#------------------------------------------------------------------------------ #$Date: 2024-01-13 04:36:20 +0200 (Sat, 13 Jan 2024) $ #$Revision: 289077 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/02/30/2023009.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2023009 _cell_angle_alpha 90.000 _cell_angle_beta 95.689 _cell_angle_gamma 90.000 _cell_length_a 10.2407 _cell_length_b 12.6295 _cell_length_c 34.1269 _exptl_crystal_F_000 1840.00 _reflns_d_resolution_high 0.7972 _cod_data_source_file dj20742sup8.hkl _cod_data_source_block 2 _shelx_title ' 1_a.res in P2(1)/n' _shelx_refln_list_code 4 _shelx_f_calc_maximum 361.46 _shelx_f_squared_multiplier 1.000 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 78085.70 71536.02 939.94 o 4 0 0 11471.54 12869.37 207.49 o 6 0 0 18622.26 18999.23 329.07 o 8 0 0 3642.96 3948.76 100.33 o 10 0 0 963.82 940.53 65.36 o 12 0 0 9.68 338.58 61.53 o 1 1 0 41899.65 40189.52 545.70 o 2 1 0 121.58 364.76 20.02 o 3 1 0 234.64 1485.59 95.15 o 4 1 0 9089.39 8558.42 99.98 o 5 1 0 2552.87 2583.81 59.40 o 6 1 0 104.07 404.28 32.42 o 7 1 0 7.08 405.97 42.22 o 8 1 0 324.26 654.55 31.39 o 9 1 0 458.21 677.08 30.94 o 10 1 0 6.51 44.15 23.95 o 11 1 0 91.09 74.43 27.46 o 12 1 0 49.07 190.05 42.20 o 0 2 0 85.36 183.81 11.41 o 1 2 0 1228.67 1084.04 18.15 o 3 2 0 1034.77 2294.90 105.49 o 4 2 0 644.70 1027.75 40.45 o 5 2 0 1591.52 1585.90 26.28 o 6 2 0 834.25 1005.81 28.09 o 7 2 0 300.16 759.03 47.00 o 8 2 0 91.76 181.31 19.29 o 9 2 0 0.28 176.38 27.58 o 10 2 0 222.58 208.22 25.84 o 11 2 0 1001.16 1134.97 55.62 o 12 2 0 58.21 136.39 37.87 o 1 3 0 3998.75 4774.42 89.77 o 2 3 0 3370.89 5284.50 139.16 o 3 3 0 2696.40 4835.53 100.36 o 4 3 0 3564.12 3577.99 50.42 o 5 3 0 1309.09 1994.45 65.67 o 6 3 0 28.19 1164.47 151.75 o 7 3 0 377.32 512.53 23.29 o 8 3 0 67.82 258.27 21.13 o 9 3 0 293.22 374.75 27.81 o 10 3 0 30.59 122.07 25.43 o 11 3 0 64.08 108.66 36.18 o 12 3 0 6.27 59.25 36.93 o 0 4 0 629.92 724.37 28.11 o 1 4 0 4719.01 4678.65 54.94 o 2 4 0 5255.44 5673.82 75.26 o 3 4 0 1889.23 2278.69 51.10 o 4 4 0 858.02 1312.94 48.26 o 5 4 0 6281.76 6057.86 80.48 o 6 4 0 306.03 359.19 18.05 o 7 4 0 5932.06 5316.29 93.78 o 8 4 0 158.85 170.26 23.50 o 9 4 0 1867.65 1914.40 60.36 o 10 4 0 6.63 75.57 31.37 o 11 4 0 135.40 150.89 36.57 o 12 4 0 37.64 129.83 53.84 o 1 5 0 1362.82 1566.14 32.57 o 2 5 0 3386.36 6319.91 197.59 o 3 5 0 1529.99 1915.59 48.42 o 5 5 0 198.67 402.34 21.35 o 6 5 0 288.64 753.50 32.54 o 7 5 0 1742.76 1604.32 40.04 