#------------------------------------------------------------------------------ #$Date: 2025-03-14 05:04:30 +0200 (Fri, 14 Mar 2025) $ #$Revision: 298434 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/02/34/2023440.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2023440 _cell_angle_alpha 90 _cell_angle_beta 90 _cell_angle_gamma 90 _cell_length_a 8.74648(10) _cell_length_b 8.74648(10) _cell_length_c 8.74648(10) _exptl_crystal_F_000 1316 _reflns_d_resolution_high 0.3778 _cod_data_source_file dk5135350Ksup16.hkl _cod_data_source_block 350K _shelx_title ' ' _shelx_refln_list_code 4 _shelx_f_calc_maximum 928.90 _shelx_f_squared_multiplier 1.000 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, z' '-x, y, -z' 'x, -y, -z' 'z, x, y' 'z, -x, -y' '-z, -x, y' '-z, x, -y' 'y, z, x' '-y, z, -x' 'y, -z, -x' '-y, -z, x' 'y, x, -z' '-y, -x, -z' 'y, -x, z' '-y, x, z' 'x, z, -y' '-x, z, y' '-x, -z, -y' 'x, -z, y' 'z, y, -x' 'z, -y, x' '-z, y, x' '-z, -y, -x' '-x, -y, -z' 'x, y, -z' 'x, -y, z' '-x, y, z' '-z, -x, -y' '-z, x, y' 'z, x, -y' 'z, -x, y' '-y, -z, -x' 'y, -z, x' '-y, z, x' 'y, z, -x' '-y, -x, z' 'y, x, z' '-y, x, -z' 'y, -x, -z' '-x, -z, y' 'x, -z, -y' 'x, z, y' '-x, z, -y' '-z, -y, x' '-z, y, -x' 'z, -y, -x' 'z, y, x' 'x, y+1/2, z+1/2' '-x, -y+1/2, z+1/2' '-x, y+1/2, -z+1/2' 'x, -y+1/2, -z+1/2' 'z, x+1/2, y+1/2' 'z, -x+1/2, -y+1/2' '-z, -x+1/2, y+1/2' '-z, x+1/2, -y+1/2' 'y, z+1/2, x+1/2' '-y, z+1/2, -x+1/2' 'y, -z+1/2, -x+1/2' '-y, -z+1/2, x+1/2' 'y, x+1/2, -z+1/2' '-y, -x+1/2, -z+1/2' 'y, -x+1/2, z+1/2' '-y, x+1/2, z+1/2' 'x, z+1/2, -y+1/2' '-x, z+1/2, y+1/2' '-x, -z+1/2, -y+1/2' 'x, -z+1/2, y+1/2' 'z, y+1/2, -x+1/2' 'z, -y+1/2, x+1/2' '-z, y+1/2, x+1/2' '-z, -y+1/2, -x+1/2' '-x, -y+1/2, -z+1/2' 'x, y+1/2, -z+1/2' 'x, -y+1/2, z+1/2' '-x, y+1/2, z+1/2' '-z, -x+1/2, -y+1/2' '-z, x+1/2, y+1/2' 'z, x+1/2, -y+1/2' 'z, -x+1/2, y+1/2' '-y, -z+1/2, -x+1/2' 'y, -z+1/2, x+1/2' '-y, z+1/2, x+1/2' 'y, z+1/2, -x+1/2' '-y, -x+1/2, z+1/2' 'y, x+1/2, z+1/2' '-y, x+1/2, -z+1/2' 'y, -x+1/2, -z+1/2' '-x, -z+1/2, y+1/2' 'x, -z+1/2, -y+1/2' 'x, z+1/2, y+1/2' '-x, z+1/2, -y+1/2' '-z, -y+1/2, x+1/2' '-z, y+1/2, -x+1/2' 'z, -y+1/2, -x+1/2' 'z, y+1/2, x+1/2' 'x+1/2, y, z+1/2' '-x+1/2, -y, z+1/2' '-x+1/2, y, -z+1/2' 