#------------------------------------------------------------------------------ #$Date: 2025-03-14 05:04:30 +0200 (Fri, 14 Mar 2025) $ #$Revision: 298434 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/02/34/2023443.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2023443 _cell_angle_alpha 90 _cell_angle_beta 90 _cell_angle_gamma 90 _cell_length_a 8.75451(10) _cell_length_b 8.75451(10) _cell_length_c 8.75451(10) _exptl_crystal_F_000 1316 _reflns_d_resolution_high 0.3781 _cod_data_source_file dk5135430Ksup19.hkl _cod_data_source_block 430K _shelx_title ' ' _shelx_refln_list_code 4 _shelx_f_calc_maximum 970.93 _shelx_f_squared_multiplier 1.000 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, z' '-x, y, -z' 'x, -y, -z' 'z, x, y' 'z, -x, -y' '-z, -x, y' '-z, x, -y' 'y, z, x' '-y, z, -x' 'y, -z, -x' '-y, -z, x' 'y, x, -z' '-y, -x, -z' 'y, -x, z' '-y, x, z' 'x, z, -y' '-x, z, y' '-x, -z, -y' 'x, -z, y' 'z, y, -x' 'z, -y, x' '-z, y, x' '-z, -y, -x' '-x, -y, -z' 'x, y, -z' 'x, -y, z' '-x, y, z' '-z, -x, -y' '-z, x, y' 'z, x, -y' 'z, -x, y' '-y, -z, -x' 'y, -z, x' '-y, z, x' 'y, z, -x' '-y, -x, z' 'y, x, z' '-y, x, -z' 'y, -x, -z' '-x, -z, y' 'x, -z, -y' 'x, z, y' '-x, z, -y' '-z, -y, x' '-z, y, -x' 'z, -y, -x' 'z, y, x' 'x, y+1/2, z+1/2' '-x, -y+1/2, z+1/2' '-x, y+1/2, -z+1/2' 'x, -y+1/2, -z+1/2' 'z, x+1/2, y+1/2' 'z, -x+1/2, -y+1/2' '-z, -x+1/2, y+1/2' '-z, x+1/2, -y+1/2' 'y, z+1/2, x+1/2' '-y, z+1/2, -x+1/2' 'y, -z+1/2, -x+1/2' '-y, -z+1/2, x+1/2' 'y, x+1/2, -z+1/2' '-y, -x+1/2, -z+1/2' 'y, -x+1/2, z+1/2' '-y, x+1/2, z+1/2' 'x, z+1/2, -y+1/2' '-x, z+1/2, y+1/2' '-x, -z+1/2, -y+1/2' 'x, -z+1/2, y+1/2' 'z, y+1/2, -x+1/2' 'z, -y+1/2, x+1/2' '-z, y+1/2, x+1/2' '-z, -y+1/2, -x+1/2' '-x, -y+1/2, -z+1/2' 'x, y+1/2, -z+1/2' 'x, -y+1/2, z+1/2' '-x, y+1/2, z+1/2' '-z, -x+1/2, -y+1/2' '-z, x+1/2, y+1/2' 'z, x+1/2, -y+1/2' 'z, -x+1/2, y+1/2' '-y, -z+1/2, -x+1/2' 'y, -z+1/2, x+1/2' '-y, z+1/2, x+1/2' 'y, z+1/2, -x+1/2' '-y, -x+1/2, z+1/2' 'y, x+1/2, z+1/2' '-y, x+1/2, -z+1/2' 'y, -x+1/2, -z+1/2' '-x, -z+1/2, y+1/2' 'x, -z+1/2, -y+1/2' 'x, z+1/2, y+1/2' '-x, z+1/2, -y+1/2' '-z, -y+1/2, x+1/2' '-z, y+1/2, -x+1/2' 'z, -y+1/2, -x+1/2' 'z, y+1/2, x+1/2' 'x+1/2, y, z+1/2' '-x+1/2, -y, z+1/2' '-x+1/2, y, -z+1/2' 