o 8 5 0 570.63 1173.69 52.85 o 9 5 0 21.85 64.56 26.45 o 10 5 0 225.32 426.67 40.52 o 11 5 0 37.87 89.85 35.30 o 12 5 0 247.77 226.67 44.64 o 0 6 0 762.50 909.01 34.53 o 1 6 0 31.71 306.06 31.17 o 2 6 0 753.49 922.38 30.99 o 3 6 0 635.24 792.05 27.08 o 4 6 0 73.13 322.02 30.15 o 5 6 0 383.20 516.00 20.89 o 6 6 0 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326.21 33.39 o 8 9 0 187.41 205.29 34.61 o 9 9 0 253.68 308.04 39.03 o 10 9 0 11.23 -32.14 36.12 o 0 10 0 1209.48 1575.84 64.28 o 1 10 0 670.12 974.70 39.45 o 2 10 0 15.81 715.49 71.27 o 3 10 0 302.06 493.67 43.00 o 4 10 0 511.07 496.00 32.23 o 5 10 0 185.08 249.59 27.99 o 6 10 0 35.13 82.17 28.98 o 7 10 0 47.09 -12.74 29.51 o 8 10 0 218.81 218.71 38.18 o 9 10 0 13.97 101.11 36.32 o 1 11 0 68.37 141.70 27.30 o 2 11 0 122.68 286.61 30.01 o 3 11 0 85.94 367.70 38.04 o 4 11 0 432.17 518.17 38.62 o 5 11 0 3.01 25.80 26.62 o 6 11 0 328.94 610.84 73.05 o 7 11 0 191.26 195.36 38.76 o 8 11 0 66.73 123.63 35.71 o 9 11 0 50.24 58.97 45.36 o 0 12 0 477.33 897.39 65.71 o 1 12 0 240.39 520.78 39.08 o 2 12 0 549.49 518.17 37.43 o 3 12 0 1132.63 1275.57 75.68 o 4 12 0 32.10 12.59 32.45 o 5 12 0 510.79 726.01 47.71 o 6 12 0 404.68 326.85 63.15 o 7 12 0 64.84 71.92 45.67 o 8 12 0 134.78 134.38 44.64 o 1 13 0 1848.25 2585.84 76.57 o 2 13 0 4.53 89.66 35.86 o 3 13 0 495.28 551.47 46.63 o 4 13 0 93.64 114.96 38.13 o 5 13 0 77.73 80.05 41.91 o 6 13 0 64.80 162.28 45.92 o 7 13 0 70.92 153.68 49.89 o 0 14 0 120.06 168.44 63.31 o 1 14 0 36.67 8.90 47.80 o 2 14 0 156.20 155.07 42.79 o 3 14 0 84.17 65.50 41.51 o 4 14 0 28.65 66.82 41.03 o 5 14 0 0.90 11.66 43.22 o 1 15 0 952.96 1068.17 85.76 o 2 15 0 251.49 224.19 50.37 o 3 15 0 1151.52 1238.21 83.11 o 4 15 0 3.66 53.00 51.97 o -11 0 1 832.50 816.96 56.45 o -9 0 1 142.94 122.38 32.08 o -7 0 1 511.01 394.43 33.28 o -5 0 1 601.48 647.90 51.73 o -3 0 1 5279.14 4603.36 78.56 o -1 0 1 512.69 381.46 8.52 o 1 0 1 1591.03 1263.28 19.33 o 3 0 1 14797.22 12253.48 210.43 o 5 0 1 851.29 921.63 46.46 o 7 0 1 1233.59 1019.84 39.84 o 9 0 1 843.35 801.97 49.45 o 11 0 1 117.34 176.91 39.60 o -12 1 1 444.53 591.58 50.46 o -11 1 1 7.91 92.45 40.80 o -10 1 1 112.85 128.59 24.53 o -9 1 1 882.64 1104.74 37.67 o -8 1 1 2820.54 2694.41 50.39 o -7 1 1 1684.53 2075.66 39.92 o -6 1 1 1228.83 1924.20 55.43 o -5 1 1 4.32 388.01 66.44 o -4 1 1 226.08 357.01 19.90 o -3 1 1 27699.68 26840.72 306.77 o -2 1 1 1366.39 1591.70 31.39 o -1 1 1 4902.39 4670.17 56.21 o 0 1 1 9576.75 10345.18 154.63 o 