#------------------------------------------------------------------------------ #$Date: 2024-02-17 05:09:09 +0200 (Sat, 17 Feb 2024) $ #$Revision: 289860 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/02/30/2023032.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2023032 _cell_angle_alpha 90.000 _cell_angle_beta 97.946 _cell_angle_gamma 90.000 _cell_length_a 8.7831 _cell_length_b 11.6621 _cell_length_c 11.0017 _exptl_crystal_F_000 512.00 _reflns_d_resolution_high 0.7892 _cod_data_source_file yz2050Isup2.hkl _cod_data_source_block I _shelx_title ' elg_ha20 in P2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 169.68 _shelx_f_squared_multiplier 1.000 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 7390.49 7618.10 251.11 o 2 0 0 47.24 53.31 1.40 o 3 0 0 4424.75 4467.05 62.08 o 4 0 0 1198.73 1110.24 14.00 o 5 0 0 2035.87 2061.31 29.96 o 6 0 0 323.41 342.02 3.56 o 7 0 0 802.77 812.78 7.09 o 8 0 0 614.97 642.84 6.10 o 9 0 0 18.11 24.57 0.87 o 10 0 0 5.28 4.43 0.48 o 11 0 0 4.62 4.20 0.81 o 1 1 0 229.77 257.78 4.74 o 2 1 0 392.07 464.54 5.60 o 3 1 0 0.89 2.76 0.52 o 4 1 0 139.03 134.21 1.67 o 5 1 0 1212.90 1237.88 11.64 o 6 1 0 79.08 77.52 0.85 o 7 1 0 28.61 29.34 0.56 o 8 1 0 210.58 205.61 1.91 o 9 1 0 510.54 499.31 5.43 o 10 1 0 203.60 208.27 2.51 o 0 2 0 4.01 6.73 0.90 o 1 2 0 3176.25 3320.93 43.90 o 2 2 0 1350.00 1434.85 15.97 o 3 2 0 74.87 77.33 1.24 o 4 2 0 4018.29 4199.65 31.57 o 5 2 0 878.80 862.22 6.90 o 6 2 0 104.84 120.49 1.10 o 7 2 0 169.43 153.16 1.52 o 8 2 0 179.20 177.48 1.63 o 9 2 0 182.63 171.59 1.77 o 10 2 0 47.10 40.72 0.65 o 1 3 0 494.27 518.15 6.22 o 2 3 0 469.27 460.77 5.61 o 3 3 0 980.07 950.49 12.16 o 4 3 0 1177.98 1312.58 13.89 o 5 3 0 997.63 1022.64 7.90 o 6 3 0 179.09 176.72 1.64 o 7 3 0 20.36 18.12 0.43 o 8 3 0 4.33 3.37 0.33 o 9 3 0 54.69 57.62 0.84 o 10 3 0 19.06 19.70 0.59 o 0 4 0 5648.44 5392.42 136.35 o 1 4 0 156.92 121.18 1.80 o 2 4 0 530.96 582.45 6.99 o 3 4 0 512.87 532.57 5.90 o 4 4 0 67.95 57.45 1.28 o 5 4 0 0.20 0.96 0.25 o 6 4 0 22.74 21.89 0.48 o 7 4 0 61.86 59.31 0.81 o 8 4 0 7.22 8.97 0.37 o 9 4 0 59.16 59.06 0.80 o 10 4 0 42.02 37.56 1.09 o 1 5 0 7.20 4.35 0.45 o 2 5 0 345.11 315.46 3.65 o 3 5 0 45.77 64.36 1.09 o 4 5 0 160.98 172.32 1.82 o 5 5 0 759.40 739.57 4.94 o 6 5 0 8.62 9.36 0.35 o 7 5 0 19.79 17.96 