'x+1/2, -y, -z+1/2' 'z+1/2, x, y+1/2' 'z+1/2, -x, -y+1/2' '-z+1/2, -x, y+1/2' '-z+1/2, x, -y+1/2' 'y+1/2, z, x+1/2' '-y+1/2, z, -x+1/2' 'y+1/2, -z, -x+1/2' '-y+1/2, -z, x+1/2' 'y+1/2, x, -z+1/2' '-y+1/2, -x, -z+1/2' 'y+1/2, -x, z+1/2' '-y+1/2, x, z+1/2' 'x+1/2, z, -y+1/2' '-x+1/2, z, y+1/2' '-x+1/2, -z, -y+1/2' 'x+1/2, -z, y+1/2' 'z+1/2, y, -x+1/2' 'z+1/2, -y, x+1/2' '-z+1/2, y, x+1/2' '-z+1/2, -y, -x+1/2' '-x+1/2, -y, -z+1/2' 'x+1/2, y, -z+1/2' 'x+1/2, -y, z+1/2' '-x+1/2, y, z+1/2' '-z+1/2, -x, -y+1/2' '-z+1/2, x, y+1/2' 'z+1/2, x, -y+1/2' 'z+1/2, -x, y+1/2' '-y+1/2, -z, -x+1/2' 'y+1/2, -z, x+1/2' '-y+1/2, z, x+1/2' 'y+1/2, z, -x+1/2' '-y+1/2, -x, z+1/2' 'y+1/2, x, z+1/2' '-y+1/2, x, -z+1/2' 'y+1/2, -x, -z+1/2' '-x+1/2, -z, y+1/2' 'x+1/2, -z, -y+1/2' 'x+1/2, z, y+1/2' '-x+1/2, z, -y+1/2' '-z+1/2, -y, x+1/2' '-z+1/2, y, -x+1/2' 'z+1/2, -y, -x+1/2' 'z+1/2, y, x+1/2' 'x+1/2, y+1/2, z' '-x+1/2, -y+1/2, z' '-x+1/2, y+1/2, -z' 'x+1/2, -y+1/2, -z' 'z+1/2, x+1/2, y' 'z+1/2, -x+1/2, -y' '-z+1/2, -x+1/2, y' '-z+1/2, x+1/2, -y' 'y+1/2, z+1/2, x' '-y+1/2, z+1/2, -x' 'y+1/2, -z+1/2, -x' '-y+1/2, -z+1/2, x' 'y+1/2, x+1/2, -z' '-y+1/2, -x+1/2, -z' 'y+1/2, -x+1/2, z' '-y+1/2, x+1/2, z' 'x+1/2, z+1/2, -y' '-x+1/2, z+1/2, y' '-x+1/2, -z+1/2, -y' 'x+1/2, -z+1/2, y' 'z+1/2, y+1/2, -x' 'z+1/2, -y+1/2, x' '-z+1/2, y+1/2, x' '-z+1/2, -y+1/2, -x' '-x+1/2, -y+1/2, -z' 'x+1/2, y+1/2, -z' 'x+1/2, -y+1/2, z' '-x+1/2, y+1/2, z' '-z+1/2, -x+1/2, -y' '-z+1/2, x+1/2, y' 'z+1/2, x+1/2, -y' 'z+1/2, -x+1/2, y' '-y+1/2, -z+1/2, -x' 'y+1/2, -z+1/2, x' '-y+1/2, z+1/2, x' 'y+1/2, z+1/2, -x' '-y+1/2, -x+1/2, z' 'y+1/2, x+1/2, z' '-y+1/2, x+1/2, -z' 'y+1/2, -x+1/2, -z' '-x+1/2, -z+1/2, y' 'x+1/2, -z+1/2, -y' 'x+1/2, z+1/2, y' '-x+1/2, z+1/2, -y' '-z+1/2, -y+1/2, x' '-z+1/2, y+1/2, -x' 'z+1/2, -y+1/2, -x' 'z+1/2, y+1/2, x' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 1 1 2214.27 2144.92 11.28 o 0 0 2 19864.60 24189.40 57.70 o 2 0 2 88383.50 94797.30 97.31 o 2 2 2 760340.00 942704.00 1079.28 o 1 1 3 6516.87 8321.48 15.58 o 3 1 3 31891.60 34363.40 40.81 o 3 3 3 65916.90 64470.60 129.68 o 0 0 4 830682.00 823350.00 1559.41 o 2 0 4 28541.00 30975.30 36.20 o 2 2 4 37725.30 41776.90 48.66 o 4 0 4 494562.00 465231.00 502.49 o 4 2 4 34519.70 34856.70 52.14 o 4 