#------------------------------------------------------------------------------ #$Date: 2024-02-09 05:15:12 +0200 (Fri, 09 Feb 2024) $ #$Revision: 289767 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/02/30/2023027.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2023027 _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 12.4094 _cell_length_b 15.9871 _cell_length_c 21.9629 _exptl_crystal_F_000 1840.00 _reflns_d_resolution_high 0.6992 _cod_data_source_file jy2044IIIsup4.hkl _cod_data_source_block III _shelx_title ' (III) in Pbca' _shelx_refln_list_code 4 _shelx_f_calc_maximum 247.80 _shelx_f_squared_multiplier 1.000 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z' '-x, -y, -z' 'x-1/2, y, -z-1/2' 'x, -y-1/2, z-1/2' '-x-1/2, y-1/2, z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 4 0 0 24618.91 20282.05 1834.19 o 6 0 0 6357.39 5803.65 608.18 o 8 0 0 7114.08 6749.61 707.70 o 10 0 0 6321.01 6110.97 641.93 o 12 0 0 191.54 301.25 62.87 o 14 0 0 1458.87 1549.65 252.47 o 16 0 0 487.77 904.12 203.09 o 2 1 0 45773.04 37142.92 6727.84 o 4 1 0 3471.34 2950.51 220.30 o 6 1 0 2893.67 2778.33 193.49 o 8 1 0 403.48 451.49 36.45 o 10 1 0 709.80 699.86 67.17 o 12 1 0 54.66 84.88 19.97 o 14 1 0 1195.00 1229.77 133.30 o 16 1 0 382.06 412.42 58.90 o 0 2 0 294.32 411.64 53.44 o 2 2 0 28936.41 24587.02 2560.91 o 4 2 0 72.20 89.91 11.50 o 6 2 0 6151.65 5860.50 481.79 o 8 2 0 3.78 6.66 6.74 o 10 2 0 867.29 951.05 88.27 o 12 2 0 433.15 437.10 47.75 o 14 2 0 94.81 128.59 28.99 o 16 2 0 12.18 19.91 57.82 o 2 3 0 35955.80 33768.03 3532.32 o 4 3 0 9283.57 10149.11 920.06 o 6 3 0 147.28 341.93 31.65 o 8 3 0 10024.34 10140.52 753.04 o 10 3 0 1340.44 1280.05 105.13 o 12 3 0 1415.07 1449.38 120.48 o 14 3 0 4.15 21.97 13.38 o 16 3 0 390.08 523.44 71.51 o 2 4 0 5813.52 5863.17 476.08 o 4 4 0 625.33 650.95 59.02 o 6 4 0 374.94 341.37 31.80 o 8 4 0 425.95 491.21 51.88 o 10 4 0 1.65 12.60 8.41 o 12 4 0 206.11 195.26 27.79 o 14 4 0 472.66 539.47 57.71 o 16 4 0 364.92 360.99 57.34 o 2 5 0 20258.83 21577.88 1739.34 o 4 5 0 406.01 676.78 60.03 o 6 5 0 0.11 22.69 8.83 o 8 5 0 64.17 79.67 13.14 o 10 5 0 52.48 53.48 13.37 o 12 5 0 410.49 404.35 47.99 o 14 5 0 969.95 1024.06 91.11 o 16 5 0 83.71 72.11 17.84 o 0 6 0 4.51 85.68 