#------------------------------------------------------------------------------ #$Date: 2025-03-14 05:04:30 +0200 (Fri, 14 Mar 2025) $ #$Revision: 298434 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/02/34/2023434.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2023434 _cell_angle_alpha 90 _cell_angle_beta 90 _cell_angle_gamma 90 _cell_length_a 8.74145(8) _cell_length_b 8.74145(8) _cell_length_c 8.74145(8) _exptl_crystal_F_000 1316 _reflns_d_resolution_high 0.3790 _cod_data_source_file dk5135300Ksup10.hkl _cod_data_source_block 300K _shelx_title ' ' _shelx_refln_list_code 4 _shelx_f_calc_maximum 940.88 _shelx_f_squared_multiplier 1.000 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, z' '-x, y, -z' 'x, -y, -z' 'z, x, y' 'z, -x, -y' '-z, -x, y' '-z, x, -y' 'y, z, x' '-y, z, -x' 'y, -z, -x' '-y, -z, x' 'y, x, -z' '-y, -x, -z' 'y, -x, z' '-y, x, z' 'x, z, -y' '-x, z, y' '-x, -z, -y' 'x, -z, y' 'z, y, -x' 'z, -y, x' '-z, y, x' '-z, -y, -x' '-x, -y, -z' 'x, y, -z' 'x, -y, z' '-x, y, z' '-z, -x, -y' '-z, x, y' 'z, x, -y' 'z, -x, y' '-y, -z, -x' 'y, -z, x' '-y, z, x' 'y, z, -x' '-y, -x, z' 'y, x, z' '-y, x, -z' 'y, -x, -z' '-x, -z, y' 'x, -z, -y' 'x, z, y' '-x, z, -y' '-z, -y, x' '-z, y, -x' 'z, -y, -x' 'z, y, x' 'x, y+1/2, z+1/2' '-x, -y+1/2, z+1/2' '-x, y+1/2, -z+1/2' 'x, -y+1/2, -z+1/2' 'z, x+1/2, y+1/2' 'z, -x+1/2, -y+1/2' '-z, -x+1/2, y+1/2' '-z, x+1/2, -y+1/2' 'y, z+1/2, x+1/2' '-y, z+1/2, -x+1/2' 'y, -z+1/2, -x+1/2' '-y, -z+1/2, x+1/2' 'y, x+1/2, -z+1/2' '-y, -x+1/2, -z+1/2' 'y, -x+1/2, z+1/2' '-y, x+1/2, z+1/2' 'x, z+1/2, -y+1/2' '-x, z+1/2, y+1/2' '-x, -z+1/2, -y+1/2' 'x, -z+1/2, y+1/2' 'z, y+1/2, -x+1/2' 'z, -y+1/2, x+1/2' '-z, y+1/2, x+1/2' '-z, -y+1/2, -x+1/2' '-x, -y+1/2, -z+1/2' 'x, y+1/2, -z+1/2' 'x, -y+1/2, z+1/2' '-x, y+1/2, z+1/2' '-z, -x+1/2, -y+1/2' '-z, x+1/2, y+1/2' 'z, x+1/2, -y+1/2' 'z, -x+1/2, y+1/2' '-y, -z+1/2, -x+1/2' 'y, -z+1/2, x+1/2' '-y, z+1/2, x+1/2' 'y, z+1/2, -x+1/2' '-y, -x+1/2, z+1/2' 'y, x+1/2, z+1/2' '-y, x+1/2, -z+1/2' 'y, -x+1/2, -z+1/2' '-x, -z+1/2, y+1/2' 'x, -z+1/2, -y+1/2' 'x, z+1/2, y+1/2' '-x, z+1/2, -y+1/2' '-z, -y+1/2, x+1/2' '-z, y+1/2, -x+1/2' 'z, -y+1/2, -x+1/2' 'z, y+1/2, x+1/2' 'x+1/2, y, z+1/2' '-x+1/2, -y, z+1/2' '-x+1/2, y, -z+1/2' 