4 4 312136.00 279057.00 454.57 o 1 1 5 12720.20 12672.90 24.89 o 3 1 5 218.61 207.88 3.06 o 3 3 5 4386.69 5046.33 16.94 o 5 1 5 21011.20 20507.30 41.54 o 5 3 5 4361.54 4390.08 18.24 o 5 5 5 25323.00 24515.30 105.78 o 0 0 6 1070.63 1134.48 16.68 o 2 0 6 75477.80 76481.40 88.12 o 2 2 6 277852.00 254295.00 217.41 o 4 0 6 4791.60 4926.69 19.05 o 4 2 6 42665.40 42573.20 48.20 o 4 4 6 9022.85 9308.13 29.62 o 6 0 6 67737.20 65486.40 147.35 o 6 2 6 119893.00 115144.00 155.10 o 6 4 6 43022.00 42473.60 89.35 o 6 6 6 55337.10 56579.80 205.98 o 1 1 7 6769.42 6941.03 23.25 o 3 1 7 20259.80 20604.00 29.62 o 3 3 7 37094.10 35239.30 63.25 o 5 1 7 316.18 368.58 6.04 o 5 3 7 4781.90 4951.85 17.65 o 5 5 7 506.91 531.66 11.57 o 7 1 7 14047.50 13991.30 47.62 o 7 3 7 23374.00 23699.10 69.51 o 7 5 7 4455.59 4417.17 28.58 o 7 7 7 15802.30 15550.80 99.33 o 0 0 8 220799.00 193902.00 499.73 o 2 0 8 34191.40 33793.70 64.77 o 2 2 8 4876.57 5159.37 23.50 o 4 0 8 148029.00 137151.00 189.11 o 4 2 8 35923.10 34805.80 55.06 o 4 4 8 100915.00 92406.60 153.08 o 6 0 8 12243.30 12126.60 46.62 o 6 2 8 10321.50 10165.60 29.61 o 6 4 8 14309.70 13947.00 37.57 o 6 6 8 13392.40 12868.80 51.38 o 8 0 8 53326.00 53219.00 172.17 o 8 2 8 30946.40 31356.90 87.89 o 8 4 8 37559.80 36724.70 99.85 o 8 6 8 14666.10 14276.50 60.47 o 8 8 8 14931.80 14578.20 119.34 o 1 1 9 4020.14 3939.79 23.19 o 3 1 9 97.51 119.50 5.82 o 3 3 9 1329.03 1488.77 17.62 o 5 1 9 7199.67 7034.59 25.77 o 5 3 9 1562.68 1544.79 13.98 o 5 5 9 9440.62 9061.77 43.77 o 7 1 9 107.90 153.92 8.22 o 7 3 9 1804.27 1842.90 15.37 o 7 5 9 208.10 238.79 9.02 o 7 7 9 1930.33 1951.10 24.47 o 9 1 9 2957.59 3019.19 28.42 o 9 3 9 648.60 643.26 17.18 o 9 5 9 4159.70 4107.88 35.72 o 9 7 9 95.06 146.13 16.16 o 9 9 9 2081.48 2037.72 55.06 o 0 0 10 120.39 224.01 19.36 o 2 0 10 47826.00 45391.10 103.09 o 2 2 10 66679.50 61520.70 143.51 o 4 0 10 187.87 218.99 11.57 o 4 2 10 31923.90 30255.80 62.21 o 4 4 10 1036.05 1002.30 17.40 o 6 0 10 42241.00 40536.90 100.14 o 6 2 10 32506.60 31496.40 66.17 o 6 4 10 29600.80 28974.50 63.72 o 6 6 10 16066.10 15636.60 67.02 o 8 0 10 2299.96 2254.13 24.55 o 8 2 10 11072.20 11041.20 38.52 o 8 4 10 3194.95 3141.08 22.08 o 8 6 10 11573.50 11162.60 41.90 o 8 8 10 4299.08 4196.94 40.82 o 