0.46 o 8 5 0 1.22 1.50 0.32 o 9 5 0 26.85 26.57 0.53 o 10 5 0 118.98 108.46 2.53 o 0 6 0 231.98 276.46 6.95 o 1 6 0 473.48 494.33 6.83 o 2 6 0 17.56 20.67 0.76 o 3 6 0 0.92 2.18 0.35 o 4 6 0 146.04 131.70 1.48 o 5 6 0 368.38 370.84 2.89 o 6 6 0 16.88 16.57 0.48 o 7 6 0 54.56 52.19 0.83 o 8 6 0 124.65 118.52 1.30 o 9 6 0 22.80 20.68 0.51 o 10 6 0 0.17 -0.20 0.31 o 1 7 0 22.33 20.95 0.76 o 2 7 0 2073.43 2148.43 14.14 o 3 7 0 1485.73 1487.72 9.65 o 4 7 0 231.11 215.68 2.08 o 5 7 0 76.95 73.21 0.95 o 6 7 0 173.39 166.76 1.93 o 7 7 0 107.15 107.41 1.26 o 8 7 0 31.59 28.75 0.58 o 9 7 0 20.80 19.61 0.55 o 0 8 0 0.01 2.37 0.33 o 1 8 0 323.02 372.81 2.50 o 2 8 0 1.62 2.03 0.25 o 3 8 0 62.93 57.85 0.76 o 4 8 0 1092.93 1031.11 7.36 o 5 8 0 47.36 41.45 0.70 o 6 8 0 69.19 64.84 1.08 o 7 8 0 64.29 61.69 0.87 o 8 8 0 3.40 3.25 0.32 o 9 8 0 34.00 35.51 0.91 o 1 9 0 127.75 131.49 1.22 o 2 9 0 298.93 282.24 2.17 o 3 9 0 4.39 5.35 0.38 o 4 9 0 288.31 297.31 2.55 o 5 9 0 14.35 13.84 0.53 o 6 9 0 0.05 0.31 0.31 o 7 9 0 37.32 43.16 0.62 o 8 9 0 45.72 39.23 1.18 o 0 10 0 446.50 444.94 4.74 o 1 10 0 232.72 225.10 2.02 o 2 10 0 366.51 348.08 3.11 o 3 10 0 605.08 608.94 5.53 o 4 10 0 290.25 293.28 2.92 o 5 10 0 19.42 18.91 0.57 o 6 10 0 4.10 3.82 0.34 o 7 10 0 34.39 37.31 0.65 o 8 10 0 34.02 31.12 1.14 o 1 11 0 167.34 162.10 1.76 o 2 11 0 286.84 286.60 2.99 o 3 11 0 7.97 7.72 0.44 o 4 11 0 14.24 13.70 0.50 o 5 11 0 100.04 95.63 1.21 o 6 11 0 10.92 10.10 0.40 o 7 11 0 25.53 23.57 0.63 o 0 12 0 394.91 427.59 6.11 o 1 12 0 300.30 315.72 3.72 o 2 12 0 120.47 117.42 1.66 o 3 12 0 4.60 3.26 0.52 o 4 12 0 57.66 63.62 1.02 o 5 12 0 46.73 48.95 1.03 o 6 12 0 0.95 0.60 0.27 o 1 13 0 128.67 129.92 2.45 o 2 13 0 19.55 20.44 0.96 o 3 13 0 3.42 4.20 0.49 o 4 13 0 118.79 125.45 2.53 o 5 13 0 95.40 91.22 2.35 o 0 14 0 5.63 5.73 0.88 o 1 14 0 70.30 66.67 2.50 o 2 14 0 7.44 6.53 0.83 o 3 14 0 184.61 178.56 6.60 o -11 1 1 141.34 117.52 2.24 o -10 1 1 43.17 41.46 0.83 o -9 1 1 8.50 8.39 0.39 o -8 1 1 12.68 11.23 0.40 o -7 1 1 28.14 26.37 0.51 o -6 1 1 326.39 358.96 2.49 o -5 1 1 236.60 233.24 2.28 o -4 1 1 143.82 163.49 1.98 o -3 1 1 892.50 966.88 11.09 o -1 1 1 2399.45 2393.90 27.20 o 0 1 1 1568.84 1702.28 25.98 o 1 1 1 3242.19 3353.69 44.51 o 2 1 1 316.70 353.71 5.01 o 3 1 1 187.43 192.84 2.65 o 4 1 1 244.31 282.48 