'x+1/2, -y, -z+1/2' 'z+1/2, x, y+1/2' 'z+1/2, -x, -y+1/2' '-z+1/2, -x, y+1/2' '-z+1/2, x, -y+1/2' 'y+1/2, z, x+1/2' '-y+1/2, z, -x+1/2' 'y+1/2, -z, -x+1/2' '-y+1/2, -z, x+1/2' 'y+1/2, x, -z+1/2' '-y+1/2, -x, -z+1/2' 'y+1/2, -x, z+1/2' '-y+1/2, x, z+1/2' 'x+1/2, z, -y+1/2' '-x+1/2, z, y+1/2' '-x+1/2, -z, -y+1/2' 'x+1/2, -z, y+1/2' 'z+1/2, y, -x+1/2' 'z+1/2, -y, x+1/2' '-z+1/2, y, x+1/2' '-z+1/2, -y, -x+1/2' '-x+1/2, -y, -z+1/2' 'x+1/2, y, -z+1/2' 'x+1/2, -y, z+1/2' '-x+1/2, y, z+1/2' '-z+1/2, -x, -y+1/2' '-z+1/2, x, y+1/2' 'z+1/2, x, -y+1/2' 'z+1/2, -x, y+1/2' '-y+1/2, -z, -x+1/2' 'y+1/2, -z, x+1/2' '-y+1/2, z, x+1/2' 'y+1/2, z, -x+1/2' '-y+1/2, -x, z+1/2' 'y+1/2, x, z+1/2' '-y+1/2, x, -z+1/2' 'y+1/2, -x, -z+1/2' '-x+1/2, -z, y+1/2' 'x+1/2, -z, -y+1/2' 'x+1/2, z, y+1/2' '-x+1/2, z, -y+1/2' '-z+1/2, -y, x+1/2' '-z+1/2, y, -x+1/2' 'z+1/2, -y, -x+1/2' 'z+1/2, y, x+1/2' 'x+1/2, y+1/2, z' '-x+1/2, -y+1/2, z' '-x+1/2, y+1/2, -z' 'x+1/2, -y+1/2, -z' 'z+1/2, x+1/2, y' 'z+1/2, -x+1/2, -y' '-z+1/2, -x+1/2, y' '-z+1/2, x+1/2, -y' 'y+1/2, z+1/2, x' '-y+1/2, z+1/2, -x' 'y+1/2, -z+1/2, -x' '-y+1/2, -z+1/2, x' 'y+1/2, x+1/2, -z' '-y+1/2, -x+1/2, -z' 'y+1/2, -x+1/2, z' '-y+1/2, x+1/2, z' 'x+1/2, z+1/2, -y' '-x+1/2, z+1/2, y' '-x+1/2, -z+1/2, -y' 'x+1/2, -z+1/2, y' 'z+1/2, y+1/2, -x' 'z+1/2, -y+1/2, x' '-z+1/2, y+1/2, x' '-z+1/2, -y+1/2, -x' '-x+1/2, -y+1/2, -z' 'x+1/2, y+1/2, -z' 'x+1/2, -y+1/2, z' '-x+1/2, y+1/2, z' '-z+1/2, -x+1/2, -y' '-z+1/2, x+1/2, y' 'z+1/2, x+1/2, -y' 'z+1/2, -x+1/2, y' '-y+1/2, -z+1/2, -x' 'y+1/2, -z+1/2, x' '-y+1/2, z+1/2, x' 'y+1/2, z+1/2, -x' '-y+1/2, -x+1/2, z' 'y+1/2, x+1/2, z' '-y+1/2, x+1/2, -z' 'y+1/2, -x+1/2, -z' '-x+1/2, -z+1/2, y' 'x+1/2, -z+1/2, -y' 'x+1/2, z+1/2, y' '-x+1/2, z+1/2, -y' '-z+1/2, -y+1/2, x' '-z+1/2, y+1/2, -x' 'z+1/2, -y+1/2, -x' 'z+1/2, y+1/2, x' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 1 1 2291.63 2182.51 11.75 o 0 0 2 19843.20 23887.20 70.58 o 0 2 2 88266.30 99428.60 106.99 o 2 2 2 764313.00 885246.00 1124.69 o 1 1 3 6603.70 8171.79 16.84 o 1 3 3 32540.50 34263.50 45.93 o 3 3 3 67528.90 65866.10 137.04 o 0 0 4 837193.00 851213.00 1686.52 o 0 2 4 28251.10 29874.60 40.06 o 2 2 4 37828.20 40889.80 53.74 o 0 4 4 503400.00 453332.00 510.99 o 2 4 4 34174.50 