23.08 o 2 6 0 335.00 392.63 29.66 o 4 6 0 795.82 1007.52 79.28 o 6 6 0 1729.30 1757.09 137.08 o 8 6 0 3246.77 3140.73 240.51 o 10 6 0 1589.85 1585.80 120.92 o 12 6 0 1120.51 1215.34 104.73 o 14 6 0 3.54 16.99 12.84 o 16 6 0 213.50 260.94 50.80 o 2 7 0 2061.53 2462.29 184.02 o 4 7 0 20.23 25.21 6.53 o 6 7 0 80.96 71.85 10.97 o 8 7 0 109.50 77.27 19.81 o 10 7 0 91.71 91.71 15.67 o 12 7 0 428.06 431.17 41.91 o 14 7 0 47.99 41.45 24.89 o 16 7 0 71.22 85.89 25.86 o 0 8 0 52.82 70.91 13.04 o 2 8 0 786.03 902.76 70.04 o 4 8 0 37.91 40.71 7.60 o 6 8 0 3435.74 3587.82 270.86 o 8 8 0 3267.31 3517.68 246.72 o 10 8 0 67.60 102.33 21.01 o 12 8 0 1834.73 1906.95 158.54 o 14 8 0 169.68 193.94 24.88 o 16 8 0 43.87 45.63 17.67 o 2 9 0 65.83 87.59 12.99 o 4 9 0 199.49 260.71 26.18 o 6 9 0 80.49 152.27 17.45 o 8 9 0 1229.24 1183.78 88.70 o 10 9 0 87.96 63.43 11.24 o 12 9 0 325.81 394.58 39.87 o 14 9 0 28.47 14.76 11.78 o 16 9 0 530.72 750.35 92.26 o 0 10 0 941.68 1256.91 118.49 o 2 10 0 2593.06 3025.54 227.44 o 4 10 0 928.79 1097.00 85.90 o 6 10 0 2259.27 2377.61 182.35 o 8 10 0 3253.12 3054.16 231.39 o 10 10 0 409.70 386.79 37.78 o 12 10 0 819.21 824.50 76.28 o 14 10 0 516.66 557.08 52.78 o 2 11 0 0.16 -3.85 5.31 o 4 11 0 6257.14 6638.33 603.01 o 6 11 0 0.19 10.63 8.66 o 8 11 0 988.37 966.55 81.46 o 10 11 0 1003.25 986.03 89.89 o 12 11 0 6.61 22.92 10.92 o 14 11 0 37.74 32.85 44.17 o 0 12 0 3312.15 2956.30 315.11 o 2 12 0 12.14 8.83 8.40 o 4 12 0 1846.89 1766.63 136.75 o 6 12 0 14.51 12.85 14.79 o 8 12 0 2457.41 2519.89 196.52 o 10 12 0 26.74 25.95 14.98 o 12 12 0 303.01 284.11 30.72 o 14 12 0 295.47 332.56 42.86 o 2 13 0 2317.76 2124.09 198.94 o 4 13 0 192.22 228.65 36.02 o 6 13 0 2281.44 2282.59 244.12 o 8 13 0 2308.80 2548.77 209.71 o 10 13 0 1819.45 1740.07 145.56 o 12 13 0 50.03 73.44 44.32 o 14 13 0 275.50 266.52 35.22 o 0 14 0 448.69 534.80 65.64 o 2 14 0 556.67 545.04 69.59 o 4 14 0 86.48 78.26 13.48 o 6 14 0 66.26 67.44 16.53 o 8 14 0 14.99 16.40 14.50 o 10 14 0 264.48 232.66 32.80 o 12 14 0 104.68 115.77 22.52 o 14 14 0 731.87 772.45 99.44 o 2 15 0 10.70 5.54 7.30 o 4 15 0 0.73 2.84 7.89 o 6 15 0 483.63 613.54 62.03 o 8 15 0 29.62 34.44 10.66 o 10 15 0 464.41 586.65 95.76 o 0 16 0 2138.73 2293.43 304.33 o 2 16 0 38.67 