'x+1/2, -y, -z+1/2' 'z+1/2, x, y+1/2' 'z+1/2, -x, -y+1/2' '-z+1/2, -x, y+1/2' '-z+1/2, x, -y+1/2' 'y+1/2, z, x+1/2' '-y+1/2, z, -x+1/2' 'y+1/2, -z, -x+1/2' '-y+1/2, -z, x+1/2' 'y+1/2, x, -z+1/2' '-y+1/2, -x, -z+1/2' 'y+1/2, -x, z+1/2' '-y+1/2, x, z+1/2' 'x+1/2, z, -y+1/2' '-x+1/2, z, y+1/2' '-x+1/2, -z, -y+1/2' 'x+1/2, -z, y+1/2' 'z+1/2, y, -x+1/2' 'z+1/2, -y, x+1/2' '-z+1/2, y, x+1/2' '-z+1/2, -y, -x+1/2' '-x+1/2, -y, -z+1/2' 'x+1/2, y, -z+1/2' 'x+1/2, -y, z+1/2' '-x+1/2, y, z+1/2' '-z+1/2, -x, -y+1/2' '-z+1/2, x, y+1/2' 'z+1/2, x, -y+1/2' 'z+1/2, -x, y+1/2' '-y+1/2, -z, -x+1/2' 'y+1/2, -z, x+1/2' '-y+1/2, z, x+1/2' 'y+1/2, z, -x+1/2' '-y+1/2, -x, z+1/2' 'y+1/2, x, z+1/2' '-y+1/2, x, -z+1/2' 'y+1/2, -x, -z+1/2' '-x+1/2, -z, y+1/2' 'x+1/2, -z, -y+1/2' 'x+1/2, z, y+1/2' '-x+1/2, z, -y+1/2' '-z+1/2, -y, x+1/2' '-z+1/2, y, -x+1/2' 'z+1/2, -y, -x+1/2' 'z+1/2, y, x+1/2' 'x+1/2, y+1/2, z' '-x+1/2, -y+1/2, z' '-x+1/2, y+1/2, -z' 'x+1/2, -y+1/2, -z' 'z+1/2, x+1/2, y' 'z+1/2, -x+1/2, -y' '-z+1/2, -x+1/2, y' '-z+1/2, x+1/2, -y' 'y+1/2, z+1/2, x' '-y+1/2, z+1/2, -x' 'y+1/2, -z+1/2, -x' '-y+1/2, -z+1/2, x' 'y+1/2, x+1/2, -z' '-y+1/2, -x+1/2, -z' 'y+1/2, -x+1/2, z' '-y+1/2, x+1/2, z' 'x+1/2, z+1/2, -y' '-x+1/2, z+1/2, y' '-x+1/2, -z+1/2, -y' 'x+1/2, -z+1/2, y' 'z+1/2, y+1/2, -x' 'z+1/2, -y+1/2, x' '-z+1/2, y+1/2, x' '-z+1/2, -y+1/2, -x' '-x+1/2, -y+1/2, -z' 'x+1/2, y+1/2, -z' 'x+1/2, -y+1/2, z' '-x+1/2, y+1/2, z' '-z+1/2, -x+1/2, -y' '-z+1/2, x+1/2, y' 'z+1/2, x+1/2, -y' 'z+1/2, -x+1/2, y' '-y+1/2, -z+1/2, -x' 'y+1/2, -z+1/2, x' '-y+1/2, z+1/2, x' 'y+1/2, z+1/2, -x' '-y+1/2, -x+1/2, z' 'y+1/2, x+1/2, z' '-y+1/2, x+1/2, -z' 'y+1/2, -x+1/2, -z' '-x+1/2, -z+1/2, y' 'x+1/2, -z+1/2, -y' 'x+1/2, z+1/2, y' '-x+1/2, z+1/2, -y' '-z+1/2, -y+1/2, x' '-z+1/2, y+1/2, -x' 'z+1/2, -y+1/2, -x' 'z+1/2, y+1/2, x' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 1 1 2384.63 2207.63 11.73 o 0 0 2 19816.20 25137.80 61.26 o 0 2 2 87985.90 100910.00 107.52 o 2 2 2 755472.00 862850.00 1106.27 o 1 1 3 6621.94 8497.97 17.05 o 1 3 3 32469.50 34279.90 41.87 o 3 3 3 66808.00 69002.50 141.75 o 0 0 4 824811.00 846495.00 1074.77 o 0 2 4 28050.80 30658.90 40.69 o 2 2 4 37438.30 41110.50 53.27 o 0 4 4 489099.00 445839.00 470.78 o 2 4 4 33553.10 34753.80 