35094.70 50.38 o 4 4 4 321381.00 296292.00 438.65 o 1 1 5 13029.60 12700.80 26.06 o 1 3 5 222.82 220.38 2.97 o 3 3 5 4541.56 5082.54 17.39 o 1 5 5 21724.70 21162.60 44.52 o 3 5 5 4517.10 4417.09 17.75 o 5 5 5 26585.90 25537.80 107.35 o 0 0 6 1012.50 1098.72 17.25 o 0 2 6 75725.30 74838.40 101.23 o 2 2 6 284448.00 251341.00 254.39 o 0 4 6 4645.47 4748.14 17.20 o 2 4 6 43070.50 42288.10 50.45 o 4 4 6 8874.43 9256.69 29.61 o 0 6 6 68924.10 70213.60 152.92 o 2 6 6 125759.00 121030.00 177.56 o 4 6 6 44170.60 45542.40 95.33 o 6 6 6 59750.90 63151.90 225.18 o 1 1 7 7045.60 6987.97 23.09 o 1 3 7 21143.90 20399.70 31.80 o 3 3 7 38888.30 37688.90 72.65 o 1 5 7 341.04 376.04 5.75 o 3 5 7 5092.95 5144.00 17.65 o 5 5 7 534.10 615.74 11.59 o 1 7 7 15107.10 15503.80 50.20 o 3 7 7 25302.50 25296.50 74.01 o 5 7 7 4910.62 4838.59 29.63 o 7 7 7 17818.10 16622.80 103.69 o 0 0 8 229497.00 219235.00 481.74 o 0 2 8 34178.00 33643.50 66.33 o 2 2 8 4891.44 4928.16 22.12 o 0 4 8 156029.00 146473.00 209.49 o 2 4 8 36274.00 35876.30 57.70 o 4 4 8 107983.00 108228.00 189.90 o 0 6 8 12309.30 12926.00 46.13 o 2 6 8 10573.30 10716.50 30.82 o 4 6 8 14620.30 15013.00 38.79 o 6 6 8 14113.70 14326.80 55.08 o 0 8 8 58758.30 63751.60 195.00 o 2 8 8 32474.20 33760.40 95.94 o 4 8 8 42112.30 42325.70 118.78 o 6 8 8 15762.70 15248.50 61.54 o 8 8 8 17621.60 15602.80 123.54 o 1 1 9 4190.03 3986.94 23.31 o 1 3 9 95.53 120.97 5.38 o 3 3 9 1452.84 1579.98 16.51 o 1 5 9 7695.09 7741.22 26.23 o 3 5 9 1668.11 1699.26 13.45 o 5 5 9 10365.90 10250.60 44.21 o 1 7 9 126.04 169.27 7.32 o 3 7 9 2036.54 2103.17 14.84 o 5 7 9 228.96 271.71 8.34 o 7 7 9 2272.45 2200.71 23.56 o 1 9 9 3340.94 3337.45 26.27 o 3 9 9 731.17 731.29 16.23 o 5 9 9 4872.77 4955.85 36.12 o 7 9 9 112.25 148.41 13.35 o 9 9 9 2641.59 2494.01 51.59 o 0 0 10 180.32 285.53 19.56 o 0 2 10 49433.50 47738.70 116.22 o 2 2 10 71590.90 68284.00 156.57 o 0 4 10 137.20 212.93 10.57 o 2 4 10 33365.90 32078.00 63.69 o 4 4 10 953.95 944.37 15.67 o 0 6 10 44913.20 45828.70 118.17 o 2 6 10 36058.50 36313.00 73.59 o 4 6 10 31916.10 30754.50 68.68 o 6 6 10 18459.20 18314.00 73.27 o 0 8 10 2305.66 2349.29 23.75 o 2 8 10 11958.70 12233.90 39.20 o 4 8 10 3324.37 3293.69 21.44 o 6 8 10 13017.50 12181.30 41.64 o 8 