20.84 9.97 o 4 16 0 59.65 62.54 16.24 o 6 16 0 205.60 173.56 36.64 o 8 16 0 5.70 8.02 15.06 o 10 16 0 413.00 404.78 72.70 o 12 16 0 64.10 65.71 27.87 o 2 17 0 56.44 45.48 12.14 o 4 17 0 6.54 4.06 9.70 o 6 17 0 1306.36 1108.66 108.95 o 8 17 0 1916.19 1868.57 201.82 o 10 17 0 441.12 365.89 79.40 o 0 18 0 289.68 364.19 65.12 o 2 18 0 416.02 390.93 52.66 o 4 18 0 320.85 253.37 41.87 o 6 18 0 139.83 120.91 39.98 o 8 18 0 7.74 -1.24 21.10 o 10 18 0 538.48 554.90 84.09 o 2 19 0 1252.84 1432.12 139.13 o 4 19 0 49.73 62.20 41.47 o 6 19 0 197.62 134.74 42.41 o 8 19 0 48.43 55.43 23.54 o 0 20 0 50.39 8.89 22.57 o 2 20 0 623.61 613.63 69.35 o 4 20 0 814.91 537.68 93.83 o 6 20 0 124.46 169.90 38.79 o 8 20 0 73.94 99.30 47.22 o 2 21 0 517.79 547.82 64.84 o 4 21 0 3.04 17.01 20.50 o 6 21 0 3.21 22.91 21.98 o 0 22 0 926.67 1011.24 153.52 o 2 22 0 655.97 634.28 76.70 o 4 22 0 20.09 5.94 29.83 o 1 1 1 8588.77 7440.00 602.86 o 2 1 1 723.94 608.51 38.81 o 3 1 1 81.41 61.44 5.34 o 4 1 1 1139.94 983.08 51.92 o 5 1 1 3095.12 3063.28 163.08 o 6 1 1 2236.46 2362.13 127.03 o 7 1 1 12.99 17.42 4.09 o 8 1 1 86.31 159.42 13.05 o 9 1 1 583.93 532.37 32.74 o 10 1 1 378.11 460.30 31.90 o 11 1 1 3215.83 2865.12 169.35 o 12 1 1 295.96 292.00 27.40 o 13 1 1 186.57 184.69 21.15 o 14 1 1 80.59 76.71 21.73 o 15 1 1 25.49 35.42 15.21 o 16 1 1 12.61 14.54 19.02 o 17 1 1 0.19 1.40 19.29 o 0 2 1 21549.71 16764.96 3035.83 o 1 2 1 6.02 3.70 1.81 o 2 2 1 63.13 68.65 6.15 o 3 2 1 116.14 120.29 11.93 o 4 2 1 4128.46 3338.01 231.89 o 5 2 1 551.52 582.31 32.61 o 6 2 1 588.55 684.99 39.50 o 7 2 1 43.43 58.85 8.76 o 8 2 1 2.95 -6.20 6.64 o 9 2 1 1112.88 1158.35 67.40 o 10 2 1 802.99 759.86 48.42 o 11 2 1 4.00 -1.71 7.55 o 12 2 1 340.52 408.51 31.56 o 13 2 1 64.00 85.30 24.33 o 14 2 1 36.51 36.25 15.39 o 15 2 1 109.86 156.06 22.09 o 16 2 1 201.34 259.26 31.09 o 17 2 1 117.67 174.99 27.73 o 1 3 1 8362.60 9555.88 575.08 o 2 3 1 3093.76 2930.99 189.77 o 3 3 1 11.08 5.45 3.43 o 4 3 1 7209.47 7443.77 450.27 o 5 3 1 2266.92 2231.42 148.17 o 6 3 1 6390.11 6422.43 354.78 o 7 3 1 62.60 77.28 8.66 o 8 3 1 13.81 13.58 6.45 o 9 3 1 252.95 274.04 21.13 o 10 3 1 64.11 64.40 8.79 o 11 3 1 43.29 68.85 12.13 o 12 3 1 1195.97 1125.76 68.69 o 13 3 1 127.19 127.92 22.90 o 14 3 