7.78 o 6 8 -10 273.23 250.08 8.91 o 8 8 -10 135.25 105.26 3.21 o 10 8 -10 143.90 127.12 3.93 o -3 9 -10 250.61 266.50 3.97 o -1 9 -10 134.15 130.97 3.39 o 1 9 -10 82.77 74.78 2.21 o 3 9 -10 52.05 58.77 2.81 o 7 9 -10 451.54 352.44 20.42 o 9 9 -10 9.96 5.56 0.93 o -2 10 -10 7.86 9.86 0.80 o 0 10 -10 8.37 12.98 0.93 o 2 10 -10 82.70 96.54 2.31 o 4 10 -10 69.60 67.22 3.93 o 6 10 -10 22.08 21.32 1.85 o 8 10 -10 30.51 33.64 1.72 o -1 11 -10 5.77 5.24 0.60 o 1 11 -10 48.81 42.30 1.67 o 3 11 -10 10.05 14.40 1.63 o 5 11 -10 43.33 45.90 2.23 o 7 11 -10 35.32 31.52 3.71 o 2 12 -10 69.86 71.69 3.09 o 4 12 -10 132.60 132.33 8.81 o -9 1 -9 23.17 20.95 0.68 o -7 1 -9 118.93 106.54 1.61 o -5 1 -9 34.21 36.76 1.00 o -3 1 -9 45.51 38.71 0.72 o -1 1 -9 107.08 104.85 1.69 o 1 1 -9 301.95 263.62 5.97 o 3 1 -9 210.94 253.35 7.56 o 5 1 -9 897.41 882.14 14.62 o 9 1 -9 82.40 82.43 1.88 o 11 1 -9 14.56 18.65 0.84 o 13 1 -9 34.20 25.61 0.84 o -8 2 -9 202.32 193.47 2.76 o -6 2 -9 28.18 41.67 0.84 o -4 2 -9 68.44 88.79 1.41 o -2 2 -9 22.84 17.64 0.59 o 0 2 -9 1266.02 1220.73 18.31 o 2 2 -9 5.66 8.70 0.53 o 4 2 -9 1743.39 1545.50 29.81 o 6 2 -9 1467.31 1449.66 27.96 o 8 2 -9 897.94 755.18 12.31 o 10 2 -9 250.28 241.78 4.95 o 12 2 -9 41.11 38.16 1.08 o 14 2 -9 130.27 133.39 2.99 o -9 3 -9 67.89 53.24 1.10 o -7 3 -9 34.96 37.74 0.66 o -5 3 -9 335.90 331.05 5.14 o -3 3 -9 18.67 16.07 0.75 o -1 3 -9 451.90 463.26 6.35 o 1 3 -9 340.31 291.16 5.16 o 3 3 -9 111.44 107.16 2.75 o 5 3 -9 139.52 130.44 2.78 o 7 3 -9 20.94 14.13 0.62 o 9 3 -9 59.02 46.51 1.81 o 11 3 -9 17.11 9.02 0.56 o 13 3 -9 94.32 103.71 2.52 o -8 4 -9 108.34 132.97 1.94 o -6 4 -9 280.53 274.95 3.72 o -4 4 -9 206.49 242.53 4.21 o -2 4 -9 71.05 79.01 1.86 o 0 4 -9 68.53 68.41 1.44 o 2 4 -9 342.14 289.11 8.74 o 4 4 -9 17.50 24.04 17.25 o 6 4 -9 227.68 262.93 5.15 o 8 4 -9 2018.87 1902.34 82.92 o 10 4 -9 997.62 790.42 14.15 o 12 4 -9 224.30 199.40 3.75 o -7 5 -9 415.79 371.02 4.56 o -5 5 -9 86.02 92.74 1.33 o -3 5 -9 592.06 621.21 7.56 o -1 5 -9 90.84 87.96 5.17 o 1 5 -9 1699.72 1629.77 39.88 o 5 5 -9 244.98 262.30 5.19 o 7 5 -9 1996.16 2001.92 83.85 o 9 5 -9 244.39 234.01 4.51 o 11 5 -9 426.95 384.55 7.12 o 13 5 -9 148.00 128.74 6.03 o -8 6 -9 21.88 22.11 0.43 o -6 6 -9 92.82 94.02 1.89 o -4 6 -9 53.14 63.10 1.28 o -2 6 -9 5.12 2.16 16.46 o 0 6 -9 141.04 125.85 7.70 o 2 6 -9 41.66 42.51 1.93 o 4 6 -9 441.91 430.91 16.91 o 6 6 -9 1748.08 1644.76 88.45 o 8 6 -9 244.40 267.19 5.70 o 10 6 -9 130.72 120.00 2.77 o 12 6 -9 471.31 411.81 12.47 o -7 7 -9 297.97 257.74 5.15 o -5 7 -9 536.96 468.31 5.99 o -3 7 -9 239.77 240.50 3.49 o -1 7 -9 2735.29 2784.06 130.70 o 1 7 -9 1343.86 1282.21 32.63 o 3 7 -9 2171.85 1977.27 63.93 o 5 7 -9 2348.54 2377.64 70.35 o 7 7 -9 243.74 242.71 6.69 o 9 7 -9 1068.26 1037.77 25.75 o 11 7 -9 193.60 187.38 5.90 o -6 8 -9 28.14 32.43 1.21 o -4 8 -9 70.50 120.19 2.10 o -2 8 -9 356.35 341.27 5.95 o 0 8 -9 1358.54 1490.09 104.83 o 2 8 -9 259.19 181.64 7.28 o 4 8 -9 601.58 557.56 14.91 o 6 8 -9 106.60 112.97 3.36 o 8 8 -9 955.78 953.10 23.60 o 10 8 -9 475.18 428.12 13.13 o -5 9 -9 333.56 294.93 5.66 o -3 9 -9 1038.96 985.82 20.02 o -1 9 -9 505.72 514.01 8.13 o 1 9 -9 2407.08 2479.62 153.44 o 3 9 -9 617.09 601.16 15.37 o 5 9 -9 1090.49 991.82 42.76 o 7 9 -9 184.05 172.55 4.96 o 9 9 -9 50.62 48.21 1.97 o 11 9 -9 31.61 25.96 1.85 o -4 10 -9 101.80 130.88 5.09 o -2 10 -9 519.70 533.33 10.37 o 0 10 -9 466.67 405.01 10.31 o 2 10 -9 401.17 325.50 9.45 o 4 10 -9 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