10 0 10 27142.00 28124.80 135.38 o 10 2 10 10119.00 10331.40 55.17 o 10 4 10 20142.10 20042.30 85.48 o 10 6 10 5043.28 5006.63 44.63 o 10 8 10 9076.90 8859.51 69.76 o 10 10 10 1562.41 1584.43 61.97 o 1 1 11 716.06 704.07 15.14 o 3 1 11 3577.77 3499.58 20.26 o 3 3 11 7890.08 7665.01 42.71 o 5 1 11 6.57 87.98 10.19 o 5 3 11 712.02 694.89 12.23 o 5 5 11 516.18 548.89 17.54 o 7 1 11 3249.35 3250.39 21.71 o 7 3 11 6152.46 6088.50 29.91 o 7 5 11 956.95 934.18 15.07 o 7 7 11 4885.21 4821.22 41.05 o 9 1 11 3.59 80.85 12.15 o 9 3 11 334.98 351.61 11.86 o 9 5 11 255.20 278.53 12.52 o 9 7 11 486.27 464.67 14.85 o 9 9 11 139.57 166.88 21.61 o 11 1 11 876.29 907.73 23.15 o 11 3 11 1942.91 1946.49 29.50 o 11 5 11 204.60 246.43 22.20 o 11 7 11 1732.94 1719.85 31.61 o 11 9 11 112.43 141.04 21.10 o 11 11 11 652.57 591.07 41.64 o 0 0 12 50922.30 46489.20 253.04 o 2 0 12 19946.50 19103.90 70.51 o 2 2 12 708.69 649.03 15.94 o 4 0 12 36648.70 34749.80 104.52 o 4 2 12 19870.10 18884.00 50.77 o 4 4 12 26475.20 25304.70 92.97 o 6 0 12 9287.13 8954.81 53.32 o 6 2 12 2190.39 2108.49 19.45 o 6 4 12 9743.60 9404.36 40.70 o 6 6 12 3414.12 3240.21 36.07 o 8 0 12 15378.90 15816.90 70.08 o 8 2 12 16658.40 16745.60 51.51 o 8 4 12 11174.30 11120.90 44.81 o 8 6 12 9049.75 9012.56 43.46 o 8 8 12 4733.14 4681.38 52.79 o 10 0 12 2602.89 2630.15 33.51 o 10 2 12 3077.97 3063.13 24.99 o 10 4 12 2983.19 3005.47 28.34 o 10 6 12 3613.46 3711.67 32.36 o 10 8 12 3278.69 3316.26 33.52 o 10 10 12 3277.65 3253.18 51.74 o 12 0 12 5152.54 5498.64 64.98 o 12 2 12 9714.24 10289.30 63.28 o 12 4 12 3763.17 3940.06 47.67 o 12 6 12 5776.07 5884.45 49.97 o 12 8 12 1591.02 1592.37 36.92 o 12 10 12 2413.50 2344.50 39.04 o 12 12 12 527.34 535.35 41.49 o 1 1 13 69.83 117.39 14.99 o 3 1 13 275.80 308.59 10.84 o 3 3 13 1516.44 1564.33 25.56 o 5 1 13 602.40 622.50 13.54 o 5 3 13 6.22 93.44 14.05 o 5 5 13 1310.70 1327.50 26.07 o 7 1 13 490.33 501.07 13.39 o 7 3 13 1537.84 1508.22 18.79 o 7 5 13 37.86 99.85 13.75 o 7 7 13 1467.59 1402.10 33.86 o 9 1 13 305.37 331.45 13.61 o 9 3 13 2.98 97.95 18.05 o 9 5 13 698.30 698.24 18.56 o 9 7 13 21.10 105.45 18.34 o 9 9 13 402.79 408.18 24.67 o 11 1 13 94.57 147.08 13.10 o 11 3 13 467.16 487.31 16.60 o 11 5 13 0.61 80.34 19.72 o 11 7 13 