1 1 1 14783.03 14791.52 220.93 o 2 1 1 18394.26 17722.07 176.59 o 3 1 1 1745.68 2274.11 121.62 o 4 1 1 4122.86 4267.07 65.45 o 5 1 1 1044.87 1295.43 59.54 o 6 1 1 205.35 478.81 29.98 o 7 1 1 71.58 231.67 21.71 o 8 1 1 712.74 823.21 31.37 o 9 1 1 1811.51 1777.28 49.95 o 10 1 1 54.74 70.31 25.33 o 11 1 1 440.56 531.00 37.11 o 12 1 1 165.08 206.82 37.88 o -12 2 1 136.60 100.95 40.44 o -11 2 1 1295.46 1482.64 74.57 o -10 2 1 72.62 71.35 23.67 o -9 2 1 1286.08 1351.67 42.92 o -8 2 1 89.34 241.28 20.98 o -7 2 1 5037.45 5221.25 73.36 o -6 2 1 763.21 1017.09 34.91 o -5 2 1 1747.01 2068.10 33.00 o -4 2 1 3559.20 3880.41 48.98 o -3 2 1 18476.54 19567.21 212.36 o -2 2 1 46158.30 46215.80 469.30 o -1 2 1 957.78 847.17 11.70 o 0 2 1 18457.27 23391.95 243.01 o 1 2 1 88764.84 95535.92 1155.85 o 2 2 1 373.47 758.48 74.06 o 3 2 1 29588.76 30911.50 313.68 o 4 2 1 17565.17 17930.39 196.60 o 5 2 1 154.31 341.29 31.04 o 6 2 1 404.15 563.63 32.56 o 7 2 1 343.73 574.50 34.41 o 8 2 1 2049.04 1749.53 41.39 o 9 2 1 852.58 910.65 36.80 o 10 2 1 337.95 331.22 29.28 o 11 2 1 343.68 578.80 47.08 o 12 2 1 24.34 26.12 42.04 o -12 3 1 13.57 22.10 36.44 o -11 3 1 82.53 148.53 52.73 o -10 3 1 850.43 874.16 47.89 o -9 3 1 3.02 159.83 23.40 o -8 3 1 106.74 429.04 29.40 o -7 3 1 479.38 576.11 20.19 o -6 3 1 609.65 1875.73 96.74 o -5 3 1 2429.13 2850.07 58.26 o -4 3 1 784.80 816.65 33.71 o -3 3 1 6986.18 7382.67 134.02 o -2 3 1 11143.46 12068.22 152.56 o -1 3 1 2553.58 3147.79 65.33 o 0 3 1 2468.66 2817.05 33.35 o 1 3 1 9512.54 10817.95 174.23 o 2 3 1 261.07 356.53 31.52 o 3 3 1 25398.69 26168.36 333.94 o 4 3 1 14.25 204.43 39.33 o 5 3 1 103.57 502.16 61.07 o 6 3 1 1552.21 2329.17 62.36 o 7 3 1 514.31 619.40 25.03 o 8 3 1 425.09 452.69 24.66 o 9 3 1 617.81 632.34 32.66 o 10 3 1 65.42 134.79 27.21 o 11 3 1 4.29 31.99 33.45 o 12 3 1 283.40 372.34 46.71 o -12 4 1 236.01 177.20 41.95 o 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o -2 8 1 44.30 139.71 18.43 o -1 8 1 34.26 34.67 12.98 o 0 8 1 61.93 293.26 47.42 o 1 8 1 281.83 322.39 17.96 o 2 8 1 12.27 429.03 48.24 o 3 8 1 842.48 1380.38 91.31 o 4 8 1 432.99 566.47 28.63 o 5 8 1 81.02 329.23 35.96 o 6 8 1 281.38 437.35 28.86 o 7 8 1 23.88 25.69 23.15 o 8 8 1 6.07 47.76 32.93 o 9 8 1 85.49 49.30 28.79 o 10 8 1 105.90 134.72 38.19 o 11 8 1 2.61 263.10 164.77 o -10 9 1 7.12 -33.09 43.93 o -9 9 1 254.52 320.16 40.28 o -8 9 1 80.62 64.58 40.09 o -7 9 1 5.76 172.35 29.45 o -6 9 1 722.35 744.53 39.15 o -5 9 1 855.08 953.75 38.57 o -4 9 1 