3.10 o 5 1 1 250.49 276.19 2.91 o 6 1 1 61.55 70.90 0.86 o 7 1 1 88.84 88.71 0.88 o 8 1 1 4.49 3.97 0.33 o 9 1 1 256.93 257.91 2.79 o 10 1 1 23.56 21.24 0.72 o -10 2 1 29.86 30.11 0.58 o -9 2 1 142.92 149.68 2.01 o -8 2 1 12.45 11.42 0.40 o -7 2 1 19.22 20.27 0.51 o -6 2 1 285.74 304.13 2.25 o -5 2 1 17.33 18.36 0.54 o -4 2 1 10.98 12.11 0.46 o -3 2 1 76.85 89.40 2.02 o -2 2 1 4591.50 4798.24 54.24 o -1 2 1 19560.59 18862.09 211.78 o 0 2 1 0.84 0.39 0.36 o 1 2 1 1.62 1.64 0.37 o 2 2 1 971.88 965.07 11.31 o 3 2 1 307.40 325.32 3.57 o 4 2 1 127.31 170.21 1.89 o 5 2 1 1269.80 1358.69 9.43 o 6 2 1 239.81 243.41 1.87 o 7 2 1 126.92 128.86 1.43 o 8 2 1 104.21 104.35 1.09 o 9 2 1 3.53 3.73 0.35 o 10 2 1 114.29 115.36 1.58 o -10 3 1 165.32 155.29 1.80 o -9 3 1 1.21 1.31 0.30 o -8 3 1 93.10 91.44 1.54 o -7 3 1 368.48 381.20 2.82 o -6 3 1 134.04 136.68 1.26 o -5 3 1 247.29 261.20 2.58 o -4 3 1 776.79 776.26 7.89 o -3 3 1 285.99 326.89 6.78 o -2 3 1 33.62 43.40 1.11 o -1 3 1 5070.49 5093.66 52.36 o 0 3 1 131.62 117.39 2.18 o 1 3 1 51.58 50.86 1.11 o 2 3 1 0.31 2.54 0.63 o 3 3 1 239.25 226.76 3.32 o 4 3 1 199.30 215.19 2.63 o 5 3 1 28.08 26.38 0.53 o 6 3 1 271.80 260.33 1.92 o 7 3 1 190.39 186.63 1.60 o 8 3 1 0.08 0.41 0.31 o 9 3 1 254.77 248.04 2.62 o 10 3 1 94.87 80.68 1.60 o -10 4 1 16.72 11.87 0.45 o -9 4 1 14.59 13.97 0.42 o -8 4 1 37.08 38.36 0.73 o -7 4 1 218.19 229.50 2.07 o -6 4 1 100.61 93.99 0.94 o -5 4 1 119.41 131.96 1.27 o -4 4 1 58.19 48.60 1.15 o -3 4 1 158.21 146.16 2.23 o -2 4 1 74.75 70.02 1.73 o -1 4 1 233.85 238.00 3.11 o 0 4 1 2057.57 2148.00 43.73 o 1 4 1 601.81 603.68 6.74 o 2 4 1 1208.33 1222.17 16.99 o 3 4 1 900.73 970.43 9.74 o 4 4 1 640.53 670.13 6.39 o 5 4 1 173.02 147.39 1.27 o 6 4 1 652.97 656.08 4.31 o 7 4 1 27.33 24.96 0.49 o 8 4 1 562.95 531.74 4.30 o 9 4 1 246.75 249.34 3.15 o 10 4 1 10.78 9.11 0.34 o -10 5 1 8.39 7.46 0.39 o -9 5 1 94.70 94.51 1.47 o -8 5 1 508.71 504.99 4.03 o -7 5 1 68.38 63.79 0.90 o -6 5 1 12.08 12.86 0.37 o -5 5 1 458.03 413.31 3.32 o -4 5 1 80.53 67.54 0.99 o -3 5 1 70.31 59.05 1.33 o -2 5 1 16.98 13.09 0.63 o -1 5 1 382.41 353.50 3.91 o 0 5 1 78.67 66.24 1.83 o 1 5 1 1085.28 1210.65 14.32 o 2 5 1 100.53 121.87 1.91 o 3 5 1 489.74 543.64 6.26 o 4 5 1 8.64 13.57 0.39 o 5 5 1 56.76 60.36 0.99 o 6 5 1 91.93 98.29 1.09 o 7 