508.76 519.49 18.49 o 11 9 13 0.51 61.13 16.88 o 11 11 13 172.77 183.18 19.87 o 13 1 13 7.31 80.27 23.72 o 13 3 13 52.67 97.88 22.49 o 13 5 13 94.40 142.57 19.50 o 13 7 13 97.24 116.95 18.27 o 13 9 13 59.79 72.48 21.32 o 13 11 13 21.11 64.77 21.69 < 13 13 13 1.85 46.14 49.78 < 0 0 14 37.06 138.78 35.95 o 2 0 14 18410.40 17575.90 76.62 o 2 2 14 16366.60 16038.30 78.31 o 4 0 14 31.93 101.23 17.76 o 4 2 14 13349.30 13066.60 49.24 o 4 4 14 217.67 241.41 17.69 o 6 0 14 16793.70 16413.10 78.19 o 6 2 14 8796.33 8756.64 40.61 o 6 4 14 12543.10 12284.90 50.11 o 6 6 14 4659.01 4762.45 52.50 o 8 0 14 554.36 579.55 22.78 o 8 2 14 5633.26 5773.13 39.61 o 8 4 14 836.07 870.30 18.85 o 8 6 14 5722.59 5736.12 39.25 o 8 8 14 1321.20 1308.67 28.98 o 10 0 14 11862.40 13337.80 85.13 o 10 2 14 3131.83 3333.61 29.95 o 10 4 14 9188.57 9484.24 49.82 o 10 6 14 1603.14 1680.50 23.38 o 10 8 14 4604.99 4666.59 34.05 o 10 10 14 507.64 477.41 23.44 o 12 0 14 782.91 856.30 25.77 o 12 2 14 1891.00 2086.22 25.56 o 12 4 14 952.66 985.07 18.42 o 12 6 14 2092.22 2159.64 23.31 o 12 8 14 1179.11 1151.59 19.88 o 12 10 14 1864.93 1821.06 23.45 o 12 12 14 968.74 879.82 28.90 o 14 0 14 5869.77 6440.24 78.27 o 14 2 14 1107.65 1168.31 27.01 o 14 4 14 4668.03 4954.80 48.34 o 14 6 14 562.73 596.58 22.35 o 14 8 14 2501.61 2483.60 38.24 o 14 10 14 172.42 159.02 19.72 o 14 12 14 1092.13 939.26 78.79 o 1 1 15 29.66 88.78 18.78 o 3 1 15 145.78 168.11 12.37 o 3 3 15 782.68 813.93 24.24 o 5 1 15 298.36 312.38 13.61 o 5 3 15 2.60 96.13 17.61 o 5 5 15 690.10 693.65 26.21 o 7 1 15 264.50 286.76 14.77 o 7 3 15 833.98 866.59 17.84 o 7 5 15 21.05 95.91 17.03 o 7 7 15 829.36 792.26 24.24 o 9 1 15 168.87 231.72 15.50 o 9 3 15 1.67 89.29 18.05 o 9 5 15 402.37 405.19 15.87 o 9 7 15 11.64 92.71 17.47 o 9 9 15 248.50 243.01 19.58 o 11 1 15 52.58 110.47 15.28 o 11 3 15 268.87 279.55 14.41 o 11 5 15 0.63 69.06 15.86 o 11 7 15 300.59 287.56 13.83 o 11 9 15 0.62 83.98 16.08 o 11 11 15 103.18 110.98 19.07 o 13 1 15 5.25 67.82 16.59 o 13 3 15 30.26 85.29 14.85 o 13 5 15 61.76 98.10 13.03 o 13 7 15 57.39 77.72 12.59 o 13 9 15 41.16 60.18 13.61 o 13 11 15 11.70 33.69 18.34 < 15 1 15 4.40 59.09 19.50 o 15 3 15 16.80 48.61 21.25 < 15 5 15 43.16 66.01 18.27 o 15 7 15 33.42 57.27 23.94 < 