49.24 o 4 4 4 308259.00 283012.00 484.92 o 1 1 5 13005.40 12591.10 24.24 o 1 3 5 228.45 214.76 3.00 o 3 3 5 4383.79 5006.59 17.27 o 1 5 5 21045.30 20541.30 39.87 o 3 5 5 4352.84 4338.06 17.68 o 5 5 5 25097.80 24384.10 99.52 o 0 0 6 1015.34 1075.87 17.73 o 0 2 6 74203.50 74071.50 83.28 o 2 2 6 273021.00 243787.00 227.02 o 0 4 6 4567.47 4764.27 16.94 o 2 4 6 41849.90 42051.80 45.12 o 4 4 6 8587.25 8898.43 28.33 o 0 6 6 66004.30 67020.40 141.67 o 2 6 6 117759.00 115180.00 147.69 o 4 6 6 41929.90 41578.60 85.10 o 6 6 6 54775.90 55820.10 204.39 o 1 1 7 6953.01 7108.84 22.73 o 1 3 7 20462.70 20230.90 30.05 o 3 3 7 37184.70 35837.20 64.17 o 1 5 7 341.13 364.20 5.74 o 3 5 7 4829.84 4903.90 17.01 o 5 5 7 477.33 548.11 11.23 o 1 7 7 14128.00 14123.10 47.05 o 3 7 7 23408.20 23450.70 65.47 o 5 7 7 4514.50 4327.82 27.42 o 7 7 7 15998.20 15054.80 94.27 o 0 0 8 217056.00 193593.00 537.64 o 0 2 8 33017.80 32568.30 62.15 o 2 2 8 4757.74 4917.26 21.77 o 0 4 8 145989.00 137437.00 186.86 o 2 4 8 34542.80 34460.30 51.60 o 4 4 8 100021.00 90373.50 155.76 o 0 6 8 11695.10 11881.60 42.90 o 2 6 8 10032.10 9906.33 28.58 o 4 6 8 13690.30 13615.40 35.56 o 6 6 8 13077.60 12633.30 49.59 o 0 8 8 53377.80 53942.90 160.74 o 2 8 8 29933.70 29543.90 82.77 o 4 8 8 37930.00 36603.80 102.60 o 6 8 8 14300.10 13699.60 56.89 o 8 8 8 15487.40 14240.20 108.38 o 1 1 9 3983.48 3884.78 22.51 o 1 3 9 95.98 114.65 5.32 o 3 3 9 1321.13 1477.15 15.98 o 1 5 9 7104.53 7126.96 24.62 o 3 5 9 1535.18 1540.50 12.99 o 5 5 9 9361.79 9135.32 42.01 o 1 7 9 116.12 150.92 7.15 o 3 7 9 1837.80 1876.90 14.15 o 5 7 9 199.66 222.98 8.07 o 7 7 9 2005.63 1941.91 22.31 o 1 9 9 2954.20 2981.68 25.07 o 3 9 9 640.56 637.75 15.39 o 5 9 9 4236.51 4252.75 34.42 o 7 9 9 93.53 141.10 13.48 o 9 9 9 2219.60 2165.27 49.46 o 0 0 10 157.83 271.06 18.80 o 0 2 10 46666.10 44045.10 99.50 o 2 2 10 65492.80 61802.20 129.77 o 0 4 10 139.04 170.72 9.90 o 2 4 10 31216.60 29814.00 56.46 o 4 4 10 908.03 934.11 15.48 o 0 6 10 41409.80 41490.70 101.49 o 2 6 10 32405.80 32350.30 63.71 o 4 6 10 29177.20 27566.90 61.01 o 6 6 10 16318.00 15450.10 63.54 o 0 8 10 2134.89 2188.31 23.15 o 2 8 10 10913.80 10921.90 36.34 o 4 8 10 3033.08 3012.56 20.57 o 6 8 10 11629.30 11265.40 38.86 o 8 8 10 4301.68 4162.38 37.50 