8 10 4859.31 4644.20 39.47 o 0 10 10 30875.50 32628.60 144.59 o 2 10 10 12002.80 12313.10 57.45 o 4 10 10 23338.30 23386.80 90.80 o 6 10 10 6207.21 5887.98 42.37 o 8 10 10 11116.20 10406.10 69.36 o 10 10 10 2054.25 2098.46 59.00 o 1 1 11 783.43 723.63 13.26 o 1 3 11 3938.96 3787.39 19.50 o 3 3 11 8759.71 8502.93 42.32 o 1 5 11 7.44 89.73 8.16 o 3 5 11 803.75 776.66 11.13 o 5 5 11 599.18 653.00 15.76 o 1 7 11 3736.49 3759.55 22.00 o 3 7 11 7153.03 7108.50 29.93 o 5 7 11 1130.22 1086.95 14.19 o 7 7 11 5986.39 5680.09 41.25 o 1 9 11 4.45 76.29 10.10 o 3 9 11 405.15 399.39 10.94 o 5 9 11 321.28 322.62 10.85 o 7 9 11 619.12 598.12 13.26 o 9 9 11 193.40 200.24 16.69 o 1 11 11 1089.52 1103.91 21.89 o 3 11 11 2461.91 2457.56 30.80 o 5 11 11 257.09 258.09 17.89 o 7 11 11 2331.67 2292.51 30.06 o 9 11 11 151.98 173.44 15.67 o 11 11 11 964.38 944.27 39.32 o 0 0 12 56631.70 51115.40 247.85 o 0 2 12 20868.80 19250.50 69.42 o 2 2 12 681.61 631.89 14.74 o 0 4 12 41506.60 39681.90 109.96 o 2 4 12 21209.50 20209.30 52.79 o 4 4 12 30548.80 29521.30 96.38 o 0 6 12 9936.55 9828.69 50.52 o 2 6 12 2293.09 2188.39 17.72 o 4 6 12 10684.70 10574.20 39.46 o 6 6 12 3779.87 3654.56 33.98 o 0 8 12 18377.20 19488.90 77.66 o 2 8 12 18941.70 19376.70 55.08 o 4 8 12 13610.60 13500.20 47.52 o 6 8 12 10674.70 10258.70 41.05 o 8 8 12 6079.73 5760.73 53.15 o 0 10 12 2913.60 2945.18 31.09 o 2 10 12 3535.99 3527.33 24.60 o 4 10 12 3460.66 3483.07 26.92 o 6 10 12 4394.79 4339.84 30.92 o 8 10 12 4174.14 4094.28 30.83 o 10 10 12 4426.01 4402.52 45.68 o 0 12 12 6727.76 6947.58 65.43 o 2 12 12 12350.60 13236.30 71.07 o 4 12 12 5004.44 5147.72 46.07 o 6 12 12 7688.92 7722.11 52.53 o 8 12 12 2219.72 2227.90 35.16 o 10 12 12 3522.69 3475.25 35.55 o 12 12 12 791.11 817.17 39.22 o 1 1 13 73.74 116.15 11.22 o 1 3 13 331.33 348.49 9.92 o 3 3 13 1800.99 1796.64 24.21 o 1 5 13 696.56 716.45 12.42 o 3 5 13 6.08 82.13 11.59 o 5 5 13 1585.53 1590.41 24.58 o 1 7 13 611.11 602.94 11.87 o 3 7 13 1922.51 1944.05 18.46 o 5 7 13 50.46 94.18 11.03 o 7 7 13 1942.12 1952.25 31.63 o 1 9 13 381.63 417.75 11.59 o 3 9 13 3.09 72.30 14.00 o 5 9 13 918.37 925.53 17.25 o 7 9 13 30.54 70.91 12.33 o 9 9 13 580.19 576.14 20.86 o 1 11 13 128.04 151.57 10.38 o 3 11 13 641.61 631.05 