1 439.05 496.40 38.76 o 15 3 1 0.36 11.85 11.55 o 16 3 1 234.89 304.67 34.76 o 17 3 1 22.13 8.69 37.18 o 0 4 1 753.15 841.09 58.52 o 1 4 1 1039.05 1308.63 66.25 o 2 4 1 5914.02 6477.97 391.45 o 3 4 1 6.97 0.35 2.35 o 4 4 1 3.95 7.20 2.92 o 5 4 1 199.27 199.60 15.21 o 6 4 1 7579.81 7329.61 404.13 o 7 4 1 1827.03 1879.58 107.97 o 8 4 1 83.84 42.87 6.33 o 9 4 1 2204.65 2142.96 119.25 o 10 4 1 184.05 224.08 19.42 o 11 4 1 1125.59 1129.77 67.66 o 12 4 1 788.49 772.24 49.82 o 13 4 1 646.36 670.18 45.69 o 14 4 1 14.84 12.81 9.67 o 15 4 1 142.70 130.95 27.22 o 16 4 1 234.14 253.70 25.48 o 17 4 1 2.01 26.14 29.11 o 1 5 1 19632.37 22732.21 1450.18 o 2 5 1 2997.05 3214.73 184.02 o 3 5 1 447.53 519.26 29.83 o 4 5 1 3105.36 3446.64 201.34 o 5 5 1 2661.17 2642.45 148.29 o 6 5 1 250.04 199.24 15.19 o 7 5 1 24.08 36.96 6.01 o 8 5 1 224.07 254.37 19.02 o 9 5 1 429.30 368.71 24.80 o 10 5 1 694.38 617.76 37.61 o 11 5 1 339.56 336.98 24.66 o 12 5 1 17.33 21.19 8.30 o 13 5 1 9.49 -4.07 11.01 o 14 5 1 186.92 154.27 17.64 o 15 5 1 60.95 62.90 18.82 o 16 5 1 48.81 78.97 27.33 o 17 5 1 12.12 7.73 33.11 o 0 6 1 6710.57 7787.73 531.65 o 1 6 1 3151.37 3598.65 174.13 o 2 6 1 883.32 971.91 49.83 o 3 6 1 523.45 546.27 28.69 o 4 6 1 2412.74 3073.72 178.79 o 5 6 1 70.63 70.62 7.82 o 6 6 1 3.47 5.03 3.14 o 7 6 1 0.53 8.97 4.58 o 8 6 1 49.66 68.74 10.80 o 9 6 1 857.21 856.51 49.28 o 10 6 1 251.14 240.97 18.93 o 11 6 1 146.73 196.21 17.25 o 12 6 1 18.08 12.46 12.47 o 13 6 1 8.09 17.85 15.42 o 14 6 1 76.64 121.14 13.95 o 15 6 1 2.52 7.74 18.10 o 16 6 1 2.86 20.67 22.32 o 17 6 1 119.05 130.08 21.84 o 1 7 1 193.44 298.76 18.26 o 2 7 1 4061.10 4685.73 282.98 o 3 7 1 2.90 26.90 7.43 o 4 7 1 0.03 -0.22 4.60 o 5 7 1 831.55 812.26 48.22 o 6 7 1 0.01 -3.52 5.96 o 7 7 1 548.18 589.52 34.46 o 8 7 1 85.71 94.37 14.32 o 9 7 1 1193.52 1274.42 73.76 o 10 7 1 7.98 13.14 7.28 o 11 7 1 757.48 699.88 41.96 o 12 7 1 332.02 282.29 22.06 o 13 7 1 47.64 24.13 8.90 o 14 7 1 6.55 -1.40 7.53 o 15 7 1 7.97 11.48 11.13 o 16 7 1 9.75 3.15 16.73 o 0 8 1 14.99 24.71 5.24 o 1 8 1 2545.72 3053.77 169.10 o 2 8 1 0.03 2.92 7.99 o 3 8 1 2649.56 3040.06 198.82 o 4 8 1 456.59 519.75 28.92 o 5 8 1 638.65 721.98 41.53 o 6 8 1 675.80 681.93 39.73 o 7 8 1 846.31 833.91 46.90 o 8 8 1 