o 0 10 10 27455.40 27546.10 120.65 o 2 10 10 10460.30 10948.30 51.87 o 4 10 10 20588.90 20400.40 81.09 o 6 10 10 5329.71 5136.67 39.52 o 8 10 10 9599.26 9151.19 62.05 o 10 10 10 1720.31 1760.52 55.86 o 1 1 11 746.16 685.56 13.23 o 1 3 11 3627.44 3493.20 18.83 o 3 3 11 7963.25 7760.74 40.56 o 1 5 11 4.88 87.19 8.65 o 3 5 11 734.46 688.04 10.74 o 5 5 11 516.34 569.32 15.31 o 1 7 11 3330.65 3363.87 20.91 o 3 7 11 6321.15 6252.63 28.10 o 5 7 11 994.38 957.84 13.65 o 7 7 11 5155.85 5005.60 38.01 o 1 9 11 3.36 71.05 10.32 o 3 9 11 355.48 364.27 10.73 o 5 9 11 271.49 284.30 10.57 o 7 9 11 526.92 505.26 12.81 o 9 9 11 158.72 169.14 16.31 o 1 11 11 927.17 918.88 20.39 o 3 11 11 2087.00 2077.57 28.73 o 5 11 11 214.44 277.06 18.22 o 7 11 11 1928.91 1883.88 27.97 o 9 11 11 122.99 141.85 16.22 o 11 11 11 762.82 790.16 37.61 o 0 0 12 50948.10 47192.50 235.60 o 0 2 12 19271.60 18684.90 64.38 o 2 2 12 647.68 605.22 14.73 o 0 4 12 37050.10 35340.60 97.56 o 2 4 12 19343.20 18688.60 49.54 o 4 4 12 27059.30 25700.70 84.90 o 0 6 12 9022.83 9111.72 47.50 o 2 6 12 2105.98 2080.70 17.48 o 4 6 12 9588.40 9464.70 37.33 o 6 6 12 3393.42 3290.50 32.74 o 0 8 12 16045.10 16481.70 66.97 o 2 8 12 16774.30 17505.50 50.74 o 4 8 12 11793.80 11638.50 44.30 o 6 8 12 9314.30 9160.26 38.74 o 8 8 12 5156.27 4907.16 49.35 o 0 10 12 2577.48 2638.93 29.56 o 2 10 12 3124.15 3086.73 23.07 o 4 10 12 3029.17 3047.65 25.07 o 6 10 12 3810.59 3777.03 29.08 o 8 10 12 3558.39 3563.96 29.16 o 10 10 12 3713.87 3707.86 43.16 o 0 12 12 5686.81 6098.97 61.37 o 2 12 12 10534.00 11362.80 63.66 o 4 12 12 4199.15 4271.90 42.75 o 6 12 12 6464.79 6554.19 47.54 o 8 12 12 1827.16 1891.87 32.39 o 10 12 12 2892.14 2846.60 33.32 o 12 12 12 638.40 699.00 38.03 o 1 1 13 65.19 122.63 12.15 o 1 3 13 293.49 310.18 9.98 o 3 3 13 1586.11 1612.20 23.06 o 1 5 13 606.47 652.06 12.32 o 3 5 13 4.99 78.04 11.40 o 5 5 13 1362.46 1426.20 23.97 o 1 7 13 530.72 526.22 11.48 o 3 7 13 1659.82 1650.39 17.48 o 5 7 13 44.04 94.01 11.31 o 7 7 13 1641.62 1645.98 30.14 o 1 9 13 319.60 354.70 11.40 o 3 9 13 2.18 72.13 13.98 o 5 9 13 762.97 813.63 16.64 o 7 9 13 26.75 70.72 13.14 o 9 9 13 465.01 458.98 19.14 o 1 11 13 107.25 140.02 10.73 o 3 11 13 535.22 528.39 14.31 o 5 11 13 0.75 66.31 15.14 o 7 11 