14.74 o 5 11 13 0.92 65.54 15.20 o 7 11 13 743.11 750.50 16.69 o 9 11 13 0.88 61.09 12.70 o 11 11 13 276.67 289.98 17.24 o 1 13 13 9.04 71.93 17.70 o 3 13 13 82.31 109.85 15.57 o 5 13 13 138.10 154.44 14.55 o 7 13 13 158.59 167.88 14.65 o 9 13 13 95.59 112.54 14.00 o 11 13 13 37.98 59.70 14.55 o 13 13 13 2.44 29.85 33.00 < 0 0 14 83.24 155.83 27.81 o 0 2 14 20467.80 18765.30 80.89 o 2 2 14 19258.60 18459.20 78.52 o 0 4 14 12.91 103.45 15.20 o 2 4 14 15091.60 14377.30 48.48 o 4 4 14 183.00 205.61 14.65 o 0 6 14 19540.10 19971.90 87.50 o 2 6 14 10773.20 10685.80 41.42 o 4 6 14 14876.90 14565.00 51.83 o 6 6 14 5938.82 5915.37 51.10 o 0 8 14 570.08 599.50 20.03 o 2 8 14 6691.48 6681.65 36.43 o 4 8 14 922.58 926.73 16.78 o 6 8 14 7185.34 7111.89 38.39 o 8 8 14 1655.47 1631.11 26.06 o 0 10 14 15164.60 16169.90 85.32 o 2 10 14 4139.25 4334.32 29.34 o 4 10 14 12012.40 12431.30 52.71 o 6 10 14 2199.12 2323.18 24.77 o 8 10 14 6430.95 6396.20 32.52 o 10 10 14 741.35 704.68 19.56 o 0 12 14 971.27 1069.28 24.67 o 2 12 14 2455.96 2629.87 24.22 o 4 12 14 1239.16 1288.81 16.88 o 6 12 14 2903.31 2977.16 22.18 o 8 12 14 1714.85 1614.04 17.90 o 10 12 14 2910.14 2835.99 21.90 o 12 12 14 1634.17 1472.70 26.53 o 0 14 14 8644.47 9345.41 78.40 o 2 14 14 1646.66 1758.51 25.32 o 4 14 14 7045.78 7415.03 49.26 o 6 14 14 866.39 836.20 19.10 o 8 14 14 4055.46 4020.41 37.23 o 10 14 14 281.18 272.09 15.67 o 1 1 15 34.59 93.62 14.83 o 1 3 15 183.02 197.46 10.01 o 3 3 15 984.04 1001.86 21.33 o 1 5 15 379.71 410.15 12.24 o 3 5 15 3.58 72.58 13.72 o 5 5 15 920.38 964.29 24.20 o 1 7 15 342.95 337.09 12.70 o 3 7 15 1100.84 1126.65 15.95 o 5 7 15 26.01 80.28 12.42 o 7 7 15 1157.10 1168.77 22.72 o 1 9 15 241.69 267.27 12.05 o 3 9 15 3.20 73.04 14.00 o 5 9 15 597.17 604.24 14.46 o 7 9 15 14.13 66.56 11.77 o 9 9 15 410.89 396.34 16.69 o 1 11 15 68.62 117.63 11.22 o 3 11 15 380.07 418.77 12.05 o 5 11 15 2.19 58.49 11.68 o 7 11 15 452.77 460.50 11.87 o 9 11 15 2.52 38.38 11.59 o 11 11 15 164.26 162.97 13.91 o 1 13 15 10.05 62.48 11.68 o 3 13 15 44.20 73.23 9.83 o 5 13 15 108.71 109.20 9.73 o 7 13 15 91.13 103.08 8.81 o 9 13 15 80.58 75.73 9.27 o 11 13 15 18.14 29.29 13.72 < 1 15 15 12.99 42.64 14.37 < 3 15 15 20.38 44.49 14.18 o 5 15 15 93.34 