Crystallography Open Database

Information card for entry 2023004

2023003 << 2023004 >> 2023005

Preview

Coordinates	2023004.cif
Original IUCr paper	HTML

Structure parameters

Chemical name	Poly[hexa-μ-bromido-bis{2-[1-(pyridin-2-yl)ethylideneamino]ethanolato}\ tetracopper(II)]
Formula	C18 H22 Br6 Cu4 N4 O2
Calculated formula	C18 H23 Br6 Cu4 N4 O2
Title of publication	Crystal structure of poly[hexa-μ-bro-mido-bis{2-[1-(py-ri-din-2-yl)ethyl-idene-amino]ethanol-ato}tetracopper(II)].
Authors of publication	Traoré, Bocar; Diouf, Ngoné; Kébé, Momath; Guéye-Sylla, Rokhaya; Thiam, Ibrahima Elhadji; Diouf, Ousmane; Retailleau, Pascal; Gaye, Mohamed
Journal of publication	Acta crystallographica. Section E, Crystallographic communications
Year of publication	2024
Journal volume	80
Journal issue	Pt 2
Pages of publication	133 - 136
a	23.1656 ± 0.0012 Å
b	7.7041 ± 0.0003 Å
c	16.5664 ± 0.0008 Å
α	90°
β	110.896 ± 0.006°
γ	90°
Cell volume	2762.1 ± 0.2 Å³
Cell temperature	291.8 ± 0.11 K
Ambient diffraction temperature	292.15 K
Number of distinct elements	6
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/c 1
Hall space group symbol	-P 2ybc
Residual factor for all reflections	0.035
Residual factor for significantly intense reflections	0.0293
Weighted residual factors for significantly intense reflections	0.0732
Weighted residual factors for all reflections included in the refinement	0.0761
Goodness-of-fit parameter for all reflections included in the refinement	1.021
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
290326 (current)	2024-03-05	cif/ Updating files of 2023004 Original log message: Adding full bibliography for 2023004.cif.	2023004.cif
289074	2024-01-13	cif/ Adding structures of 2023004 via cif-deposit CGI script.	2023004.cif