13 605.26 634.42 16.06 o 9 11 13 0.63 63.06 13.98 o 11 11 13 215.31 202.09 16.72 o 1 13 13 6.60 73.46 18.72 o 3 13 13 69.87 94.18 16.72 o 5 13 13 108.06 113.73 14.73 o 7 13 13 129.57 132.87 14.56 o 9 13 13 71.13 80.53 14.48 o 11 13 13 30.01 52.25 16.14 o 13 13 13 1.28 32.36 40.52 < 0 0 14 67.15 117.31 27.62 o 0 2 14 18395.30 17835.00 73.82 o 2 2 14 16827.20 16679.50 72.01 o 0 4 14 14.72 87.02 15.14 o 2 4 14 13445.80 13049.50 44.99 o 4 4 14 174.84 202.17 14.56 o 0 6 14 17215.20 17406.00 77.48 o 2 6 14 9283.40 9452.67 38.16 o 4 6 14 12999.60 12997.70 48.25 o 6 6 14 5046.91 5016.22 46.60 o 0 8 14 519.13 523.90 19.22 o 2 8 14 5823.39 5975.21 34.94 o 4 8 14 825.67 832.63 16.31 o 6 8 14 6141.74 6139.38 35.28 o 8 8 14 1432.97 1387.89 25.14 o 0 10 14 12922.60 13673.90 74.01 o 2 10 14 3482.94 3672.66 27.49 o 4 10 14 10156.20 10731.90 47.45 o 6 10 14 1827.08 1850.42 22.23 o 8 10 14 5322.36 5350.14 30.43 o 10 10 14 606.78 609.37 19.31 o 0 12 14 841.80 902.21 23.39 o 2 12 14 2075.75 2223.61 22.48 o 4 12 14 1061.11 1050.76 15.98 o 6 12 14 2411.09 2488.60 21.15 o 8 12 14 1424.54 1360.22 17.65 o 10 12 14 2336.59 2329.37 20.65 o 12 12 14 1299.49 1175.83 25.72 o 0 14 14 7049.17 7394.63 68.07 o 2 14 14 1346.68 1390.73 23.64 o 4 14 14 5699.68 5922.38 43.86 o 6 14 14 703.64 733.47 18.81 o 8 14 14 3209.06 3151.86 33.32 o 10 14 14 229.81 207.51 15.48 o 12 14 14 1520.89 1118.36 75.02 o 1 1 15 28.89 93.09 15.72 o 1 3 15 160.76 168.64 10.07 o 3 3 15 852.77 844.37 20.22 o 1 5 15 322.08 332.23 11.81 o 3 5 15 2.77 71.80 13.56 o 5 5 15 774.77 800.99 22.97 o 1 7 15 291.28 307.44 12.65 o 3 7 15 929.96 936.94 15.40 o 5 7 15 21.86 81.36 12.98 o 7 7 15 952.97 954.18 21.89 o 1 9 15 199.10 206.34 11.90 o 3 9 15 2.40 71.46 13.56 o 5 9 15 488.31 487.11 13.56 o 7 9 15 11.60 60.48 12.06 o 9 9 15 325.22 315.01 16.14 o 1 11 15 54.61 112.06 11.48 o 3 11 15 305.98 335.23 11.57 o 5 11 15 2.03 54.24 12.73 o 7 11 15 354.76 355.37 11.48 o 9 11 15 2.16 39.27 12.98 o 11 11 15 120.90 137.11 14.39 o 1 13 15 7.86 53.49 12.81 o 3 13 15 35.48 64.98 9.90 o 5 13 15 84.85 98.59 10.15 o 7 13 15 70.48 87.94 9.23 o 9 13 15 60.16 61.56 9.90 o 11 13 15 13.05 28.37 13.64 < 1 15 15 10.89 42.18 14.97 < 3 15 15 14.66 44.84 14.48 o 5 15 15 73.09 54.74 14.14 o 7 15 15 34.41 