126.18 177.35 13.77 o 9 8 1 2365.85 2453.31 124.35 o 10 8 1 1534.16 1409.70 78.37 o 11 8 1 56.03 51.03 9.02 o 12 8 1 130.51 112.74 15.81 o 13 8 1 27.88 19.64 10.06 o 14 8 1 75.71 73.66 18.73 o 15 8 1 38.97 53.36 22.13 o 16 8 1 2.43 2.90 23.25 o 1 9 1 3804.80 4497.71 246.62 o 2 9 1 15.52 19.30 4.56 o 3 9 1 3119.37 3485.30 224.46 o 4 9 1 7.66 21.88 4.60 o 5 9 1 0.48 4.69 3.30 o 6 9 1 128.09 112.53 13.59 o 7 9 1 2.67 2.84 5.28 o 8 9 1 506.48 455.41 30.03 o 9 9 1 28.19 15.79 5.29 o 10 9 1 2031.33 1877.25 104.76 o 11 9 1 90.80 95.91 11.34 o 12 9 1 134.40 119.00 11.80 o 13 9 1 147.55 146.90 14.01 o 14 9 1 6.10 19.63 15.85 o 15 9 1 50.55 60.28 15.86 o 16 9 1 1.07 8.40 20.95 o 0 10 1 343.36 566.56 39.32 o 1 10 1 4625.59 5022.39 289.30 o 2 10 1 2928.22 3409.00 188.35 o 3 10 1 3018.42 3398.24 207.54 o 4 10 1 1154.81 1239.92 66.79 o 5 10 1 351.91 361.54 22.32 o 6 10 1 785.91 836.46 50.61 o 7 10 1 20.28 14.56 5.75 o 8 10 1 3397.43 3225.67 167.29 o 9 10 1 177.64 154.74 17.10 o 10 10 1 49.52 44.55 8.60 o 11 10 1 5.76 0.20 8.32 o 12 10 1 583.19 585.60 37.81 o 13 10 1 146.86 148.28 14.57 o 14 10 1 8.47 -3.55 13.48 o 15 10 1 45.77 59.25 25.29 o 1 11 1 478.84 485.64 28.81 o 2 11 1 126.37 152.06 11.68 o 3 11 1 145.09 127.68 10.72 o 4 11 1 53.04 73.66 8.84 o 5 11 1 361.82 330.06 23.37 o 6 11 1 241.73 229.21 20.29 o 7 11 1 943.59 954.26 54.76 o 8 11 1 248.52 310.36 22.93 o 9 11 1 516.13 567.89 35.62 o 10 11 1 35.52 39.50 10.06 o 11 11 1 1006.83 934.81 56.34 o 12 11 1 49.16 43.52 13.32 o 13 11 1 214.99 190.91 18.79 o 14 11 1 22.45 18.26 12.04 o 15 11 1 42.97 26.19 36.65 o 0 12 1 125.08 145.26 19.60 o 1 12 1 526.68 535.43 32.38 o 2 12 1 1830.96 1953.45 110.27 o 3 12 1 483.96 387.60 28.54 o 4 12 1 103.97 124.67 16.80 o 5 12 1 582.01 562.66 38.64 o 6 12 1 497.70 528.75 39.51 o 7 12 1 1147.85 1176.81 76.10 o 8 12 1 87.74 101.00 11.58 o 9 12 1 737.26 642.73 41.57 o 10 12 1 107.29 101.79 13.44 o 11 12 1 175.77 175.39 18.88 o 12 12 1 10.18 32.26 15.72 o 13 12 1 0.31 4.01 15.23 o 14 12 1 3.41 -8.63 37.94 o 15 12 1 101.69 108.56 15.92 o 1 13 1 110.68 139.82 15.69 o 2 13 1 3644.16 3451.10 200.90 o 3 13 1 17.60 12.71 6.75 o 4 13 1 1369.45 1331.16 83.95 o 5 13 1 25.71 35.93 11.34 o 6 13 1 851.33 995.52 58.06 o 7 13 1 219.07 187.82 20.83 o 8 13 