#------------------------------------------------------------------------------
#$Date: 2025-02-09 20:23:52 +0200 (Sun, 09 Feb 2025) $
#$Revision: 297658 $
#$URL: file:///home/coder/svn-repositories/cod/hkl/2/02/33/2023394.hkl $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/. The original data for this entry
# were provided by IUCr Journals, http://journals.iucr.org/.
#
# The file may be used within the scientific community so long as
# proper attribution is given to the journal article from which the
# data were obtained.
#
data_2023394
_cell_angle_alpha                90.000
_cell_angle_beta                 90.000
_cell_angle_gamma                90.000
_cell_length_a                   4.7452
_cell_length_b                   4.7452
_cell_length_c                   4.7452
_exptl_crystal_F_000             100.00
_reflns_d_resolution_high        0.6178
_cod_data_source_file            dk5032Ca3GeO_500Ksup13.hkl
_cod_data_source_block           Ca3GeO_500K
_shelx_title                     ' mue83a_0m in Pm-3m'
_shelx_refln_list_code           4
_shelx_f_calc_maximum            67.81
_shelx_f_squared_multiplier      1.000
loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x, -y, z'
'-x, y, -z'
'x, -y, -z'
'z, x, y'
'z, -x, -y'
'-z, -x, y'
'-z, x, -y'
'y, z, x'
'-y, z, -x'
'y, -z, -x'
'-y, -z, x'
'y, x, -z'
'-y, -x, -z'
'y, -x, z'
'-y, x, z'
'x, z, -y'
'-x, z, y'
'-x, -z, -y'
'x, -z, y'
'z, y, -x'
'z, -y, x'
'-z, y, x'
'-z, -y, -x'
'-x, -y, -z'
'x, y, -z'
'x, -y, z'
'-x, y, z'
'-z, -x, -y'
'-z, x, y'
'z, x, -y'
'z, -x, y'
'-y, -z, -x'
'y, -z, x'
'-y, z, x'
'y, z, -x'
'-y, -x, z'
'y, x, z'
'-y, x, -z'
'y, -x, -z'
'-x, -z, y'
'x, -z, -y'
'x, z, y'
'-x, z, -y'
'-z, -y, x'
'-z, y, -x'
'z, -y, -x'
'z, y, x'
loop_
_refln_index_h
_refln_index_k
_refln_index_l
_refln_F_squared_calc
_refln_F_squared_meas
_refln_F_squared_sigma
_refln_observed_status
0 0 1 30.79 27.39 0.66 o
0 1 1 306.48 323.76 2.81 o
1 1 1 3765.04 3668.66 58.49 o
0 0 2 4598.39 4561.79 51.22 o
0 1 2 29.41 23.60 0.36 o
1 1 2 236.15 231.35 1.62 o
0 2 2 2825.46 2858.99 21.98 o
1 2 2 27.16 26.06 0.44 o
2 2 2 1873.59 1904.41 17.36 o
0 0 3 65.36 65.16 1.49 o
0 1 3 125.22 122.15 1.17 o
1 1 3 1548.16 1579.93 8.94 o
0 2 3 48.77 48.42 0.65 o
1 2 3 109.15 103.86 0.77 o
2 2 3 35.34 35.65 0.62 o
0 3 3 62.30 59.48 1.23 o
1 3 3 781.33 784.04 5.31 o
2 3 3 55.03 53.16 0.89 o
3 3 3 436.29 421.32 6.59 o
0 0 4 1324.63 1376.05 15.94 o
0 1 4 15.22 16.33 0.50 o
1 1 4 135.36 132.83 1.43 o
0 2 4 958.66 980.14 6.56 o
1 2 4 11.08 10.90 0.34 o
2 2 4 712.72 709.95 5.58 o
0 3 4 16.38 16.22 0.65 o
1 3 4 69.15 66.30 0.77 o
2 3 4 11.44 11.16 0.38 o
3 3 4 37.50 36.10 1.13 o
0 4 4 420.27 425.91 5.87 o
1 4 4 3.34 3.61 0.37 o
2 4 4 326.39 328.74 3.44 o
3 4 4 3.62 2.89 0.42 o
4 4 4 160.98 156.43 4.38 o
0 0 5 50.47 54.26 2.30 o
0 1 5 28.76 28.55 0.86 o
1 1 5 449.88 461.23 3.98 o
0 2 5 35.66 36.95 0.98 o
1 2 5 26.24 26.73 0.66 o
2 2 5 25.33 25.31 0.95 o
0 3 5 15.79 15.83 0.69 o
1 3 5 264.10 264.36 2.18 o
2 3 5 14.78 14.29 0.49 o
3 3 5 159.22 154.77 2.52 o
0 4 5 12.39 13.20 0.65 o
1 4 5 19.82 20.01 0.59 o
2 4 5 8.96 9.17 0.34 o
3 4 5 12.00 11.55 0.54 o
4 4 5 3.40 5.62 0.87 o
0 5 5 5.17 5.01 0.65 o
1 5 5 100.07 99.94 1.88 o
2 5 5 5.15 5.33 0.40 o
3 5 5 61.79 55.93 4.27 o
0 0 6 344.89 358.87 7.15 o
0 1 6 1.24 2.30 0.31 o
1 1 6 61.04 63.40 1.36 o
0 2 6 269.60 273.19 3.35 o
1 2 6 0.89 1.17 0.22 o
2 2 6 212.05 214.42 3.10 o
0 3 6 1.64 1.41 0.27 o
1 3 6 35.28 38.00 0.80 o
2 3 6 1.19 1.65 0.24 o
3 3 6 21.23 20.04 0.87 o
0 4 6 134.40 131.20 2.51 o
1 4 6 0.37 0.32 0.23 o
2 4 6 107.05 103.91 1.77 o
0 0 7 23.61 20.78 1.92 o
0 1 7 3.07 3.31 0.39 o
1 1 7 110.72 112.53 1.97 o
0 2 7 17.51 17.62 0.80 o
1 2 7 3.30 4.64 0.39 o
2 2 7 13.05 14.90 1.42 o
0 3 7 2.20 3.75 0.79 o
1 3 7 68.08 55.12 3.81 o