Crystallography Open Database

Information card for entry 2023275

2023274 << 2023275 >> 2023276

Preview

Coordinates	2023275.cif
Original IUCr paper	HTML

Structure parameters

Chemical name	(μ-Tetrathioantimonato-κ^2^<i>S</i>:<i>S</i>')bis[(1,4,8,11-tetraazacyclotetradecane-κ^4^<i>N</i>)zinc(II)] perchlorate 0.8-hydrate
Formula	C20 H49.6 Cl N8 O4.8 S4 Sb Zn2
Calculated formula	C20 H49.6 Cl N8 O4.8 S4 Sb Zn2
Title of publication	Synthesis, crystal structure and properties of μ-tetrathioantimonato-bis[(cyclam)zinc(II)] perchlorate 0.8-hydrate
Authors of publication	Näther, Christian; Lühmann, Henning; Bensch, Wolfgang
Journal of publication	Acta Crystallographica Section E Crystallographic Communications
Year of publication	2024
Journal volume	80
Journal issue	11
Pages of publication	1151 - 1156
a	9.11238 ± 0.00007 Å
b	13.67434 ± 0.0001 Å
c	27.49214 ± 0.00018 Å
α	90°
β	92.9206 ± 0.0006°
γ	90°
Cell volume	3421.23 ± 0.04 Å³
Cell temperature	100.01 ± 0.1 K
Ambient diffraction temperature	100.01 ± 0.1 K
Number of distinct elements	8
Space group number	7
Hermann-Mauguin space group symbol	P 1 c 1
Hall space group symbol	P -2yc
Residual factor for all reflections	0.0238
Residual factor for significantly intense reflections	0.0227
Weighted residual factors for significantly intense reflections	0.0577
Weighted residual factors for all reflections included in the refinement	0.0582
Goodness-of-fit parameter for all reflections included in the refinement	1.025
Diffraction radiation probe	x-ray
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
296768 (current)	2024-12-07	cif/ Updating files of 2023275 Original log message: Adding full bibliography for 2023275.cif.	2023275.cif
295453	2024-10-12	cif/ Adding structures of 2023275 via cif-deposit CGI script.	2023275.cif