37.60 16.72 < 9 15 15 53.91 36.11 26.96 < 0 0 16 14931.70 13860.20 151.56 o 0 2 16 6423.30 6338.01 51.88 o 2 2 16 357.39 336.65 18.97 o 0 4 16 11495.50 11334.20 73.63 o 2 4 16 6667.29 6727.12 38.62 o 4 4 16 8829.55 8839.54 53.93 o 0 6 16 3442.85 3534.80 35.32 o 2 6 16 845.55 858.60 16.23 o 4 6 16 3731.18 3803.59 28.99 o 6 6 16 1323.48 1313.49 24.47 o 0 8 16 5695.00 5986.17 47.11 o 2 8 16 6437.90 6842.30 34.11 o 4 8 16 4336.16 4717.61 33.50 o 6 8 16 3914.45 4083.16 28.16 o 8 8 16 2063.84 2091.10 28.06 o 0 10 16 1220.29 1333.82 24.14 o 2 10 16 1260.65 1291.31 16.40 o 4 10 16 1428.14 1498.41 17.06 o 6 10 16 1590.74 1572.25 17.56 o 8 10 16 1721.07 1745.07 18.56 o 10 10 16 1662.18 1658.38 24.81 o 0 12 16 2328.60 2369.33 29.64 o 2 12 16 4678.86 4836.83 27.50 o 4 12 16 1756.04 1801.20 18.23 o 6 12 16 3040.11 3076.55 22.41 o 8 12 16 807.59 841.86 14.15 o 10 12 16 1482.88 1405.88 19.98 o 0 14 16 485.01 500.42 15.31 o 2 14 16 940.19 953.00 14.15 o 4 14 16 594.38 593.23 13.40 o 6 14 16 1117.51 1083.27 18.48 o 8 14 16 777.43 722.63 22.72 o 0 16 16 1072.79 1142.15 56.02 o 2 16 16 2336.01 2401.77 57.05 o 4 16 16 820.81 994.16 81.73 o 1 1 17 119.44 133.45 14.48 o 1 3 17 555.25 533.14 14.31 o 3 3 17 1249.59 1169.29 24.55 o 1 5 17 0.39 60.48 14.23 o 3 5 17 140.12 158.74 10.32 o 5 5 17 78.13 99.34 16.22 o 1 7 17 624.82 658.14 15.15 o 3 7 17 1217.78 1294.37 19.39 o 5 7 17 215.61 236.79 11.07 o 7 7 17 1164.12 1175.14 22.47 o 1 9 17 0.28 60.40 13.39 o 3 9 17 90.40 107.24 9.90 o 5 9 17 50.52 75.62 10.65 o 7 9 17 142.38 139.61 9.90 o 9 9 17 33.35 62.65 15.56 o 1 11 17 230.92 243.20 10.48 o 3 11 17 524.08 535.29 12.32 o 5 11 17 60.25 78.20 9.82 o 7 11 17 531.94 534.13 12.40 o 9 11 17 40.68 54.58 10.98 o 11 11 17 237.92 235.97 28.62 o 1 13 17 37.15 58.24 9.57 o 3 13 17 163.15 151.34 9.40 o 5 13 17 0.30 35.19 12.81 < 7 13 17 192.38 164.99 12.56 o 1 15 17 18.14 25.29 18.47 < 3 15 17 94.86 111.90 22.88 o 0 0 18 14.96 88.77 29.78 < 0 2 18 5250.76 4989.23 41.43 o 2 2 18 5894.18 5635.94 50.62 o 0 4 18 85.53 126.71 16.89 o 2 4 18 3996.01 4109.33 30.41 o 4 4 18 197.51 204.67 14.64 o 0 6 18 5325.18 5370.65 41.35 o 2 6 18 3610.33 3636.42 24.74 o 4 6 18 4156.44 4263.31 26.42 o 6 6 18 2164.59 2191.83 27.64 o 0 8 18 361.99 383.74 16.31 o 2 8 18 