816.71 1079.93 52.21 o -3 9 1 331.58 492.73 26.28 o -2 9 1 506.73 750.71 35.97 o -1 9 1 141.46 126.96 16.08 o 0 9 1 3872.16 4512.83 81.68 o 1 9 1 11.73 33.34 17.67 o 2 9 1 186.43 321.62 19.30 o 3 9 1 3079.37 3034.42 55.54 o 4 9 1 1310.22 1786.94 74.17 o 5 9 1 1098.74 1411.89 43.53 o 6 9 1 798.73 869.03 50.44 o 7 9 1 1505.06 1465.18 54.39 o 8 9 1 39.99 85.94 31.65 o 9 9 1 310.00 361.36 44.37 o 10 9 1 109.40 50.98 37.51 o -9 10 1 363.68 323.41 42.54 o -8 10 1 179.76 149.66 42.65 o -7 10 1 187.28 153.65 33.15 o -6 10 1 392.56 404.79 37.62 o -5 10 1 28.59 134.01 26.23 o -4 10 1 302.06 399.20 30.69 o -3 10 1 26.71 444.04 48.63 o -2 10 1 5941.48 6354.98 101.74 o -1 10 1 2531.07 3061.69 65.78 o 0 10 1 661.83 756.52 29.19 o 1 10 1 329.33 475.79 25.71 o 2 10 1 1116.19 1292.78 42.24 o 3 10 1 2206.99 2503.32 59.54 o 4 10 1 1130.51 1133.74 43.47 o 5 10 1 548.17 586.15 35.35 o 6 10 1 311.53 308.60 34.77 o 7 10 1 81.61 36.27 29.13 o 8 10 1 142.76 180.46 35.23 o 9 10 1 23.27 55.59 36.08 o -9 11 1 101.89 -1.62 41.66 o -8 11 1 140.73 114.72 37.64 o -7 11 1 81.61 77.30 35.03 o -6 11 1 1340.51 1598.73 65.28 o -5 11 1 54.38 32.60 26.52 o -4 11 1 408.65 432.94 33.44 o -3 11 1 1368.22 1675.46 59.89 o -2 11 1 1.62 343.99 45.80 o -1 11 1 554.86 640.50 37.34 o 0 11 1 6573.81 8186.36 135.56 o 1 11 1 51.55 18.99 24.39 o 2 11 1 106.73 111.03 27.07 o 3 11 1 0.01 159.14 29.54 o 4 11 1 0.00 65.66 30.50 o 5 11 1 98.44 85.31 30.23 o 6 11 1 411.93 606.80 47.74 o 7 11 1 0.33 41.22 33.04 o 8 11 1 46.31 130.09 37.51 o 9 11 1 16.60 7.11 38.01 o -8 12 1 107.05 124.71 52.03 o -7 12 1 10.96 -4.79 40.67 o -6 12 1 120.14 127.34 57.28 o -5 12 1 44.52 71.99 32.94 o -4 12 1 56.89 30.33 30.06 o -3 12 1 209.77 301.03 43.38 o -2 12 1 20.20 10.69 28.60 o -1 12 1 7.09 349.96 34.54 o 0 12 1 90.40 153.68 32.15 o 1 12 1 182.45 337.22 35.14 o 2 12 1 337.96 409.70 35.45 o 3 12 1 153.35 315.09 35.36 o 4 12 1 307.89 284.28 35.36 o 5 12 1 3.88 64.21 33.01 o 6 12 1 284.66 239.85 47.98 o 7 12 1 44.96 5.45 42.78 o 8 12 1 9.01 38.35 39.91 o -7 13 1 0.94 39.83 45.87 o -6 13 1 346.55 315.05 51.68 o -5 13 1 12.06 120.24 44.28 o -4 13 1 350.81 290.69 38.68 o -3 13 1 28.06 93.75 32.56 o -2 13 1 738.47 887.31 53.48 o -1 13 1 484.61 643.90 43.97 o 0 13 1 1592.39 1951.86 67.14 o 1 13 1 888.03 1262.41 59.69 o 2 13 1 178.24 193.97 37.94 o 3 13 1 1020.47 1169.41 77.29 o 4 13 1 62.78 58.17 35.36 o 5 13 1 1434.43 1213.19 68.54 o 6 13 1 4.95 16.72 44.76 o 7 13 1 1215.55 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