1 459.50 439.49 34.07 o 9 13 1 3.24 7.54 5.82 o 10 13 1 96.88 70.12 9.30 o 11 13 1 92.45 111.50 21.79 o 12 13 1 273.74 254.44 23.17 o 13 13 1 3.81 -10.79 20.31 o 14 13 1 11.18 -1.86 24.75 o 0 14 1 88.76 73.51 18.07 o 1 14 1 1613.59 1476.88 88.13 o 2 14 1 1508.27 1498.47 93.44 o 3 14 1 3841.93 3828.13 248.75 o 4 14 1 1439.57 1371.74 91.58 o 5 14 1 143.02 131.04 22.70 o 6 14 1 15.02 24.37 6.54 o 7 14 1 90.45 110.80 20.85 o 8 14 1 39.99 31.74 13.68 o 9 14 1 6.48 8.83 6.15 o 10 14 1 26.73 26.38 9.59 o 11 14 1 57.73 68.42 15.03 o 12 14 1 700.75 798.76 69.99 o 13 14 1 43.72 41.93 21.83 o 14 14 1 624.32 570.81 67.10 o 1 15 1 96.24 76.55 11.89 o 2 15 1 1265.33 1296.02 81.68 o 3 15 1 4.42 1.70 7.56 o 4 15 1 1479.54 1537.10 101.36 o 5 15 1 4.55 8.95 6.71 o 6 15 1 1037.16 1106.78 71.36 o 7 15 1 79.17 51.22 13.09 o 8 15 1 88.75 67.39 13.79 o 9 15 1 7.42 26.47 8.42 o 10 15 1 1562.66 1675.48 110.42 o 11 15 1 146.10 98.39 30.92 o 12 15 1 367.36 326.92 28.53 o 13 15 1 325.64 296.37 32.35 o 0 16 1 71.10 56.66 12.89 o 1 16 1 24.86 6.11 6.53 o 2 16 1 867.57 891.59 55.10 o 3 16 1 694.97 770.40 48.71 o 4 16 1 1692.58 1562.95 102.95 o 5 16 1 475.22 445.91 35.20 o 6 16 1 47.40 51.15 12.15 o 7 16 1 65.78 83.84 11.43 o 8 16 1 237.65 231.97 29.07 o 9 16 1 93.88 70.82 21.58 o 10 16 1 0.06 0.57 12.18 o 11 16 1 5.75 -1.89 10.71 o 12 16 1 2.83 -5.36 18.91 o 1 17 1 135.19 133.12 19.57 o 2 17 1 333.16 306.78 29.15 o 3 17 1 338.27 373.27 30.13 o 4 17 1 99.24 65.77 12.02 o 5 17 1 376.45 314.01 34.28 o 6 17 1 50.42 45.52 22.23 o 7 17 1 21.78 25.32 8.90 o 8 17 1 121.03 133.97 31.04 o 9 17 1 84.66 98.33 18.10 o 10 17 1 128.06 104.91 20.63 o 11 17 1 18.33 5.87 19.37 o 0 18 1 697.29 650.53 72.29 o 1 18 1 275.84 282.37 24.18 o 2 18 1 0.04 6.16 8.41 o 3 18 1 172.40 149.74 25.87 o 4 18 1 121.87 129.18 24.44 o 5 18 1 127.04 111.51 20.87 o 6 18 1 90.17 146.06 24.50 o 7 18 1 10.84 7.42 12.12 o 8 18 1 23.49 8.75 21.20 o 9 18 1 28.70 10.90 22.97 o 10 18 1 1.94 4.91 14.26 o 1 19 1 25.85 21.48 9.62 o 2 19 1 830.91 852.74 61.77 o 3 19 1 0.12 20.55 16.29 o 4 19 1 139.69 106.80 22.99 o 5 19 1 161.89 142.19 39.12 o 6 19 1 53.24 31.81 12.92 o 7 19 1 200.03 224.07 38.97 o 8 19 1 211.48 292.75 61.93 o 9 19 1 3.75 -29.17 29.17 o 0 20 1 23.17 55.39 24.23 o 1 20 1 