5 1 1.14 1.27 0.30 o 8 5 1 44.10 35.50 0.65 o 9 5 1 0.54 0.70 0.34 o 10 5 1 40.25 32.30 0.95 o -10 6 1 124.23 109.71 2.34 o -9 6 1 12.35 12.49 0.42 o -8 6 1 59.79 59.14 0.85 o -7 6 1 53.05 53.63 0.88 o -6 6 1 364.26 356.29 2.77 o -5 6 1 226.83 225.05 2.25 o -4 6 1 289.33 247.75 2.21 o -3 6 1 16.44 10.92 0.44 o -2 6 1 1556.04 1516.95 16.48 o -1 6 1 887.03 927.15 9.70 o 0 6 1 2.36 3.41 0.58 o 1 6 1 2558.59 2613.64 30.66 o 2 6 1 473.19 425.77 5.75 o 3 6 1 0.55 0.30 0.34 o 4 6 1 694.67 677.85 4.68 o 5 6 1 491.49 481.48 3.60 o 6 6 1 76.01 67.15 1.03 o 7 6 1 26.91 27.47 0.58 o 8 6 1 7.52 7.94 0.42 o 9 6 1 77.43 76.77 1.32 o -9 7 1 9.28 9.93 0.42 o -8 7 1 1.11 1.49 0.29 o -7 7 1 45.99 43.09 0.69 o -6 7 1 158.22 168.51 1.60 o -5 7 1 39.34 36.47 0.65 o -4 7 1 265.43 234.90 2.02 o -3 7 1 36.12 36.49 0.56 o -2 7 1 148.68 150.72 1.42 o -1 7 1 421.89 369.77 3.98 o 0 7 1 214.63 186.03 2.98 o 1 7 1 1.98 1.56 0.38 o 2 7 1 348.93 400.50 3.07 o 3 7 1 1467.74 1434.82 9.32 o 4 7 1 596.36 559.90 4.37 o 5 7 1 29.73 31.59 0.84 o 6 7 1 518.17 510.68 4.19 o 7 7 1 196.15 205.39 2.20 o 8 7 1 55.23 60.07 0.83 o 9 7 1 86.40 76.73 1.35 o -9 8 1 48.74 45.85 1.00 o -8 8 1 2.82 1.88 0.31 o -7 8 1 293.77 288.98 2.56 o -6 8 1 948.18 936.54 7.17 o -5 8 1 817.64 811.68 6.50 o -4 8 1 11.04 10.05 0.44 o -3 8 1 2433.26 2387.85 16.22 o -2 8 1 455.92 451.11 3.42 o -1 8 1 1.78 3.53 0.25 o 0 8 1 133.83 123.97 0.98 o 1 8 1 450.28 432.65 2.89 o 2 8 1 1296.69 1260.80 8.07 o 3 8 1 84.23 81.84 0.84 o 4 8 1 163.52 156.26 1.72 o 5 8 1 85.08 77.12 0.99 o 6 8 1 95.16 85.94 1.12 o 7 8 1 7.19 7.75 0.35 o 8 8 1 235.93 218.34 2.33 o 9 8 1 238.54 211.58 4.25 o -8 9 1 168.24 165.15 1.97 o -7 9 1 111.45 104.06 1.52 o -6 9 1 0.01 0.24 0.34 o -5 9 1 8.32 9.70 0.40 o -4 9 1 831.07 855.58 7.03 o -3 9 1 554.57 576.81 4.67 o -2 9 1 97.18 89.93 1.09 o -1 9 1 447.98 424.03 3.21 o 0 9 1 568.04 562.67 3.92 o 1 9 1 1090.00 1114.86 7.30 o 2 9 1 2.61 3.21 0.30 o 3 9 1 370.34 350.60 2.83 o 4 9 1 378.50 368.01 3.44 o 5 9 1 13.11 10.38 0.46 o 6 9 1 39.54 35.55 0.65 o 7 9 1 290.87 303.14 3.04 o 8 9 1 177.72 168.59 2.43 o -8 10 1 15.55 12.31 0.48 o -7 10 1 21.64 22.92 0.48 o -6 10 1 139.76 152.81 1.69 o -5 10 1 10.28 8.04 0.44 o -4 10 1 85.09 76.65 1.19 o -3 10 1 649.49 621.19 5.26 o -2 10 1 717.85 693.71 5.87 o -1 10 1 405.64 399.57 3.05 o 0 