Crystallography Open Database

Information card for entry 2023293

2023292 << 2023293 >> 2023294

Preview

Coordinates	2023293.cif
Original IUCr paper	HTML

Structure parameters

Chemical name	[μ~2~-7-[{Bis(pyridin-2-ylmethyl)amino-1κ^3^<i>N</i>,<i>N</i>',<i>N</i>''}methyl]-5-chloroquinolin-8-olato-2κ<i>N</i>;1:2κ^2^<i>O</i>]trichlorido-1κ<i>Cl</i>,2κ^2^<i>Cl</i>-dizinc(II)
Formula	C22 H18 Cl4 N4 O Zn2
Calculated formula	C22 H18 Cl4 N4 O Zn2
Title of publication	Crystal structure of (μ2-7-{[bis(pyridin-2-ylmethyl)amino-1κ3 N,N′,N′′]methyl}-5-chloroquinolin-8-olato-2κN;1:2κ2 O)trichlorido-1κCl,2κ2 Cl-dizinc(II)
Authors of publication	Kubono, Koji; Tanaka, Kanata; Tani, Keita; Kashiwagi, Yukiyasu
Journal of publication	Acta Crystallographica Section E Crystallographic Communications
Year of publication	2024
Journal volume	80
Journal issue	11
Pages of publication	1175 - 1179
a	35.5812 ± 0.0004 Å
b	29.757 ± 0.0003 Å
c	8.8942 ± 0.0001 Å
α	90°
β	90°
γ	90°
Cell volume	9417.09 ± 0.18 Å³
Cell temperature	100.01 ± 0.1 K
Ambient diffraction temperature	100.01 ± 0.1 K
Number of distinct elements	6
Space group number	43
Hermann-Mauguin space group symbol	F d d 2
Hall space group symbol	F 2 -2d
Residual factor for all reflections	0.0285
Residual factor for significantly intense reflections	0.028
Weighted residual factors for significantly intense reflections	0.0726
Weighted residual factors for all reflections included in the refinement	0.0731
Goodness-of-fit parameter for all reflections included in the refinement	1.037
Diffraction radiation probe	x-ray
Diffraction radiation wavelength	1.54184 Å
Diffraction radiation type	CuKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
296786 (current)	2024-12-07	cif/ Updating files of 2023293 Original log message: Adding full bibliography for 2023293.cif.	2023293.cif
295504	2024-10-16	cif/ Adding structures of 2023293 via cif-deposit CGI script.	2023293.cif