2.18 7.48 10.29 o 2 20 1 29.36 32.83 18.06 o 3 20 1 171.89 168.00 21.59 o 4 20 1 0.17 -17.47 24.25 o 5 20 1 52.86 16.39 12.66 o 6 20 1 34.54 43.64 17.69 o 7 20 1 186.16 184.96 28.79 o 8 20 1 223.59 265.08 42.26 o 1 21 1 88.78 104.47 18.18 o 2 21 1 87.15 63.35 19.98 o 3 21 1 157.74 168.04 22.26 o 4 21 1 0.05 -0.04 16.56 o 5 21 1 1.45 -0.18 13.50 o 6 21 1 109.28 120.99 19.99 o 0 22 1 23.17 84.00 57.17 o 1 22 1 60.29 54.73 20.22 o 2 22 1 6.62 44.97 24.91 o 3 22 1 0.00 28.61 16.42 o 4 22 1 170.03 146.06 23.08 o 0 0 2 43779.89 42134.94 7742.66 o 1 0 2 4031.59 2885.21 524.08 o 2 0 2 19092.45 15650.87 1266.73 o 3 0 2 745.74 717.40 56.04 o 4 0 2 3752.50 3069.87 213.05 o 5 0 2 324.73 306.77 25.23 o 6 0 2 2986.92 2544.11 178.01 o 7 0 2 2940.17 2665.19 201.35 o 8 0 2 17.75 22.37 8.10 o 9 0 2 309.66 348.45 37.74 o 10 0 2 564.36 576.75 55.77 o 11 0 2 289.96 360.77 40.09 o 12 0 2 29.06 56.41 14.80 o 13 0 2 257.33 317.43 54.48 o 14 0 2 123.15 146.94 29.10 o 15 0 2 4.06 -4.33 28.87 o 16 0 2 127.71 171.91 54.53 o 17 0 2 1022.08 1190.15 138.82 o 1 1 2 1859.81 1545.99 115.15 o 2 1 2 930.58 761.37 48.13 o 3 1 2 9795.74 7946.52 480.11 o 4 1 2 0.74 -0.52 3.07 o 5 1 2 1800.87 1649.40 90.30 o 6 1 2 254.18 318.92 19.87 o 7 1 2 873.54 994.43 56.36 o 8 1 2 112.30 130.45 11.47 o 9 1 2 3794.87 3341.58 198.25 o 10 1 2 37.66 34.28 8.13 o 11 1 2 6.70 7.98 6.13 o 12 1 2 53.02 84.28 13.45 o 13 1 2 46.94 49.31 24.33 o 14 1 2 78.87 44.94 21.21 o 15 1 2 580.63 708.54 62.02 o 16 1 2 38.13 36.84 16.39 o 17 1 2 28.37 49.48 30.76 o 0 2 2 1334.24 1257.72 94.04 o 1 2 2 1537.29 1573.54 102.07 o 2 2 2 15490.20 13898.16 948.38 o 3 2 2 1763.64 1729.58 101.74 o 4 2 2 1838.61 1690.33 94.91 o 5 2 2 11044.89 10534.92 677.77 o 6 2 2 989.98 997.99 54.27 o 7 2 2 3515.47 3647.00 195.04 o 8 2 2 1029.25 972.88 59.47 o 9 2 2 142.34 159.14 13.39 o 10 2 2 493.94 558.14 37.37 o 11 2 2 2269.71 2125.68 122.02 o 12 2 2 1024.21 1054.21 68.61 o 13 2 2 760.72 783.74 59.54 o 14 2 2 2.94 -7.32 17.94 o 15 2 2 11.05 6.23 23.04 o 16 2 2 63.15 55.02 18.23 o 17 2 2 28.16 49.89 51.34 o 1 3 2 26457.40 26413.86 2391.69 o 2 3 2 4063.93 3799.34 244.89 o 3 3 2 4632.23 4442.46 269.97 o 4 3 2 3373.43 2906.28 168.55 o 5 3 2 859.86 952.58 55.85 o 6 3 2 509.54 526.40 33.53 o 7 3 2 1203.59 1185.28 