15 9 15 29.81 35.73 42.35 < 0 0 16 13938.30 13745.00 141.27 o 2 0 16 6302.03 6108.25 54.36 o 2 2 16 397.00 398.86 24.02 o 4 0 16 10581.00 10917.00 81.43 o 4 2 16 6407.63 6678.15 43.27 o 4 4 16 8015.03 8024.17 58.34 o 6 0 16 3314.10 3310.18 38.70 o 6 2 16 845.02 856.40 18.78 o 6 4 16 3503.12 3579.38 31.70 o 6 6 16 1238.58 1230.93 27.89 o 8 0 16 5033.73 5291.03 49.52 o 8 2 16 5820.36 6043.45 35.67 o 8 4 16 3782.56 3972.12 33.82 o 8 6 16 3431.31 3552.74 31.12 o 8 8 16 1734.04 1748.15 29.86 o 10 0 16 1119.58 1231.30 27.74 o 10 2 16 1133.99 1200.80 18.64 o 10 4 16 1268.15 1386.09 19.51 o 10 6 16 1357.72 1308.45 18.93 o 10 8 16 1410.83 1412.23 20.02 o 10 10 16 1303.02 1218.36 26.36 o 12 0 16 1922.65 2035.15 31.83 o 12 2 16 3841.06 4065.46 30.47 o 12 4 16 1431.40 1482.65 20.10 o 12 6 16 2408.19 2449.59 24.62 o 12 8 16 633.57 611.67 15.65 o 12 10 16 1093.35 997.92 21.92 o 14 0 16 393.95 396.82 18.63 o 14 2 16 753.58 785.17 16.45 o 14 4 16 467.77 474.86 15.43 o 14 6 16 854.17 821.18 21.77 o 14 8 16 567.69 458.30 23.95 o 16 0 16 793.67 778.67 60.93 o 16 2 16 1703.23 1719.74 56.15 o 16 4 16 596.84 594.30 47.54 o 1 1 17 114.13 131.58 18.34 o 3 1 17 502.61 479.23 16.74 o 3 3 17 1106.19 1121.95 28.98 o 5 1 17 0.47 95.26 19.87 o 5 3 17 125.38 142.79 12.88 o 5 5 17 62.16 112.00 21.47 o 7 1 17 534.28 531.87 16.89 o 7 3 17 1024.29 1109.82 20.97 o 7 5 17 179.82 197.45 12.66 o 7 7 17 932.26 957.98 24.53 o 9 1 17 0.25 77.58 17.10 o 9 3 17 72.79 104.50 12.81 o 9 5 17 40.44 86.60 13.97 o 9 7 17 108.40 110.91 12.23 o 9 9 17 27.04 61.20 20.01 o 11 1 17 182.80 195.26 13.03 o 11 3 17 408.85 402.42 14.12 o 11 5 17 46.37 75.98 13.39 o 11 7 17 396.73 352.71 13.61 o 11 9 17 28.36 54.22 14.70 o 11 11 17 167.02 120.52 29.62 o 13 1 17 24.31 60.11 13.46 o 13 3 17 113.83 123.86 12.74 o 13 5 17 0.11 42.64 20.45 < 13 7 17 129.88 109.53 15.79 o 15 1 17 13.64 63.68 34.64 < 15 3 17 69.32 76.20 25.91 < 0 0 18 30.02 81.21 39.37 < 2 0 18 4792.10 4781.49 46.67 o 2 2 18 5196.66 5145.06 54.55 o 4 0 18 104.78 132.60 20.09 o 4 2 18 3605.69 3769.41 33.74 o 4 4 18 205.94 222.34 20.45 o 6 0 18 4670.52 4770.11 43.75 o 6 2 18 3078.60 3217.67 27.03 o 6 4 18 3596.90 3674.93 28.71 o 6 6 18 1784.38 1864.84 30.88 o 8 0 18 331.56 386.40 19.43 o 8 2 18 1659.21 1750.05 