10 1 21.30 20.17 0.50 o 1 10 1 820.00 842.60 6.57 o 2 10 1 195.08 196.83 1.84 o 3 10 1 678.07 666.42 5.24 o 4 10 1 348.46 341.30 3.53 o 5 10 1 675.60 660.55 7.71 o 6 10 1 1.67 1.63 0.33 o 7 10 1 1.18 0.92 0.30 o -7 11 1 47.89 44.00 1.38 o -6 11 1 11.41 11.03 0.45 o -5 11 1 5.01 3.96 0.44 o -4 11 1 65.54 63.40 1.05 o -3 11 1 135.19 130.48 1.46 o -2 11 1 12.56 12.09 0.47 o -1 11 1 266.59 265.88 2.54 o 0 11 1 645.32 637.13 5.54 o 1 11 1 33.18 28.39 0.68 o 2 11 1 93.30 99.61 1.22 o 3 11 1 119.55 127.62 1.73 o 4 11 1 371.60 371.46 4.12 o 5 11 1 51.23 55.40 0.92 o 6 11 1 378.07 376.79 4.16 o 7 11 1 53.93 50.95 1.37 o -6 12 1 333.72 320.44 5.16 o -5 12 1 153.73 161.98 2.34 o -4 12 1 0.29 0.30 0.37 o -3 12 1 28.24 30.92 0.75 o -2 12 1 5.29 5.50 0.45 o -1 12 1 20.28 21.39 0.65 o 0 12 1 70.16 70.47 1.62 o 1 12 1 207.90 206.75 2.38 o 2 12 1 5.57 6.95 0.49 o 3 12 1 31.03 26.19 0.69 o 4 12 1 15.54 12.99 0.55 o 5 12 1 1.14 0.65 0.36 o 6 12 1 30.48 24.65 0.75 o -5 13 1 18.80 14.76 0.72 o -4 13 1 3.54 2.52 0.42 o -3 13 1 17.19 21.68 0.70 o -2 13 1 210.32 211.56 3.32 o -1 13 1 78.14 81.43 1.75 o 0 13 1 4.62 3.41 0.48 o 1 13 1 69.74 64.12 1.31 o 2 13 1 127.60 125.98 3.31 o 3 13 1 57.38 58.54 1.49 o 4 13 1 100.15 102.48 1.79 o 5 13 1 12.73 9.30 0.99 o -3 14 1 18.57 16.43 1.12 o -2 14 1 17.56 18.12 0.96 o -1 14 1 19.33 16.19 1.09 o 0 14 1 9.66 8.20 0.59 o 1 14 1 111.48 112.85 2.60 o 2 14 1 74.64 65.57 2.10 o 3 14 1 26.41 25.18 1.64 o -11 0 2 342.83 276.61 8.35 o -10 0 2 15.65 12.12 0.63 o -9 0 2 0.69 0.83 0.42 o -8 0 2 13.96 14.05 0.65 o -7 0 2 94.18 98.87 1.50 o -6 0 2 1155.22 1200.60 11.90 o -5 0 2 22.48 19.03 0.87 o -4 0 2 160.43 142.01 2.30 o -3 0 2 0.46 3.15 0.57 o -2 0 2 8530.00 8839.94 116.76 o -1 0 2 2546.67 2538.88 39.02 o 0 0 2 1811.83 1813.53 31.50 o 1 0 2 409.62 380.06 7.09 o 2 0 2 7483.30 8064.36 151.11 o 3 0 2 5769.30 5976.36 73.76 o 4 0 2 1005.50 1099.21 13.30 o 5 0 2 98.96 91.99 1.87 o 6 0 2 544.62 513.89 4.94 o 7 0 2 264.06 250.60 2.79 o 8 0 2 88.47 89.72 1.49 o 9 0 2 123.87 122.57 2.09 o 10 0 2 270.07 250.69 8.68 o -11 1 2 0.28 0.75 0.33 o -10 1 2 193.45 202.10 2.85 o -9 1 2 131.67 132.78 1.35 o -8 1 2 4.79 5.18 0.37 o -7 1 2 1211.45 1204.69 9.25 o -6 1 2 1392.42 1373.93 8.89 o -5 1 2 234.17 244.49 2.57 o -4 1 2 1.22 1.45 0.40 o -3 1 2 1690.53 1651.90 15.75 o -2 1 2 27564.71 