67.53 o 8 3 2 515.41 545.36 35.71 o 9 3 2 86.91 83.93 14.69 o 10 3 2 305.17 355.75 26.50 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689.69 639.13 54.33 o 2 0 12 836.38 992.81 92.73 o 3 0 12 1094.74 1090.26 90.42 o 4 0 12 2139.96 1656.42 139.52 o 5 0 12 313.19 354.69 54.91 o 6 0 12 3175.51 2722.30 291.84 o 7 0 12 4895.23 3605.76 479.50 o 8 0 12 6182.85 5493.96 583.65 o 9 0 12 3903.08 3805.12 414.39 o 10 0 12 84.09 200.13 50.82 o 11 0 12 20.42 57.37 60.83 o 12 0 12 555.24 550.83 80.56 o 13 0 12 501.84 501.70 65.73 o 14 0 12 70.71 30.42 34.15 o 15 0 12 10.93 -24.59 30.98 o 16 0 12 23.40 76.94 107.43 o 1 1 12 129.01 123.10 9.62 o 2 1 12 821.75 870.60 52.42 o 3 1 12 144.46 129.66 10.87 o 4 1 12 0.55 -1.99 4.38 o 5 1 12 153.79 173.27 15.87 o 6 1 12 234.11 361.33 40.26 o 7 1 12 347.83 384.32 40.27 o 8 1 12 713.09 809.75 73.92 o 9 1 12 661.71 628.83 57.43 o 10 1 12 79.16 44.44 16.10 o 11 1 12 120.29 88.28 18.02 o 12 1 12 151.98 90.97 20.83 o 13 1 12 38.42 14.58 25.94 o 14 1 12 153.09 99.09 33.22 o 15 1 12 17.93 -11.05 19.40 o 16 1 12 94.05 -2.76 75.11 o 0 2 12 397.89 410.45 31.28 o 1 2 12 730.81 632.83 35.55 o 2 2 12 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8 22 235.85 239.56 40.26 o 9 8 22 134.41 118.53 46.05 o 10 8 22 50.94 48.02 27.70 o 11 8 22 396.68 472.23 128.40 o 1 9 22 350.40 276.42 31.16 o 2 9 22 4.36 13.73 9.44 o 3 9 22 777.41 842.24 55.01 o 4 9 22 136.17 130.82 15.74 o 5 9 22 38.96 66.27 18.63 o 6 9 22 65.63 66.09 16.88 o 7 9 22 550.95 608.09 59.40 o 8 9 22 10.22 -7.93 25.38 o 9 9 22 117.02 108.55 65.26 o 10 9 22 155.74 240.00 43.71 o 0 10 22 18.54 46.58 38.67 o 1 10 22 18.78 7.93 12.77 o 2 10 22 36.75 35.95 17.42 o 3 10 22 0.03 -3.77 9.70 o 4 10 22 349.19 402.58 35.98 o 5 10 22 13.33 29.96 10.73 o 6 10 22 438.95 436.58 47.13 o 7 10 22 13.40 -3.83 29.89 o 8 10 22 44.82 51.39 25.89 o 9 10 22 1.04 37.85 35.29 o 1 11 22 151.35 138.32 21.76 o 2 11 22 233.79 236.48 24.78 o 3 11 22 7.43 -11.66 13.29 o 4 11 22 135.09 142.44 17.75 o 5 11 22 152.65 187.67 27.24 o 6 11 22 4.11 57.72 42.56 o 7 11 22 390.75 376.93 45.39 o 8 11 22 188.95 209.83 54.42 o 9 11 22 3.21 17.73 37.96 o 0 12 22 748.93 577.86 76.75 o 1 12 22 14.43 35.28 13.00 o 2 12 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