1904.14 2044.50 19.90 o 4 8 18 503.66 494.35 12.23 o 6 8 18 2125.26 2221.35 19.73 o 8 8 18 782.22 700.37 18.47 o 0 10 18 4517.99 4772.83 40.00 o 2 10 18 1598.49 1625.61 18.73 o 4 10 18 3627.46 3760.32 24.91 o 6 10 18 923.39 928.70 14.73 o 8 10 18 2001.41 1959.19 22.90 o 10 10 18 368.95 333.08 24.21 o 0 12 18 508.86 485.87 18.56 o 2 12 18 754.66 784.34 14.98 o 4 12 18 613.12 570.10 14.81 o 6 12 18 910.91 905.35 19.23 o 8 12 18 782.70 599.40 28.88 o 0 14 18 2741.68 2646.46 64.14 o 2 14 18 718.92 685.67 33.37 o 4 14 18 2240.67 2392.84 204.15 o 1 1 19 133.32 131.62 13.31 o 1 3 19 2.84 61.81 12.81 o 3 3 19 60.29 101.58 15.56 o 1 5 19 324.59 347.04 10.90 o 3 5 19 76.42 98.17 9.90 o 5 5 19 546.12 523.98 16.89 o 1 7 19 4.73 47.50 12.06 o 3 7 19 101.86 103.75 9.48 o 5 7 19 19.29 48.00 10.07 o 7 7 19 135.85 150.26 12.40 o 1 9 19 227.68 225.97 10.07 o 3 9 19 56.73 69.14 9.57 o 5 9 19 381.50 346.22 11.57 o 7 9 19 15.85 33.69 11.98 < 9 9 19 270.17 213.09 22.38 o 1 11 19 3.29 32.53 12.73 < 3 11 19 20.10 39.52 13.23 < 5 11 19 43.32 45.67 12.98 o 7 11 19 37.58 37.60 18.64 < 1 13 19 47.88 41.93 23.21 < 0 0 20 5475.54 5009.16 88.79 o 0 2 20 1619.38 1554.62 25.22 o 2 2 20 343.13 367.18 16.06 o 0 4 20 4405.76 4374.95 37.25 o 2 4 20 1764.33 1698.39 17.65 o 4 4 20 3532.01 3525.74 34.24 o 0 6 20 897.91 892.98 18.64 o 2 6 20 562.19 578.57 11.65 o 4 6 20 1020.62 1008.88 14.56 o 6 6 20 764.77 783.43 19.56 o 0 8 20 2447.03 2524.80 30.40 o 2 8 20 1895.19 1883.77 19.82 o 4 8 20 1942.14 1979.42 22.23 o 6 8 20 1181.48 1138.34 19.48 o 8 8 20 1038.56 890.72 46.36 o 0 10 20 332.12 332.74 20.47 o 2 10 20 729.49 703.96 16.48 o 4 10 20 408.21 369.53 18.97 o 6 10 20 866.92 839.40 96.63 o 1 1 21 94.39 121.13 13.06 o 1 3 21 274.98 270.24 9.73 o 3 3 21 532.19 541.45 16.56 o 1 5 21 12.56 50.42 10.32 o 3 5 21 100.10 113.23 9.40 o 5 5 21 3.09 29.62 16.56 < 1 7 21 299.53 293.79 11.98 o 3 7 21 523.86 506.02 15.14 o 5 7 21 129.46 115.90 13.81 o 1 9 21 9.01 42.93 23.63 < 3 9 21 69.39 76.12 19.80 o 0 0 22 99.82 141.35 35.44 o 0 2 22 1265.84 1288.35 27.39 o 2 2 22 2405.89 2466.13 34.48 o 0 4 22 163.66 142.85 16.06 o 2 4 22 964.57 925.01 18.56 o 4 4 22 233.46 215.33 20.38 o 0 6 22 1361.41 1271.95 40.04 o 2 6 22 1610.68 1565.36 32.39 o 1 1 23 55.53 49.25 19.97 <