71.38 13.44 o 7 15 15 48.48 53.39 16.59 o 9 15 15 71.96 38.10 24.47 < 0 0 16 17368.40 15985.70 159.39 o 0 2 16 7295.34 7035.68 55.50 o 2 2 16 394.55 390.68 19.75 o 0 4 16 13471.00 13076.50 81.72 o 2 4 16 7647.53 7624.89 40.81 o 4 4 16 10424.70 10003.80 58.08 o 0 6 16 3970.22 4014.66 37.04 o 2 6 16 956.21 922.67 16.51 o 4 6 16 4343.93 4410.06 30.18 o 6 6 16 1526.52 1539.85 25.69 o 0 8 16 6812.81 6955.42 48.79 o 2 8 16 7582.23 8005.72 36.72 o 4 8 16 5225.91 5646.60 35.67 o 6 8 16 4677.87 4911.42 30.46 o 8 8 16 2535.50 2532.57 30.43 o 0 10 16 1437.60 1599.70 25.69 o 2 10 16 1476.10 1540.64 17.25 o 4 10 16 1699.45 1783.14 18.18 o 6 10 16 1898.75 1878.35 18.74 o 8 10 16 2105.68 2088.60 19.39 o 10 10 16 2056.90 2005.84 25.98 o 0 12 16 2869.03 3028.58 33.13 o 2 12 16 5735.16 5967.16 30.19 o 4 12 16 2176.91 2250.73 19.57 o 6 12 16 3782.30 3781.99 24.78 o 8 12 16 1013.87 1021.35 15.21 o 10 12 16 1893.44 1776.92 22.54 o 0 14 16 580.60 635.57 16.97 o 2 14 16 1148.10 1207.43 15.12 o 4 14 16 722.32 691.24 13.63 o 6 14 16 1395.45 1383.25 19.76 o 8 14 16 980.46 868.67 23.74 o 0 16 16 1374.32 1476.44 67.34 o 2 16 16 3021.95 3267.95 64.05 o 4 16 16 1054.85 1157.81 80.04 o 1 1 17 144.87 149.62 14.28 o 1 3 17 665.01 630.87 14.93 o 3 3 17 1495.61 1468.33 25.69 o 1 5 17 0.51 69.43 14.00 o 3 5 17 171.72 186.61 10.38 o 5 5 17 91.76 122.46 15.39 o 1 7 17 764.86 816.80 15.86 o 3 7 17 1490.63 1580.35 20.50 o 5 7 17 268.93 268.01 10.85 o 7 7 17 1457.86 1443.61 23.65 o 1 9 17 0.36 58.31 12.05 o 3 9 17 112.58 137.38 9.73 o 5 9 17 62.69 84.73 10.01 o 7 9 17 181.14 179.84 9.73 o 9 9 17 44.19 51.91 12.79 o 1 11 17 295.67 320.21 10.66 o 3 11 17 669.85 712.18 13.17 o 5 11 17 78.90 92.42 8.99 o 7 11 17 696.87 664.53 12.70 o 9 11 17 54.04 57.94 9.83 o 11 11 17 327.71 287.96 28.83 o 1 13 17 47.09 61.92 9.27 o 3 13 17 210.24 214.52 9.92 o 5 13 17 0.30 34.58 11.68 < 7 13 17 255.18 231.21 12.70 o 1 15 17 24.75 50.61 20.49 < 3 15 17 129.24 143.50 25.68 o 0 0 18 13.68 72.77 33.93 < 0 2 18 6127.98 5983.58 44.69 o 2 2 18 7035.95 6723.22 56.23 o 0 4 18 89.70 125.51 15.85 o 2 4 18 4702.20 4770.55 32.32 o 4 4 18 216.21 237.88 14.55 o 0 6 18 6328.98 6219.59 45.16 o 2 6 18 4371.48 4402.07 26.74 o 4 6 18 4980.30 5084.54 28.42 o 6 6 18 2656.00 2665.63 