26917.37 300.07 o -1 1 2 1739.21 1783.86 22.77 o 0 1 2 726.79 642.25 12.42 o 1 1 2 1577.55 1475.89 15.71 o 2 1 2 107.24 94.59 1.66 o 3 1 2 130.31 131.63 1.77 o 4 1 2 433.51 475.49 4.61 o 5 1 2 653.63 674.40 5.01 o 6 1 2 120.13 130.87 1.15 o 7 1 2 600.82 575.79 4.07 o 8 1 2 152.13 152.86 1.51 o 9 1 2 0.55 0.53 0.30 o 10 1 2 0.77 0.29 0.25 o -11 2 2 1.19 1.07 0.39 o -10 2 2 19.02 22.07 0.52 o -9 2 2 113.31 125.67 1.34 o -8 2 2 146.73 149.49 1.59 o -7 2 2 14.96 16.62 0.48 o -6 2 2 0.42 1.32 0.24 o -5 2 2 1179.12 1119.43 9.55 o -4 2 2 77.65 91.15 1.40 o -3 2 2 969.52 923.10 10.25 o -2 2 2 28792.06 28298.88 281.33 o -1 2 2 744.74 744.44 9.57 o 0 2 2 1.66 2.88 0.36 o 1 2 2 450.57 511.28 6.59 o 2 2 2 1572.94 1614.09 17.99 o 3 2 2 2438.80 2466.99 26.10 o 4 2 2 4.68 3.27 0.44 o 5 2 2 108.48 110.61 0.97 o 6 2 2 481.35 512.82 3.54 o 7 2 2 1062.00 1069.88 7.27 o 8 2 2 156.73 157.41 1.49 o 9 2 2 3.33 2.29 0.32 o 10 2 2 7.87 9.48 0.32 o -10 3 2 79.85 82.19 1.13 o -9 3 2 81.32 79.83 1.03 o -8 3 2 38.86 41.16 0.73 o -7 3 2 266.29 255.04 2.04 o -6 3 2 397.09 371.43 3.10 o -5 3 2 325.46 350.54 2.92 o -4 3 2 385.31 429.56 4.47 o -3 3 2 1387.18 1355.27 13.71 o -2 3 2 170.31 143.00 2.23 o -1 3 2 6.70 5.38 0.52 o 0 3 2 1237.79 1282.04 17.07 o 1 3 2 109.95 112.79 1.88 o 2 3 2 611.23 648.43 10.17 o 3 3 2 266.92 293.64 4.69 o 4 3 2 143.20 177.12 2.61 o 5 3 2 4.30 7.87 0.29 o 6 3 2 67.76 65.10 0.81 o 7 3 2 578.78 551.91 3.90 o 8 3 2 523.29 523.27 4.38 o 9 3 2 14.08 12.30 0.44 o 10 3 2 122.38 105.46 1.89 o -10 4 2 71.87 73.38 1.32 o -9 4 2 35.69 34.97 0.86 o -8 4 2 0.54 0.55 0.31 o -7 4 2 26.52 28.18 0.50 o -6 4 2 49.69 46.01 0.70 o -5 4 2 103.95 88.83 1.05 o -4 4 2 127.56 114.00 1.69 o -3 4 2 1187.97 1270.18 14.38 o -2 4 2 23.46 29.76 0.74 o -1 4 2 358.67 356.13 4.43 o 0 4 2 735.48 775.60 10.55 o 1 4 2 19.96 22.96 1.27 o 2 4 2 5473.46 5759.24 81.28 o 3 4 2 4643.07 4913.67 46.57 o 4 4 2 0.47 2.42 0.65 o 5 4 2 183.15 188.60 1.51 o 6 4 2 199.41 181.86 1.49 o 7 4 2 0.49 0.75 0.29 o 8 4 2 28.36 28.34 0.60 o 9 4 2 222.44 217.71 2.45 o 10 4 2 181.30 169.45 3.61 o -10 5 2 19.40 16.93 0.50 o -9 5 2 3.29 3.31 0.33 o -8 5 2 212.76 219.64 2.31 o -7 5 2 110.12 110.85 1.07 o -6 5 2 222.10 220.82 1.98 o -5 5 2 298.36 310.31 2.72 o -4 5 2 393.16 405.33 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