21.77 o 8 4 18 438.79 434.24 13.68 o 8 6 18 1765.77 1823.09 20.46 o 8 8 18 617.37 594.77 20.60 o 10 0 18 3676.57 3912.99 41.62 o 10 2 18 1274.01 1336.43 18.57 o 10 4 18 2906.78 2944.29 26.67 o 10 6 18 709.48 681.42 15.43 o 10 8 18 1532.05 1477.55 24.83 o 10 10 18 261.29 178.75 33.12 o 12 0 18 394.64 382.05 19.87 o 12 2 18 610.90 635.90 17.18 o 12 4 18 462.67 451.35 18.12 o 12 6 18 700.59 645.34 22.57 o 12 8 18 552.14 498.93 38.58 o 14 0 18 2021.70 1853.93 59.66 o 14 2 18 513.41 456.11 27.95 o 14 4 18 1625.32 1843.68 212.10 o 1 1 19 115.45 135.58 17.61 o 3 1 19 3.00 82.31 15.43 o 3 3 19 46.54 83.54 19.14 o 5 1 19 262.39 281.66 13.25 o 5 3 19 61.03 91.62 12.95 o 5 5 19 423.21 388.09 19.29 o 7 1 19 4.06 63.24 16.45 o 7 3 19 81.55 109.38 12.66 o 7 5 19 13.08 59.53 13.68 o 7 7 19 108.71 102.10 17.10 o 9 1 19 167.16 157.49 11.50 o 9 3 19 39.39 76.48 12.44 o 9 5 19 273.11 227.00 12.66 o 9 7 19 8.96 26.49 15.28 < 9 9 19 180.64 124.82 34.50 o 11 1 19 1.17 45.92 17.39 < 11 3 19 19.04 49.70 16.88 < 11 5 19 25.51 36.31 17.39 < 11 7 19 33.28 26.20 28.60 < 13 1 19 30.37 54.87 45.05 < 0 0 20 4593.10 4441.61 96.09 o 2 0 20 1363.49 1336.55 27.67 o 2 2 20 337.99 325.26 19.21 o 4 0 20 3633.17 3566.38 41.10 o 4 2 20 1453.25 1468.39 19.08 o 4 4 20 2862.82 2812.43 34.90 o 6 0 20 737.04 787.92 22.57 o 6 2 20 492.49 490.29 14.05 o 6 4 20 817.68 828.57 15.58 o 6 6 20 619.64 608.24 22.27 o 8 0 20 1917.52 1872.62 30.01 o 8 2 20 1470.13 1451.61 20.61 o 8 4 20 1494.51 1441.02 21.48 o 8 6 20 888.28 819.02 21.55 o 8 8 20 755.77 569.96 39.68 o 10 0 20 257.23 265.07 21.83 o 10 2 20 558.06 510.34 20.89 o 10 4 20 307.75 259.33 23.44 o 10 6 20 630.75 519.41 54.96 o 1 1 21 78.11 110.47 16.16 o 3 1 21 217.02 194.68 11.35 o 3 3 21 410.54 386.63 18.78 o 5 1 21 10.68 61.78 15.65 o 5 3 21 77.17 86.82 12.23 o 5 5 21 2.06 43.37 24.67 < 7 1 21 221.79 213.97 13.97 o 7 3 21 383.62 326.22 16.09 o 7 5 21 92.63 71.03 16.52 o 9 1 21 6.04 20.52 27.65 < 9 3 21 48.11 56.47 29.47 < 0 0 22 97.74 102.18 33.77 o 2 0 22 967.84 987.28 27.81 o 2 2 22 1857.44 1881.19 34.67 o 4 0 22 142.67 137.84 18.78 o 4 2 22 729.06 706.79 19.00 o 4 4 22 188.78 171.25 24.31 o 6 0 22 1011.76 878.37 37.42 o 6 2 22 1190.91 1117.74 29.64 o 6 4 22 781.16 628.37 36.77 o 1 1 23 35.56 55.60 25.25 <