29.14 o 0 8 18 409.98 401.53 16.22 o 2 8 18 2288.24 2396.96 21.06 o 4 8 18 580.59 566.59 12.24 o 6 8 18 2601.45 2666.86 20.69 o 8 8 18 937.10 828.53 18.82 o 0 10 18 5563.54 5930.42 45.24 o 2 10 18 1980.57 2107.34 20.22 o 4 10 18 4503.47 4730.50 27.95 o 6 10 18 1154.55 1135.01 15.39 o 8 10 18 2540.29 2524.59 25.33 o 10 10 18 463.62 399.89 24.94 o 0 12 18 605.80 591.45 18.91 o 2 12 18 928.53 974.59 15.86 o 4 12 18 741.81 704.05 15.48 o 6 12 18 1146.42 1150.92 20.87 o 8 12 18 985.43 882.44 31.44 o 0 14 18 3557.73 3730.43 75.58 o 2 14 18 916.48 965.94 35.61 o 1 1 19 164.73 175.39 13.35 o 1 3 19 4.04 54.13 11.22 o 3 3 19 70.72 94.37 14.09 o 1 5 19 403.46 404.12 10.85 o 3 5 19 97.00 106.51 9.46 o 5 5 19 686.71 671.66 17.43 o 1 7 19 5.43 45.79 11.12 o 3 7 19 125.23 124.87 9.18 o 5 7 19 25.25 49.96 8.71 o 7 7 19 173.87 179.01 12.51 o 1 9 19 293.94 286.92 10.38 o 3 9 19 74.68 78.14 8.90 o 5 9 19 498.66 444.65 11.96 o 7 9 19 21.45 36.71 11.03 o 9 9 19 368.02 312.07 23.73 o 1 11 19 4.23 37.73 13.53 < 3 11 19 26.71 49.41 12.14 o 5 11 19 57.34 49.13 12.61 o 7 11 19 51.99 56.45 19.56 < 1 13 19 66.06 63.31 24.29 < 0 0 20 6710.15 6484.66 91.16 o 0 2 20 1901.66 1848.10 25.97 o 2 2 20 400.26 413.67 15.67 o 0 4 20 5443.71 5322.97 40.13 o 2 4 20 2096.82 2033.68 18.28 o 4 4 20 4398.96 4326.49 37.42 o 0 6 20 1065.00 1102.22 19.66 o 2 6 20 667.53 682.23 11.87 o 4 6 20 1226.78 1231.11 15.02 o 6 6 20 926.84 912.18 19.75 o 0 8 20 3090.56 3190.59 32.76 o 2 8 20 2329.43 2344.27 21.25 o 4 8 20 2469.55 2541.72 24.31 o 6 8 20 1471.84 1367.56 20.68 o 8 8 20 1341.92 1433.46 60.48 o 0 10 20 396.61 423.88 21.23 o 2 10 20 896.75 900.98 18.18 o 4 10 20 496.93 477.21 19.47 o 1 1 21 123.79 132.84 12.14 o 1 3 21 354.88 360.82 10.01 o 3 3 21 685.01 669.90 16.69 o 1 5 21 17.78 45.05 9.36 o 3 5 21 132.80 125.33 8.99 o 5 5 21 3.38 24.19 18.35 < 1 7 21 395.89 413.49 12.52 o 3 7 21 692.95 678.45 16.13 o 5 7 21 174.90 153.52 13.63 o 1 9 21 12.59 28.27 18.82 < 3 9 21 94.46 79.26 18.45 o 0 0 22 110.19 94.09 28.64 o 0 2 22 1536.36 1557.34 27.92 o 2 2 22 3045.07 3095.76 37.22 o 0 4 22 186.56 180.96 15.67 o 2 4 22 1177.26 1118.11 18.55 o 4 4 22 272.72 237.15 19.65 o 0 6 22 1695.45 1675.97 42.95 o 2 6 22 2069.13 2041.33 34.52 o 1 1 23 73.03 69.62 18.63 o